Jurnal Kimia Terapan Indonesia
Vol 22, No 1 (2020)

Synthesis and Characterization of Gold Nanoparticles (AuNPs) by Utilizing Bioactive Compound of Imperata cylndrica L

Iwan Syahjoko Saputra (Academy of Analytical Chemistry Caraka Nusantara)
Siti Suhartati (Academy of Analytical Chemistry Caraka Nusantara)
Yoki Yulizar (Indonesia University (UI))
Sudirman Sudirman (The Center for Science and Technology Advanced Material, National Nuclear Energy Agency of Indonesia)



Article Info

Publish Date
31 Dec 2020

Abstract

Gold nanoparticles (AuNPs) have been successfully synthesized using bioactive compounds of Imperata cylindrica L leaf extract. In this study, precursors used HAuCl4 7x10-4 M, 8x10-4 M and 9x10-4 M. Concentration of Imperata cylindrica L used was 5%. The colloid of Gold nanoparticle (AuNPs) formed were characterized using Ultraviolet-visible Spectrophotometer (UV-Vis), Fourier Transform Infrared Spectroscopy (FTIR), Transmission Electron Microscopy (TEM), X-ray Diffraction (XRD). The formation of gold nanoparticles (AuNPs) at concentration 9x10-4 M showed the best results with a color change to red. UV-Vis showed an absorbance value of 1.4 and a wavelength of 530 nm. FTIR analysis showed the interaction of -OH functional group on phenolic compounds of Imperata cylindrica L leaf extract with Au3+ ions. There was a shift on the peak at wavenumber 3414 cm-1 to 3404 cm-1, indicating the formation of Au nanoparticles. TEM analysis showed the morphology of AuNPs is sphere-shaped with a particle size of 20 nm. XRD analysis showed a crystal size average of gold nanoparticles is 12 nm.

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