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All Journal Jurnal Ilmu Fisika Lensa : Jurnal Kependidikan Fisika Sainstek : Jurnal Sains dan Teknologi
Akrajas Ali Umar
University Kebangsaan Malaysia
Astronomy Computer Science & IT Earth & Planetary Sciences Education Materials Science & Nanotechnology Physics Other

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Sintesis Nanopartikel Titanium Dioksida Didoping Rhutenium Bajili, Abdil; Dahlan, Dahyunir; Umar, Akrajas Ali
Jurnal Ilmu Fisika Vol 8, No 2 (2016): JURNAL ILMU FISIKA
Publisher : Jurnal Ilmu Fisika

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (382.911 KB) | DOI: 10.25077/jif.8.2.54-59.2016

Abstract

Nanopartikel titanium dioksoda (TiO2) yang didoping ruthenium (Ru/TiO2) ditumbuhi dengan menggunakan metode penumbuhan Liquid Phase Deposition (LPD) telah berhasil dilakukan. Konsentrasi doping ruthenium yang digunakan adalah 2,5 mM. Variasi lama waktu penumbuhan dilakukan selama 3 jam, 5 jam, 7 jam dan 10 jam. Kemudian dilakukan karakterisasi Ultraviolet-visible, fotoelektron sinar-x dan teknik difraksi sinar-x. Energi gap yang didapatkan dengan waktu penumbuhan 3 jam dan 5 jam adalah 3,22 eV dan 3,28 eV. Sedangkan waktu penumbuhan 7 jam dan 10 jam adalah 3,16 eV dan 3,29 eV. Morfologi dari Ru/TiO2 bersifat nanopori dengan fasa adalah anatase. Kata kunci: Liquid Phase Deposition (LPD), nanopartikel Ru/TiO2, doping ruthenium, fase anatase. 
Pengaruh Lama Penumbuhan Titanium Dioksida Didoping Copper Terhadap Energi Gap Berli, Ade Usra; Dahlan, Dahyunir; Umar, Akrajas Ali
Jurnal Ilmu Fisika Vol 8, No 2 (2016): JURNAL ILMU FISIKA
Publisher : Jurnal Ilmu Fisika

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (187.812 KB) | DOI: 10.25077/jif.8.2.60-63.2016

Abstract

Deposisi lapisan TiO2 didoping Cu telah berhasil ditumbuhkan dengan menggunakan metoda Liquid Phase Deposition (LPD). Lapisan TiO2-Cu dibuat dengan menggunakan material Ammonium hexafluorotitanate ((NH4)2TiF6), Copper (II) Nitrate hydrate (Cu(NO3)2·xH2O), dan Hexamethylen tetramine (C6H12N4). Dalam penelitian ini dilakukan variasi lama penumbuhan lapisan yaitu 3 jam, 5 jam, 7 jam dan 10 jam. Lapisan TiO2-Cu dikarakterisasi menggunakan Spektrometri Ultraviolet-Visible (UV-Vis) untuk menentukan energi gap melalui spektra difusi reflektansi. Hasil energi gap yang diperoleh pada lapisan TiO2-Cu dengan variasi lama penumbuhan yaitu antara 3,26-3,30 eV.Kata kunci: Titanium dioksida (TiO2), Liquid Phase Deposition (LPD) dan doping 
EFEK KONSENTRASI Cu PADA STRUKTUR DAN SIFAT HANTARAN LISTRIK NANOPARTIKEL CuPt Imamora, Marjoni; R, Setia Erlila; Rahmi, Elvy; Maiyena, Sri; Umar, Akrajas Ali
Sainstek : Jurnal Sains dan Teknologi Vol 7, No 1 (2015)
Publisher : IAIN Batusangkar

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (492.139 KB) | DOI: 10.31958/js.v7i1.128

Abstract

The investigation of bimetallic CuPt Nanoparticles (CuPt NPs) with average diameters in the 196.7±98 nm range have been prepared by the Liquid phase deposition methods and synthesized directly on an indium tin oxide (ITO) substrate. CuPt NPs with  high surface defect grown on (ITO) surface were prepared via a simple immersion of the substrate into a solution contains 1 mM Potassium Hexachloro Platinate (K2PtCl6), 0.2 mM Anhydrous Copper (II) Sulfate (CuSO4) anhydrous, 0.01 M Sodium dodecyl sulfate (SDS) and 10 mM Formic acid for 4 h at room temperature. The modification of Cu2+ ion precursor play a role to determine the nanoparticles geometry obtained. The simultaneous reduction of metal ions leads to either a surface enriched with one component or an alloy type of structure depending on the bimetal composition. The bimetallic CuPt NPs dispersions are characterized by FESEM, EDX Mapping, XRD, HRTEM and XPS analysis.Key words: CuPt, Liquid phase deposition, Bimetallic CuPt NPs
APLIKASI SINTESIS TiO2 NANOPARTIKEL DALAM DEGRADASI FOTOKATALITIK METIL JINGGA Husna, Isramil; Umar, Akrajas Ali; Ramli, Muhammad Adam
Sainstek : Jurnal Sains dan Teknologi Vol 10, No 1 (2018)
Publisher : IAIN Batusangkar

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (324.546 KB) | DOI: 10.31958/js.v10i1.1203

Abstract

The development in textile industry results in the increase of the use of non-organic materials in human life, such as the use of dyes that cannot be decomposed naturally, such as the use of artificial dyes in textile industry and other similar fields. This implies that if those artificial dye are not carefully managed, they will have a definite impact on the environment, such as water pollution where those substances contaminate clean water and therefore will be very dangerous for human daily needs of water for drinking, bathing and other needs. This in turn will cause various diseases in living things and pollute nature as well. The purpose of this study is to figure out the effect of methyl orange degradation by the addition of TiO2 photocatalyst. In this study, 10 ppm orange methyl solution were used, where 5 ml of orange methyl were dissolved in 5 ml of water then added with TiO2 and then irradiated with UV for 180 minutes. By calculating the degradation of methyl orange every 10 minutes, which was measured using a UV-Vis spectrophotometer. The finding shows that the longer the irradiation takes place, the more desirable degradation of methyl orange is desired. The results obtained from 180 minutes are absorbance values that are worth 0.8 down to 0.3.
Pengaruh Doping Palladium (Pd) Terhadap Lapisan TiO2 dengan Metode LPD untuk Applikasi Fotoanoda Sel Surya DSSC Dwipanur, Andhika; Dahlan, Dahyunir; Firmawati, Nini; Umar, Akrajas Ali
Jurnal Ilmu Fisika Vol 12, No 1 (2020): Published in March 2020
Publisher : Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (794.519 KB) | DOI: 10.25077/jif.12.1.6-10.2020

Abstract

Lapisan TiO2 yang didoping Pd dengan metode deposisi fase cair (Liquid Phase Deposition, LPD) telah dilakukan. Adapun tujuan sintesis lapisan tersebut adalah untuk mendapatkan lapisan yang terdiri dari nanoplate yang akan diaplikasikan untuk fotoanoda sel surya. Sebagai larutan prekursor digunakan 0,5 M (NH4)2TiF6 dengan variasi doping Pd adalah 0; 6.25; 12.50; 25,00 dan 50,00 mM. Penumbuhan lapisan dilakukan pada suhu 900°C selama 9 jam.Didapatkan berturut-turut energi gap adalah 3,20; 3,25; 3,18; 3,16; dan 3,10 eV. Karakterisasi FESEM menunjukkan bahwa lapisan yang dihasilkan terdiri dari partikel berbentuk nanoplate yang tersebar merata di permukaan substrat ITO. Luas nanoplate yang dihasilkan di bawah 100 μm2 dengan ketebalan beberapa nanometer. Karakterisasi-karakterisasi ini menunjukkan bahwa lapisan TiO2 yang didoping oleh Pd sangat berpotensi sebagai photoanode untuk elektroda sel surya DSSC (Dye Sensitized Solar Cell).
SYNTHESIS AND CHARACTERIZATION OF TIO2 SEMICONDUCTOR DOPED BY AGNO3 AND THEIR APPLICATION AS PHOTOANODE IN DYE-SENSITIZED SOLAR CELLS Ali Umar, Marjoni Imamora; Faizil, Nanda; Umar, Akrajas Ali; Saad, Siti Khatijah Md
Lensa: Jurnal Kependidikan Fisika Vol 8, No 1: June 2020 (in Press)
Publisher : IKIP Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33394/j-lkf.v8i1.2728

Abstract

The use of Titanium dioxide (TiO2) semiconductors in Dye-Sensitized Solar Cells (DSSC) devices have been extensively studied and synthesized with various techniques to obtain optimal performance. The TiO2 semiconductors with optimal performance are influenced by the growth method, the time of growth, the shape of the microstructure, and the optical properties. In this study, it was reported about the effect of silver nanoparticles (AgNO3) doping onto TiO2 semiconductors on their microstructure, reflectance, and efficiency of the DSSC device. The synthesis of TiO2 was carried out using liquid phase deposition (LPD) and immersed into an AgNO3 solution with a variation of time namely 0.5 h, 1 h, 2 h, 4 h, and 6 h. The entire TiO2 + AgNO3 sample, then used as a photoanode on DSSC with plastisol as a counter electrode. Characterization of microstructure, reflectance, and DSSC performance was carried out by using field emission scanning electron microscopy (FESEM), Uv-Vis Spectrophotometer, and Gamry Instrument, respectively. The FESEM results show that AgNO3 has successfully grown on the ITO substrate in a spherical shape with an average particle diameter ranging from 1.52-2.29 ?m. From observations using the Uv-Vis Spectrophotometer, obtained the energy band gap values ranged from 0.22 to 2.27 eV. The best results of DSSC device efficiency, with TiO2+AgNO3/Dye/Plastisol structure, have resulted in the Voc of 0.694 V, current density (Jsc) of 0,943 mA/cm2and fill factor (FF) of 43,50% which is obtained at sample 1.
Co-Authors Ade Usra Berli Bajili, Abdil Dahyunir Dahlan Dwipanur P.U, Andhika Dwipanur, Andhika Elvy Rahmi Faizil, Nanda Husna, Isramil Marjoni Imamora Ali Umar Nini Firmawati R, Setia Erlila Ramli, Muhammad Adam Saad, Siti Khatijah Md Sri Maiyena