Indonesian Mining Journal
Vol 22, No 1 (2019): INDONESIAN MINING JOURNAL, Vol. 22 No. 1, April 2019

SYNTHESIS AND CHARACTERIZATION OF GAMMA ALUMINA AND ITS ADSORPTION CAPABILITY TEST FOR POMALAA MAGNESIUM LATERITE, SOUTHEAST SULAWESI

Titin Siti Fatimah (R&D Center for Mineral and Coal Technology Jalan Jenderal Sudirman 623 Bandung Phone. (+6222) 6030483. Fax. (+6222) 6003373 e-mail:tisif.tsf@gmail.com Department of Chemistry Faculty of Mathematics & Natural Science Padjadjaran University Jalan Raya )
Atiek Rostika Noviyanti (Department of Chemistry Faculty of Mathematics & Natural Science Padjadjaran University Jalan Raya Bandung Sumedang Km. 21 Phone/Fax. (+6222) 7794391)
Juliandri Juliandri (Department of Chemistry Faculty of Mathematics & Natural Science Padjadjaran University Jalan Raya Bandung Sumedang Km. 21 Phone/Fax. (+6222) 7794391)
Solihudin Solihudin (Department of Chemistry Faculty of Mathematics & Natural Science Padjadjaran University Jalan Raya Bandung Sumedang Km. 21 Phone/Fax. (+6222) 7794391)



Article Info

Publish Date
30 Apr 2019

Abstract

Based on variations in calcination temperature, gamma alumina has successfully been made using a simple sol-gel method for Pomalaa magnesium-laterite adsorption from the South East of Sulawesi. The laterite leached by sulfuric acid was then precipitated by ammonia, to make the magnesium was separated from its main impurities (Si, Fe and Al). Temperature variations at 500, 650, 800 and 950 °C in gamma alumina making formed the gamma alumina phase while the alpha alumina phase was formed at 1100 °C. The higher calcination temperature the lower the specific surface area respectively from 196.385, 156.239, 105.725, 96.134 and 15.396 (m2/g). This results in decreasing the magnesium of the laterite 9.04, 8.70, 8.09, 6.39 and 0.29 (mg/L) respectively. The 800 °C-calcination gamma alumina has the highest volume of the pore, namely 0.3265 mL/g and the radius of 61.76 Å. The gamma alumina isotherm curve is type IV. The SEM-EDS test shows an aggregation spherical shape. Gamma alumina was detected to adsorb Mg laterite. The X-ray mapping of SEM-EDS test shows even distribution between gamma alumina, magnesium and nickel. The highest adsorption is retained by GA-800/3 sample, namely 81.31 %.

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Journal Info

Abbrev

imj

Publisher

Subject

Chemical Engineering, Chemistry & Bioengineering Earth & Planetary Sciences Energy Engineering Environmental Science

Description

This Journal is published periodically two times annually : April and October, containing papers of research and development for mineral and coal, including exploration, exploitation, processing, utilization, environment, economics and policy. The editors only accept relevant papers with the ...