Jurnal ILMU DASAR
Vol 17 No 1 (2016)

Synthesis of precipitated Calcium Carbonate (PCC) From Lime Rock Nature Methods Caustic Soda (Studies Concentration HNO3)

Noor Isnaini Azkiya (Jurusan Kimia, FMIPA, Universitas Brawijaya, Malang)
Fanny Prasetia (Jurusan Kimia, FMIPA, Universitas Brawijaya, Malang)
Elsa Desyta Putri (Jurusan Kimia, FMIPA, Universitas Brawijaya, Malang)
Anggita Rosiana (Jurusan Kimia, FMIPA, Universitas Brawijaya, Malang)
Sri Wardhani (Jurusan Kimia, FMIPA, Universitas Brawijaya, Malang)



Article Info

Publish Date
24 Jan 2017

Abstract

The limestones was abundant in Tuban, East Java and have high calcium mineral content. Nevertheless, in the economic value, limestone have low price. Aim the research is prepare  Precipitated Calcium Carbonate (PCC) by caustic soda method. In this method, calcium  was dissolved in HNO3 with different concentration (2, 4,6, 8 M). The Filtrate obtained then was added by Na2CO3 1 M to get PCC. As the results, The white PCC obtained with the highest rendement is 64,7% when added HNO3 6M. Analysis of functional group by FTIR show that there were strong absorption in the 844,76; 912,27 dan 1411,40 cm-1 that indicated carbonate group. Analysis of Cristallinity by XRD show that there were the peak characteristic of 2 on 29,50˚; 36,07˚ dan 39,50˚that representative calcite structure. SEM-EDX Analysis show that PCC have a mixing structure of calcite and vaterite.   Keywords: limestone, PCC, caustic soda 

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Journal Info

Abbrev

JID

Publisher

Subject

Biochemistry, Genetics & Molecular Biology Chemistry Mathematics Physics

Description

Jurnal ILMU DASAR (JID) adalah jurnal ilmiah yang melingkupi bidang matematika, fisika, kimia dan biologi. Naskah yang diusulkan untuk diterbitkan Jurnal Ilmu Dasar adalah naskah yang belum pernah diterbitkan dan atau tidak sedang dipertimbangkan penerbitannya di majalah lain. Jurnal Ilmu Dasar ...