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Efrizon Umar
Badan Riset dan Inovasi Nasional (BRIN)
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SINTESIS DAN KARAKTERISASI NANOSELULOSA SERBUK DARI TANDAN KOSONG KELAPA SAWIT MENGGUNAKAN ULTRASONIFIKASI Tri Yuni Hendrawati; Efrizon Umar; Anwar Ilmar Ramadhan; Alvika Meta Sari; Mutiara Salsabila; Rahmawati Suryani; Firmansyah Firmansyah; Istianto Budhi Rahardja
Jurnal Teknologi Vol 15, No 1 (2023): Jurnal Teknologi
Publisher : Fakultas Teknik Universitas Muhammadiyah Jakarta

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24853/jurtek.15.1.159-166

Abstract

Indonesia is the largest palm oil producing country in the world. In the palm oil production process, solid waste is produced, one of which is empty palm fruit bunches (EFB) of 25-26% w/w of the total palm oil raw material. OPEFB has several constituent components such as lignin, hemicellulose and cellulose. The high content of α-cellulose in OPEFB can be used as a base material for making nanocellulose. Nanocellulose was made in this study through delignification, ultrasonication and hydrothermal processes with the aim of obtaining the optimum ultrasonication temperature of nanocellulose. Temperature variations were carried out at 40, 50, 60 and 70 °C for 30 minutes. The results of the synthesis process can be seen visually for each temperature variation. Characterization analysis was performed using SEM (Scanning Electron Microscopy). The correlation between temperature variations (x) to the yield percentage of nanocellulose (y) follows the equation y = 7.921x + 7.345 and R2 = 0.9471. The optimum temperature of the ultrasonication process is 70 °C with a yield of 36.9%. The size of nanocellulose powder is 174.85-460.84 nm with SEM at 70 °C.
SINTESA NANO ZIRKON DARI PASIR ZIRKON LOKAL DENGAN METODE FUSI KAUSTIK SODA-PRESIPITASI-KALSINASI Alvika Meta Sari; Efrizon Umar; Djoko Hadi Prajitno; Rian Fitriana; Anwar Ilmar Ramadhan; Firmansyah Firmansyah; Istianto Budhi Rahardja; Akmal Imam Faisal; Fikriyansyah Fikriyansyah
Jurnal Teknologi Vol 15, No 2 (2023): Jurnal Teknologi
Publisher : Fakultas Teknik Universitas Muhammadiyah Jakarta

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24853/jurtek.15.2.189-198

Abstract

Indonesia is one of countries that has the potential of mineral natural resources in the form of zircon sand. Zircon sand is a raw material that has the potential to be synthesized into nano zircon because of its ingredients of zircon oxide (ZrO2). In this study the aim was to study the aim to synthesize nano zircon from local zircon sand from Kalimantan using caustic soda-precipitation-calcination modification method. Nano zircon was prepared in this study by modifying existing methods, namely caustic fusion, washing, acid leaching using hydrochloric acid, precipitation using ammonia and calcination processes to produce nano zircon in the form of white powder. The efficiency of the process was analyzed by calculating the yield of the product formed, then the FTIR (Fourier Transform Infra-Red) spectroscopic test was performed to determine the functional groups of nano zircons and the morphology was analyzed using SEM (Scanning Electron Microscopy). Yield obtained is 2.7%  with the size of nano zircon is 41.983 nm. The FTIR spectrum shows the presence of the-Zr-O2 functional group at wave numbers 600 – 700 cm-1.
Co-Authors Akmal Imam Faisal Alvika Meta Sari Anwar Ilmar Ramadhan Djoko Hadi Prajitno Fikriyansyah Fikriyansyah Firmansyah Firmansyah Istianto Budhi Rahardja Mutiara Salsabila Rahmawati Suryani Rian Fitriana Tri Yuni Hendrawati