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Indonesian Journal of Pure and Applied Chemistry

IJoPAC
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Published by Universitas Tanjungpura

ISSN : 26208571 EISSN : 2620858X DOI : -

Core Subject : Science,

Biochemistry, Genetics & Molecular Biology Chemistry

Indonesian Journal of Pure and Applied Chemistry (IJoPAC) was first established in 2018 as a scientific journal that accommodates researchers and education practitioners to publish scientific work and research results which are the results of experiments or literature studies in the field of chemistry. Publications are carried out periodically with three issues (January-April, May-August, September-December) in one volume per year. Published scientific work can be in the form of original articles, short communications and review results covering the fields of Physical chemistry, Organic chemistry, Analytical chemistry, Inorganic chemistry, Biochemistry / Biological Chemistry, Applied Chemistry. Focus and Scope of Indonesian Journal of Pure and Applied Chemistry covering the fields : Physical chemistry Organic chemistry Analytical chemistry Inorganic chemistry Biochemistry/Biological Chemistry Applied Chemistry

Arjuna Subject : Kimia(semua kategori) - Kimia (Lain-Lain)

Articles 93 Documents

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ADSORPSI ASAM LEMAK BEBAS PADA CRUDE PALM OIL MENGGUNAKAN ZEOLIT TERAKTIVASI K2CO3 Nia Dahlia; Winda Rahmalia; Thamrin Usman
Indonesian Journal of Pure and Applied Chemistry Vol 2, No 3 (2019)
Publisher : Tanjungpura University

Research on the use of K2CO3-activated zeolite as an adsorbent for free fatty acid (FFA) adsorption on crude palm oil (CPO) has been done. CPO is one of the mainstay products of Indonesian plantations which are used as raw material for cooking oil. The aim of this study to determine the adsorption capacity of activated zeolites against free fatty acid of CPO. The results showed that the iodium uptake capacity of zeolites before activation was 495.6%, activated zeolites were 527.1% and impregnated zeolites were 642.6%. The number of zeolites with the best absorption was 2 grams and ALB was absorbed 4.079% for activated zeolites (ZAA), 4.98% for impregnated zeolites (ZAI), and the water content and impurities were still below SNI standards. The CPO adsorption process with zeolites shows the Langmuir model with a correlation value (R2) of 0.9999 for ZAA and (R2) of 0.9976 for ZAI. The results showed that activated zeolites had lower absorption than impregnated zeolites.

PENGARUH VARIASI KOMPOSISI SELULOSA JERAMI PADI DAN LIMBAH BOTOL PLASTIK POLIETILEN TEREFTALAT (PET) TERHADAP KARAKTERISTIK BIODEGRADABLE PLASTIC Hanna Sjafarina; Intan Syahbanu; Nurlina Nurlina
Indonesian Journal of Pure and Applied Chemistry Vol 3, No 3 (2020)
Publisher : Tanjungpura University

Research on the effect of variations in the composition of rice straw cellulose on the characteristics of biodegradable PET-Cellulose plastic. The purpose of this study is to explain the effect of the composition of rice straw cellulose and PET on the characteristics of biodegradable plastic made from composite of rice straw cellulose and PET. This research was conducted in several stages, the isolation of cellulose from rice straw, recycling PET from mineral water bottle, mixing cellulose and PET, then testing the characteristics, the DTA-TGA thermal characteristic test, and degradation test with the soil burial test method. . In the thermal characteristics test there was a decrease in weight in samples with composition PET: cellulose 90:10; 60:40; and 50:50 each with 0.719; 0.710; 0.581 mg in the temperature range 38.30-68.32 ° C, 40.72-68.17 ° C, 41.45-80.40 ° C, while in the samples 80:20 and 70:30 there was no decrease in weight the temperature. In the sample 90:10; 80:20; 70:30; 60:40 and 50; 50 there is a decrease in weight each of 4,045; 3,909; 3,464; 2,760 and 3,205 mg at temperatures 328, 16-430.65 ° C, 362.05-442.15 ° C, 349.96-439.82 ° C, 388.29-446.70 ° C, and 325.39-420.79 ° C. The degradation test using soil burial test method obtained percent weight loss in samples with PET composition: 70:30 cellulose which was 38.24%.

PENGARUH JENIS MINYAK TERHADAP SIFAT FISIK D AN KIMIA BATH BOMB (THE EFFECT OF THE TYPE OIL ON THE PHYSICAL AND CHEMICAL PROPERTIES OF BATH BOMB) Annisa Bella Maharani; Lia Destiarti; Nurlina Nurlina; Intan Syahbanu; Winda Rahmalia
Indonesian Journal of Pure and Applied Chemistry Vol 3, No 1 (2020)
Publisher : Tanjungpura University

Bath bombs were produced with ten different types of oil to determine the effect of the oil used on their physical and chemical properties. Bath bombs were prepared by mixing the dry ingredients first (citron, cornstarch, baking soda) and stirring until all the ingredients were well blended. Then, mixed the wet ingredients (water, oil, perfume ore, food coloring) into the beaker. After that, the wet ingredients were poured gradually into the dry dough, and this step was done until all the wet ingredients run out, and the texture of the bath bomb dough was slightly moist so that it can be put in the mold. Finally, the bath bomb is printed and tested in a laboratory. The result showed that the difference in essential oils used in the manufacture of bath bombs does not affect the pH of the bath bomb but affects the stability of the resulting foam. The acceptability test results showed that the resulting bath bomb provided a sensation of freshness and relaxation and did not cause allergies. Based on the SWOT analysis results, these bath bombs can advance and develop by implementing a vertical integration strategy

SINTESIS DAN STUDI STABILITAS NANOPARTIKEL PERAK TERTUDUNG ASAM SALISILAT Rizky Noviani Ridwan; Gusrizal Gusrizal; Nurlina Nurlina; Sri Juari Santosa
Indonesian Journal of Pure and Applied Chemistry Vol 1, No 3 (2018)
Publisher : Tanjungpura University

Silver nanoparticles capped with salicylic acid have been synthesized by reduction of silver nitrate with salicylic acid without additional capping agent. In the formation of silver nanoparticles, the solution of silver nitrate was first mixed with the pH 11 salicylic acid solutions at a mole ratio of 1:40. The mixture was heated for 45 minutes in a boiling water bath. The formation of silver nanoparticles was indicated by the appearance of yellow color and monitored using UV-Vis spectrophotometer. The maximum peak of resulted silver nanoparticles appeared in the range of 410-420 nm with the average size of particles was 66±28 nm. Stability test over a period of 16 weeks showed that silver nanoparticles capped with salicylic acid were stable. The results of stability test show that salicylic acid simultaneously act as reducing as well as capping agent in the formation of silver nanoparticles.

ENKAPSULASI FRAKSI N-HEKSAN DAUN KESUM (Polygonum Minus Huds) TERSALUT Carboxymethylcellulose (CMC) DAN PATI DAN UJI AKTIVITAS ANTIOKSIDAN DENGAN TEKNIK FREEZE DRYING Fitriani Fitriani; Muhammad Agus Wibowo; Andi Hairil Alimuddin
Indonesian Journal of Pure and Applied Chemistry Vol 2, No 1 (2019)
Publisher : Tanjungpura University

Kesum have a scientific name Polygonum Minus Huds is one of the endemic plants originating from West Borneo. Extracts of kesum leaf is easily damaged and the compounds contained therei are volatile. Therefore it is necessary to take measures to protect the extracts of kesum leaf. One effort that can be made to im exprove the stability of the compounds in the extract is by the process of encapsulation. This process needs to be done so that the leaf extract can last longer so it can be used for various purposes. Encapsulation aims to protect sensitive material components and reduce the degradation of the active compounds in the material. This study aims to determine the effect of mass of core materials on the efficiency of encapsulation and antioxidant activity and the effect of temperature on encapsulation. The results showed that the encapsulated with the mass of core material 10% gave the highest efficiency of 89.7%. The mass of the core material affects the encapsulation efficiency, the less the core material will provide a high value of encapsulation efficiency. Enkapsulates containing n-heksan fractions of 444.53 ppm have a lower value IC50, thus having better antioxidant activity properties. The stability of the encapsulated antioxidant activity performed at room temperature 25◦C at 10% n-hexane fraction yielded 88.36% ihibisi on day 1, 80.90% on day 3, 79.67% on day 6 and 78.04% on day 9. Activity the antioxidant encapsulant on the first day at room temperature 25◦C is better than the third, sixth and ninth days. SEM leaf extract analysis results have uneven spherical particles, no visible fracture or pore holes as large as encapsulation have round particles that are almost as large.

SINTESIS DAN AKTIVITAS ANTIKANKER SENYAWA C-4-ALILOKSI-3-METOKSIFENILKALIKS[4]RESORSINARENA Endah Sayekti; Jumina Jumina; Dwi Siswanta; Mustofa Mustofa
Indonesian Journal of Pure and Applied Chemistry Vol 3, No 1 (2020)
Publisher : Tanjungpura University

The aims of this study was to synthesize of C-4-alyloxy-3-methoxyphenylcalix[4]resorcinarene (3). The syntheses was conducted by condensation reaction of resorcinol with 4-allyloxy-3-methoxybenzaldehyde (2) in ethanol with hydrochloric acid as a catalyst. The (2) compound was synthesized by the reaction of the 4-hydroxy-3-methoxybenzaldehyde (vanillin) (1) via allylation reaction using an allylbromide with the sodium metal as a catalyst in ethanol. A (3) compound was orange solid. m.p. of 176–177 °C (dec.). Yield (78%). FTIR (KBr, ν; cm-1): 3441 (-OH); 3086 and 3008 (Csp2-H); 2939 (Csp3-H ); 1612 (C=C aliphatic); 1512 (C=C aromatic); 1427 (>CH- methine); 1234, 1211, 1080 and 1018 (C-O-C asymmetric); 925 (C=CH2 terminal). 1H-NMR (DMSO-d6; 500 MHz) δ (ppm): 8,50 (8H, s, OH); 6.43 (4H, s, ArC-H); 6,36-6,38 (4H, d, J=10 Hz); 6.32 (4H, s, ArC-H); 6.26-6.28 (4H, d, J=10 Hz); 6.13 (4H, s, ArC-H); 6.00-6.05 (4H, m, =C-H); 5.38-5.40 (4H, d, J=10 Hz); 5.31 (4H, s, >C-H methine); 5.16-5.18 (4H, d, J=10 Hz); 4.34-4.36 (8H, d, J=10 Hz); 3.29 (12H, s, -OCH3). 13C-NMR (DMSO-d6; 500 MHz) dC (ppm): 33 (4 x CH methine); 55 (4 x CH3); 69 (4 x CH2-); 101 (4 x ArC-H); 112 (4 x ArC-H); 113 (4 x ArC-H); 116 (4 x =CH allyl terminal); 120 (4 x ArC-H); 122 (8x ArC-); 132 (4 x ArC-H); 134 (4 x =CH allyl); 137 (4 x ArC-); 145 (4 x ArC-O); 148 (4 x ArC-O); 152 (8 x ArC-OH). MS (ESI) m/z: 1137.5 (M+). Anticancer evaluation was performed on (3) compound by MTT (3-(4,5-dimethyltiazole-2-yl)-2,5-diphenyltetrazolium bromide) method showed that (3) compound has a cytotoxic activity against HeLa and T47D cells which IC50 value respectively are 13,58 and 65,26 µg/mL.

DETEKSI KEBERADAAN BAKTERI RESISTEN LOGAM MERKURI (Hg) PADA PENAMBANGAN EMAS TANPA IZIN (PETI) DI SIMPI, SEKADAU, KALIMANTAN BARAT Abdullah Abdullah
Indonesian Journal of Pure and Applied Chemistry Vol 1, No 2 (2018)
Publisher : Tanjungpura University

The purpose of this research is to know the existence of mercury metal degradation bacteria in the activity of illegal gold mining (PETI) in Simpi Village, Belitang Hilir sub-district, Sekadau District, West Kalimantan. The samples were taken from one location with three different sampling points. Isolation of bacteria by pour plate method in NA-HgCl medium. Detection of bacteria by paper disc method based on inhibit zone resistant of Mueller-Hinton Agar (MHA) with mercury levels such as 10 mg/L, 20 mg/L and 30 mg/L . The results showed that it was found that one pure isolate (PP) showed the most resistant isolate to the mercury stress of 10 mg/L can be detected

UJI KELARUTAN LOGAM DARI TAILING TIMAH MENGGUNAKAN PELARUT EUTEKTIK BERBASIS KOLIN KLORIDA DAN ASAM p-TOLUENASULFONAT Nimas Ade Kusdayanti; Winda Rahmalia; Thamrin Usman
Indonesian Journal of Pure and Applied Chemistry Vol 2, No 2 (2019)
Publisher : Tanjungpura University

Deep eutectic solvents (DES) are defined as combinations of two or three components which are able to establish hydrogen bond interactions with each other to form an eutectic mixture, that have a melting point lower than that of the each individual component. This study aims to determine the characteristics of DES based on choline chloride (ChCl) as quaternary ammonium salts and p-toluenasulfonic acid (PTSA) as hydrogen bond donors and to investigate their selectivity for dissolving metals in tin tailings. Synthesis of DES was carried out by mixing ChCl and PTSA with variations of the mole fraction, then stirring at 80 oC for 15 minutes. Resulted products were characterized their freezing point, density, viscosity, conductivity and functional groups. Mixture with a mole fraction of ChCl 0.6 formed homogeny clear liquid. It has a freezing point of 8 oC, density of 1.207 g/mL, viscosity of 4.663 cP, and conductivity of 182.4 mS/cm. Based on fourier transform infrared (FTIR) analysis, the interaction between ChCl and PTSA was due to the formation of hydrogen bonds between the O atoms of PTSA and the H atoms of ChCl. Inductively coupled plasma atomic emission spectroscopy (ICP-AES) analysis showed the presence of 1962 ppm of Fe metal dissolved in DES. This value was significant greater than the presence of other metals in the DES.

KOMPOSISI UNSUR DAN KARAKTERISTIK MINERAL PASIR PUYA DARI SINTANG, KALIMANTAN BARAT (ELEMENT COMPOSITION AND MINERAL CHARACTERISTIC OF PUYA SAND FROM SINTANG, WEST KALIMANTAN) Duwan Agustina; Risa Nofiani; Imelda H Silalahi
Indonesian Journal of Pure and Applied Chemistry Vol 4, No 1 (2021)
Publisher : Tanjungpura University

Puya sand is a byproduct from local gold mining activities found in Sintang, West Kalimantan. Puya sand is usually left by the miners after the mining activity leaving a pile of abandoned sands. Mineral characterisation conducted by using XRD and XRF methods demonstrated that the sand contains valuable elements and mineral, i.e. zircon silicate, quartz and ilmenite. A simple physical flotation separation method removed quartz remaining material containing concentrated zircon silicate. XRD analysis by using Search-Match followed by amount calculation by using Rietveld refinement showed that the sand consists of zircon silicate (58.3%), ilmenite (35.2%) and anatase (6.5%). Elemental analysis by using XRF presented the percentage of Zr, Ti, Fe and Si is 41.0, 23.9, 13.06 and 8.3, respectively. Hafnium with 1.5% was also observed along with Th, U and rare earth elements (REEs), such as Nd, Y, Eu, and Yb.

PENINGKATAN KUALITAS MINYAK JELANTA MENGGUNAKAN KARBON AKTIF DAN EKSTRAK PUCUK IDAT (Cratoxylum glaucum) Robby Gus Mahardika; Sito Enggiwanto; Ary Samsiar
Indonesian Journal of Pure and Applied Chemistry Vol 1, No 1 (2018)
Publisher : Tanjungpura University

Silica Waste cooking oil can be used as a soap or biodiesel. Good soaps or biodiesel should be from oils that have low levels of fatty acids and free radicals. However, waste cooking oil has high free fatty acid and free radical, it is necessary to increase the quality of waste cooking oil. One effort to improve the quality of waste cooking oil can use activated carbon as an adsorbent. Decrease in free radicals in cooking oil can use antioxidants from extract pucuk idat (Cratoxylum glaucum). This study aims to see the effect of extract pucuk idat on the process of improving the quality of waste cooking oil. The process of improvement by adding activated carbon and varying the concentration of ethanol extract pucuk idat. Activated carbon used 10% with variation of extract 0,25%; 0,5% and 0,75%. This process followed by stirring for 15 minutes at 80°C, then soaked for 3 days. Oil quality are identified by the method of determining the levels of free fatty acids and acid numbers. The results of this study indicate that extract pucuk idat in ethanol with 0,75% concentration has the lowest free fatty acid and acid number. Extract pucuk idat can improve the quality of waste cooking oil.

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Editorial Address Department of Chemistry, Faculty of Mathematics and Natural Sciences, Tanjungpura University Jl. Prof. Dr. Hadari Nawawi, Pontianak, Kalimantan Barat, Indonesia

Location Kota pontianak, Kalimantan barat INDONESIA

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Ajuk Sapar

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ajuk.sapar@chemistry.untan.ac.id

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+6281282990575

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anthoni.b.aritonang@chemistry.untan.ac.id

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Department of Chemistry, Faculty of Mathematics and Natural Sciences, Tanjungpura University Jl. Prof. Dr. Hadari Nawawi, Pontianak, Kalimantan Barat, Indonesia

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