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All Journal Journal of Aceh Physics Society PROSIDING SEMINAR KIMIA Jurnal Kimia Mulawarman Indonesian Journal of Chemistry Jurnal Natural

Binawati Ginting

Jurusan KimiaFakultas Matematika dan Ilmu Pengetahuan AlamUniversitas Mulawarman

Author-ID : 3048526

Agriculture, Biological Sciences & Forestry Astronomy Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Earth & Planetary Sciences Energy Immunology & microbiology Neuroscience Physics

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Articles

Instrumentation of realtime monitoring system towards level of C6H12O6, C2H5OH, CO2, temperature in tapai fermentation process Yuliani Yuliani; Khairi Suhud; Dedi Satria; Lelifajri Lelifajri; Binawati Ginting; Yuliani Aisyah; Fauzi Fauzi; Muhammad Syukri Surbakti
Journal of Aceh Physics Society Volume 10, Number 3, July 2021
Publisher : PSI-Aceh

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24815/jacps.v10i3.19161

Abstrak. Tapai merupakan makanan yang dihasilkan dari hasil fermentasi, salah satunya berbahan dasar dari ubi kayu. Fermentasi oleh ragi (saccharomyces serevesiae) menjadikan perubahan kimia pada substrat karena aktivitas enzim yang dihasilkan mikroorganisme. Parameter-parameter yang ditinjau adalah perubahan kadar C6H12O6, gas C2H5OH, gas CO2, suhu dan kelembapan dalam proses fermentasi melalui sistem pengukuran elektronik berbasis mikrokontroller Arduino Uno. Rangkaian sensor mengandung modul input yaitu sensor FC-28, sensor MQ-3, sensor MG-811, sensor DHT-11 dan modul pemroses mikrokontroler ATMEGA238 dengan sistem Arduino Uno dan pada komponen output menggunakan layar LCD 2X16. Kadar karakterisasi berdasarkan keluaran ADC (Analog to Digital Converter) untuk C6H12O6 adalah 535 untuk tapai ubi kayu. Kadar C6H12O6 akan terus menurun dari hari pertama sampai hari keempat yang mencapai 175 pada tapai ubi kayu. Diperoleh nilai akhir kadar gas C2H5OH yaitu 582. Kadar gas CO2 406 untuk tapai ubi. Selanjutnya nilai suhu 31oC untuk tapai ubi dengan nilai kelembaban 95RH. Waktu panen tapai dapat dipersingkat yaitu dari 7 hari menjadi 4 hari. Penelitian ini diharapkan dapat memberikan informasi pemakaian yang dapat dipergunakan untuk tampilan komposisi tapai secara komersial atau untuk tujuan kesehatan. Abstract. Tapai is food produced from fermentation, one of which is made from cassava. Fermentation by yeast (Saccharomyces serevesiae) causes chemical changes in the substrate due to the activity of enzymes produced by microorganisms. The parameters reviewed are changes in levels of C6H12O6, C2H5OH gas, CO2 gas, temperature and humidity in the fermentation process through an electronic measurement system based on the Arduino Uno microcontroller. The sensor circuit contains an input module, namely FC-28 sensor, MQ-3 sensor, MG-811 sensor, DHT-11 sensor and ATMEGA238 microcontroller processing module with the Arduino Uno system and the output component uses a 2X16 LCD screen. The grade based on the ADC (Analog to Digital Converter) output for the C6H12O6 is 535 for cassava tapai. Levels of C6H12O6 will continue to decline from the first day to the fourth day reaching 175 in cassava tapai. Obtained the final value of C2H5OH gas content is 582. CO2 gas content of 406 for cassava tapai. Furthermore, the temperature value of 31oC for cassava tapai with a humidity value of 95RH. The harvest time for tapai can be shortened from 7 days to 4 days. This research is expected to provide usage information that can be used to display tapai composition commercially or for health purposes. Keywords: fermentation, tapai, cassava, FC-28, MQ-3, MG-811, DHT11, Microcontroller.

AKTIVITAS ANTIOKSIDAN EKSTRAK KULIT BATANG ZIG-ZAG (Pedilanthus tithymaloides L. Poit) Binawati Ginting; Nurdin Nurdin; Juliawati Juliawati
PROSIDING SEMINAR KIMIA SEMINAR NASIONAL KIMIA 2018
Publisher : PROSIDING SEMINAR KIMIA

Show Abstract | Download Original | Original Source | Check in Google Scholar

Kulit batang Zig-Zag (Pedilanthus tithymaloides L. Poit) telah dilakukan isolasi dan uji aktivitas antioksidan. Kulit batang P. tithymaloides sebanyak 1,5 kg dimaserasi dengan metanol menghasilkan 72,15 g ekstrak metanol, ekstrak tersebut dipartisi dengan n-heksana dan diekstraksi dengan etil asetat, menghasilkan 35,59 g ekstrak n-heksana dan 12,79 g ekstrak etil asetat. Sisa hasil ekstraksi tersebut adalah ekstrak metanol sebanyak 22,79 g.Hasil uji fitokimia menunjukkan bahwa ekstrak n-heksana mengandung senyawa steroid dan terpenoid, ekstrak etil asetat dan ekstrak metanol mengandung alkaloid, terpenoid, steroid, saponin, flavonoid, kumarin dan fenolik. Uji aktivitas antioksidanekstrak n-heksana, etil asetat dan metanol terhadapradikal DPPH (1,1-diphenil-2-pycrilhydrazil) menunjukkan sifat antioksidan yang lemah dengan nilai IC50secara berturut-turut yaitu 230,92 ppm; 150,01 ppm; 259,62 ppm. Ekstrak etil asetat diisolasi dengan metode kromatografi kolom menggunakan fase diam silika gel G60 F254 dan fase gerak n-heksana : etil asetatsecara gradien elusi, diperoleh 6 fraksi gabungan yaitu PTEA-1 sampai PTEA-6. Hasil uji aktivitas antioksidan 6 fraksi gabungan menunjukkan bahwa fraksi PTEA-5 memiliki aktivitas antioksidan yang paling kuatdengan IC5097,45 ppm. Fraksi PTEA-2 yang memiliki berat yang lebih banyak dibandingkan PTEA-5 direkromatografi menggunakan kromatografi kolom sehingga diperoleh 91 subfraksi. Subfraksi 32-37 menghasilkan kristal berbentuk jarum.Berdasarkan hasil analisis fitokimiakristal tersebut diduga sebagai senyawa kumarin karena berflouroensensi di bawah UV λ365 nm. Kata Kunci: Tumbuhan Zig-Zag (Pedilanthus tithymaloides L. Poit), ekstrak etil asetat, antioksidan, 1,1-diphenyl-2-pycrilhidrazil (DPPH).

Isolation Of Antioxidant Compounds Of N-Hexane Extract Of Nutmeg (Myristica Fragrans Houtt) Leaves Binawati Ginting; Siti Hadijah; Hira Helwati
JURNAL KIMIA MULAWARMAN Vol 15 No 1 (2017)
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/jkm.v15i1.584

The isolation of antioxidant active compounds from n-hexane extract of nutmeg leaves (Myristica fragrans Houtt) with dipphenylpicrylhydrazyl (DPPH) has been carried out. n-Hexane extract of nutmeg leaves (0.35%) was obtained by partitioning of methanol extract (535.7 g) using n-hexane solvent. Isolation of active compound of n-hexane extract with gravitational column chromatography gradient elution of n-hexane : ethyl acetate with ratio (9 : 1) – (7 : 3) obtained 7 mixed fraction of MFHD1 - MFHD 7. MFHD 2 fraction further isolated obtained MFHD 2.1. The nutmeg n-hexane extracts and their fractions showed strong antioxidant activity with IC50 values <100 ppm except MFHD 6 fraction showed for IC50 values of 114.95 ppm. The most potent antioxidant activity in MFHD 4 fraction with IC50 value of 0.729 ppm (compared with vitamin C value of IC50 7,875 ppm as positive control). The GC-MS analysis of the MFHA 2.1 fraction shows the presence of sitostenone and eucalyptol compounds, both of which have been reported to have been isolated from several different plants and have antioxidant activity.

Optimization of Polyurethane Membrane Physical Characteristics of Red Seaweed Biomass Using a Box-Behnken Design Salfauqi Nurman; Saiful Saiful; Binawati Ginting; Rahmi Rahmi; Marlina Marlina
Indonesian Journal of Chemistry Vol 21, No 4 (2021)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ijc.63649

The polyurethane membrane is used as a separator either by filtration or adsorption, and this process is significantly affected by its strength and physical condition. We synthesized polyurethane membranes using red seaweed with Gracilaria sp as a hydroxyl source. The Box-Behnken Design of the Response Surface Methodology (RSM) using Software Design Expert Version 10.0.3.0 with three factors (TRL, TDI, and Glycerin). The F-value of 0.42 suggests that the membrane is less fit, while the P-value of 75.10% indicates that the quadratic design model is suitable for data analysis of physical characteristics. The optimal physical characteristics were obtained at a composition of 0.233 g TRL, 2.675 g TDI, and 0.254 g glycerin with a physical point of 6.5 (strong and elastic). Optimal polyurethane membrane has good thermal and mechanical properties at temperatures of Tg 58 °C, Tm 322 °C, and Td 534 °C, as well as stress and nominal strain values of 69.3 MPa and 5.74%. Polyurethane membrane synthesized from red seaweed has good physical properties. The result of this research is the basis for the development of polyurethane membrane applications from red seaweed.

ISOLATION OF ANTIOXIDANT COMPOUNDS OF METHANOL EXTRACT OF NUTMEG LEAVES (Myristica fragrans Houtt) Nurmilasari Nurmilasari; Binawati Ginting; Hira Helwati
Jurnal Natural Volume 17, Number 1, March 2017
Publisher : Universitas Syiah Kuala

Abstract.The antioxidant activity from methanol extract of nutmeg leaves (Myristica fragrans Houtt) was performed using 2,2-diphenyl-1-picrylhydrazil (DPPH). Antioxidant assay using DPPH of the methanol extract at a concentration of 25 ppm, 50 ppm and 100 ppm, showed high antioxidant activity with IC50 = 36.31 ppm and Vitamin C showed antioxidant activity with IC50 = 3.657 ppm. The methanol extract of nutmeg leaves were partitioned with chloroform to obtain chloroform extract of the leaves with IC50 = 28.30 ppm. isolation of the active compounds from the chloroform extract of the nutmeg leaf using column chromatography yielded 6 mix fractions MFMD 1, MFMD 2, MFMD 3, MFMD 4, MFMD 5 and MFMD 6. The test results of antioxidant activity in very strong category is fractions MFMD 4, MFMD 3, MFMD 2, MFMD 6 and MFMD 5 with IC50 of each are 26.590 ppm, 27.239 ppm, 29.639 ppm, 39.766 ppm and 55.436 ppm, while antioxidant activity in a weak catagory is fraction MFMD 1 with IC50 is 126.270 ppm. This shows that the fraction of the leaf has a better inhibitory activity, because some of the active compound contained in the fraction can synergize in inhibiting free radicals, so that the IC50 value of the fraction is stronger than the extract. Keywords: Antioxidant, chromathography, Nutmeg (Myristica fragransHoutt), methanol extract, leaves

ANTIOXIDANT ACTIVITY OF ETHYL ACETATE EXTRACT OF NUTMEG (Myristica fragrans Houtt) STEM BARK Ilham Maulana; Binawati Ginting; Nurdin Nurdin; Saiful Fakri
Jurnal Natural Volume 19 Number 3, October 2019
Publisher : Universitas Syiah Kuala

Antioxidant activity test for the extract of ethyl acetate nutmeg stem bark (Myristica fragrans Houtt) was carried out using 2,2-diphenyl-1picrylhydrazil (DPPH). The test results of antioxidant activity of ethyl acetate nutmeg stem bark extract with DPPH method at a concentration of 25 ppm, 50 ppm and 100 ppm obtained IC50 value = 68.14 ppm with IC50 value of vitamin C (as positive control) 3.657 ppm. The results of column chromatographic separation of ethyl acetate nutmeg stem bark extract obtained 5 combined fractions namely MFEK 1, MFEK 2, MFEK 3, MFEK 4 and MFEK 5. The test results of the fraction antioxidant activity in a good category were the MFEK 1 fraction. The MFEK 2 fraction to MFEK 5 showed an antioxidant activity lower than compared to the ethyl acetate extract. This shows that the ethyl acetate nutmeg stem bark extract has a better inhibitory activity, because there are several active compounds contained in the extract which can inhibit free radicals, so the IC50 value of the extract is better than the fractions.

ANTIOXIDANT ACTIVITY OF N-HEXANE EXTRACT OF NUTMEG PLANTS FROM SOUTH ACEH PROVINCE Binawati Ginting; Mustanir Mustanir; Hira Helwati; Lydia Septa Desiyana; Eralisa Eralisa; Rohmat Mujahid
Jurnal Natural Volume 17, Number 1, March 2017
Publisher : Universitas Syiah Kuala

Abstract. It has tested the antioxidant activity of n-hexane extract respective roots, bark, fruit and seed crops of nutmeg against DPPH. Each extracted by maceration method with n-hexane. The extraction of each plant nutmeg with n-hexane extract obtained yield of n-hexane respectively 8,35%; 81,5%; 11,89% and 55,63%. The result of the antioxidant activity of n-hexane extract of each plant nutmeg against DPPH with a concentration of 25 ppm, 50 ppm and 100 ppm is obtained IC50, respectively, are 0,216 ppm, 63,755 ppm, 43,998 ppm and 11,599 ppm and positive control vitamin C ( IC50 = 3,657 ppm). Vitamin C is a standard compound is more often used than butyl for very high antioxidant activity. The antioxidant activity increases from high to low at the roots, seeds, fruits and bark of plants nutmeg in a row. Based on data GC-MS chemical components of each successive extracts of roots, bark, fruit and seeds are 41, 41, 44, 43 components of secondary metabolites. The main components of each part of the plant based on data from GC-MS are a 5-Octadecanoic acid, linalool, eugenol, myristicin, methoxyeugenol. The compounds are thought to play an active role in inhibiting free radicals from DPPH. n-Hexane extract nutmeg plant potential as an antioxidant. Keywords:Nutmeg (Myristica fragrans Houtt), n-hexane extract, Antioxidant, DPPH

Co-Authors Dedi Satria Eralisa Eralisa Fauzi Fauzi Hira Helwati Hira Helwati Ilham Maulana Juliawati Juliawati KHAIRI SUHUD Lelifajri Lelifajri Lydia Septa Desiyana Marlina Marlina Mustanir Mustanir Nurdin Nurdin Nurdin Nurdin Nurmilasari Nurmilasari Rahmi Rahmi Rohmat Mujahid Saiful Fakri Saiful Saiful Salfauqi Nurman, Salfauqi Siti Hadijah Surbakti, Muhammad Syukri Yuliani Aisyah Yuliani Yuliani

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