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Sintesis Nanokomposit -Fe2O3/SiO2 dengan Metode Salt-Assisted Spray Pyrolysis untuk Menurunkan Viskositas Minyak Berat Anrokhi, Mohamad Samsul; Nuryadin, Bebeh Wahid; Abdullah, Mikrajuddin; Khairurrijal, Khairurrijal; Iskandar, Ferry
Jurnal Matematika dan Sains Vol 22 No 1 (2017)
Publisher : Institut Teknologi Bandung

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Abstract

A α-Fe2O3/SiO2 nanocomposite as aquathermolisys catalyst material at heavy oil has been synthesized and optimized by using  Salt-Assisted Spray Pyrolysis method. The α-Fe2O3/SiO2 nanocomposite is obtained by thermal decomposition from the precursor.  The precursor is made of FeCl3, SiO2 and NaCl and water as a solvent. Concentration of FeCl3, SiO2, and NaCl are 1:1:5 in order. the composition of SiO2 in the composite is 0%, 25% and 50% of total mass, respectively. the droplets were transported to the furnace reactor using air as a carrier gas with a fixed flow rate at 5 liter/min and the furnace’s temperature is 800 °C in order to get the pyrolysis reaction. The resulted powder is then characterized by using XRD, SEM and Chatalytic aquathermolysis test. The result of XRD characterization shows that crystal peaks of α-Fe2O3 has been formed. SEM result shows nanocomposite morphology of α-Fe2O3/SiO2 with circle particle form with average particle diametre of α-Fe2O3, SiO2 25% and SiO2 50% of total mass are 765 nm, 850 nm, and 746 nm, respectively. Catalytic Aquathermolysis test showed catalyst α-Fe2O3/SiO2 50%  has catalytic properties better than catalytic properties of α-Fe2O3/SiO2 and α-Fe2O3/SiO2 25%.
Characteristics And Mineral Content of Lampung Tengah Ironsands Puspitarum, Deska Lismawenning; Safitri, Gita; Ardiyanti, Harlina; Anrokhi, Mohamad Samsul
Journal of Science and Applicative Technology Vol 2 No 1 (2019): ICoSITeR Special Edition
Publisher : Lembaga Penelitian, Pengabdian Masyarakat, dan Penjaminan Mutu (LPPM), Institut Teknologi Sumatera, Lampung Selatan, Lampung, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (269.224 KB) | DOI: 10.35472/281488

Abstract

Characteristics and Mineral Content of Lampung Tengah Ironsands. This study is carried out to investigate the characteristics and mineral content of ironsands from Bekri, Lampung Tengah Regency by using precipitation method. The research was conducted in Physics Laboratory of Institut Teknologi Sumatera from June to September 2018. Mineral content of sand is analayzed with X-Ray Diffractometer. The extraction was varied in temperature and stirring time. The temperature is varied in 80oC, 120oC, dan 160oC and yields different size; 33.76 nm, 11.84 nm and 11.14 nm. Meanwhile, the extraction is varied for 2 hours, 4 hours and 6 hours stirring and yields particle with 43.12 nm, 11.14 nm and 11.32 size. Mineral content of ironsands in Lampung Tengah are dominated by Ilmenite and Potassium Chloride.