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Erika Sempana Ginting
universitas lampung
Materials Science & Nanotechnology Physics

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THE INFLUENCE OF ELECTRICAL VOLTAGE ON FORMATION OF SILICA NANO FIBER WITH ELECTROSPINNING METHOD Erika Sempana Ginting; Posman Manurung; Yanti Yulianti
Jurnal Teori dan Aplikasi Fisika Vol 10, No 1 (2022): Jurnal Teori dan Aplikasi Fisika
Publisher : Universitas Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/jtaf.v10i1.2907

Abstract

Silica nanofibers have been successfully fabricated using electrospinning method. Silica solution was prepared with molar rasio of tetraethyl orthosilicate (TEOS): ethanol: aquabides:hydrogen chloride (HCl) of 1 : 10 : 3 : 0.04. Polyvinyl alcohol (PVA) of 10% was added to solution. The solutions were then mixed with a ratio of silica: PVA solution of 2: 3 ml. The functional group of silica/PVA was characterized by Fourier transform Infrared Spectroscopy (FTIR). Morphology and elements analysis was tested by Scanning Electron Microscopy - Energy Dispersive Spectroscopy (SEM - EDS). The functional groups of silica/PVA solution formed are –OH, C-H, CH2, C=O, Si-O, and Si-O-Si which indicate the occurrence of cross-linking between silica and PVA. The functional groups shown in the solution are still visible on the silica nanofibers in the presence of C, O, and Si elements in the EDS results of the nanosilica fibers. The surface morphology shows that the silica nanofibers are more continuous and the beads are relatively less with increasing electrospinning voltage. The average fiber diameter by taking into account the estimated standard deviation, shows a graph with a linear trend and increasing the applied electrospinning voltage. Silica nanofibers with diameter range (80-150) nm are obtained
Co-Authors Posman Manurung Yanti Yulianti