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All Journal Sainmatika: Jurnal Ilmiah Matematika dan Ilmu Pengetahuan Alam Jurnal Kumparan Fisika Jurnal Mitrawarga
Parmin Lumban Toruan
Jurusan Fisika, Fakultas Sains Dan Teknologi, Universitas PGRI Palembang
Agriculture, Biological Sciences & Forestry Humanities Chemistry Education Environmental Science Law, Crime, Criminology & Criminal Justice Mathematics Physics Social Sciences

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Journal : Sainmatika: Jurnal Ilmiah Matematika dan Ilmu Pengetahuan Alam

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SIFAT OPTIK DAN PERMITIVITAS LISTRIK MEMBRAN POLIMER PADAT KITOSAN/PEO Kartika Sari; Sunardi Sunardi; Agung Bambang Setio Utomo; Parmin Lumban Toruan; Evi Yulianti; Mashadi Mashadi
Sainmatika: Jurnal Ilmiah Matematika dan Ilmu Pengetahuan Alam Vol. 17 No. 2 (2020): Sainmatika : Jurnal Ilmiah Matematika dan Ilmu Pengetahuan Alam
Publisher : Universitas PGRI Palembang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31851/sainmatika.v17i2.4987

Abstract

Synthesis and characterization of the chitosan/PEO solid polymer membranes were carried out to determine the morphological structure, crystal structure and functional groups. Synthesis of the chitosan/PEO solid polymer membrane was carried out by solution casting method. Characterization was performed using the FTIR (Fourier Transform Infra Red), XRD (X-ray Diffraction), SEM (Scanning Electron Microscopy) and EIS (Electrochemical Impedance Spectroscopy). The FTIR results showed that the chitosan/PEO solid polymer membrane interacted with the –OH and C-H functional groups at wave numbers 1500 - 945 cm-1 and formed a bending bond between functional groups  of the C-C and –NH3. The SEM results showed that the homogeneous agglomeration was formed on the membrane surface due to the addition of PEO powder. This causes the formation of bonds between atoms to unstable. The XRD results obtained that the chitosan/PEO solid polymer membrane pattern tended to have a semicrystalline structure. The graph of the EIS results shows the electric permittivity does not form a semicircular arc. There was no grain response on the chitosan / PEO solid polymer membrane. The results of SEM, XRD, FTIR and EIS characterization show that chitosan /PEO solid polymer membranes can be used as an alternative to solid polymer electrolytes.
Kajian Hasil Pengujian X-Ray Diffraction (XRD) Dan Konstanta Dielektrik Membran Polimer Kitosan/PEG4000 dengan Lithium Triflat (LiCF3SO3) Kartika - Sari; Agung Bambang Setio Utomo; Parmin Lumban Toruan; Ampala Khoryanton
Sainmatika: Jurnal Ilmiah Matematika dan Ilmu Pengetahuan Alam Vol. 18 No. 2 (2021): Sainmatika : Jurnal Ilmiah Matematika dan Ilmu Pengetahuan Alam
Publisher : Universitas PGRI Palembang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31851/sainmatika.v18i2.6717

Abstract

Synthesis and testing of chitosan/PEG4000 solid electrolyte polymer membrane with LiCF3SO3 salt as a surfactant was carried out to determine crystalline size and type of structure using X-Ray Diffraction (XRD) and dielectric constant using Electrochemical Impedance Spectroscopy (EIS). The manufacture of chitosan/PEG4000 electrolyte polymer membrane with LiCF3SO3 salt using the solution casting method. The samples used in the XRD and EIS tests were in the form of solid electrolyte polymer membranes of chitosan, chitosan/PEG4000 and chitosan/PEG4000 with LiCF3SO3 salt. XRD test showed that the crystalline size of the chitosan, chitosan/PEG4000, and chitosan/PEG4000 electrolyte polymer membranes with LiCF3SO3 salt experienced a 2θ angle shift and formed a semicrystalline phase. The peak intensity increase occurred after chitosan was added with PEG4000 with LiCF3SO3 salt. The crystalline size obtained for the electrolyte polymer membrane of chitosan, chitosan/PEG4000 and chitosan/PEG4000 salt LiCF3SO3 was 4,002 nm; 2,474 nm and 4,183 nm. Meanwhile, the type of structure produced by chitosan, chitosan/PEG4000 and chitosan/PEG4000 electrolyte polymer membranes with LiCF3SO3 salt is a semicrystalline phase. The dielectric constant for solid electrolyte polymer membranes of chitosan/PEG4000, and chitosan/PEG4000 with LiCF3SO3 salt are 3,4 and 16,6 x 103. XRD and EIS test results show that chitosan/PEG4000 polymer membrane with LiCF3SO3 salt as a surfactant can be applied as an alternative to solid electrolyte polymer secondary batteries.
Co-Authors Agung Bambang Setio Utomo Agung Bambang Setio Utomo Ampala Khoryanton Asiah Jumarni Atina, Atina Bella Margareta Evi Yulianti Kartika Sari Mashadi Mashadi Sihombing, Sagita Charolina Sunardi Sunardi Syahnas Ski Pratiwi