Jurnal Sains Materi Indonesia
Vol 19, No 2: JANUARI 2018

EFFECT OF CONCENTRATION OF IMPERATA CYLINDRICA L LEAF EXTRACT ON SYNTHESIS PROCESS OF GOLD NANOPARTICLES

Iwan Syahjoko Saputra (Akademi Kimia Analisis Caraka Nusantara)
Yoki Yulizar (Departemen Kimia, FMIPA Universitas Indonesia)
Sudirman Sudirman (Pusat Sains dan Teknologi Bahan Maju-BATAN)



Article Info

Publish Date
31 Jan 2018

Abstract

Gold Nanoparticles (GoldNPs) successful was performed using HAuCl4 precursor as Au3+ ion source with 7x10-4 M concentration. The research aims to knows effect of concentration variation of Imperata cylindrica L leaf extract on synthesis process of gold nanoparticles. The research used of green synthesis method. Colloid of nanoparticles which is formed in analyzed using UV-Vis Spectrophotometer, FT-IR Spectroscopy, PSA, PZC, XRD and TEM. The results of synthesis showed the best concentration of Imperata cilindrica L leaf extract at 3,46%, happen a shift of wavelength at UV-Vis from 216 nm to 530 nm with 1.779 absorbance value. The PSA analysis showed a particle size of 51.87 nm and a PZC value of -19.2 mV. The result of FT-IR indicated a shift of wavenumber in the hidroxyl group from 3354 cm-1 to 3390 cm-1 and showed a interaction of hydroxyl group at imperata cylindrica L leaf extract with Au3+ ion. TEM analysis shows the morphology of GoldNPs that spherical shape with a particle size of 20 nm. XRD calculation results show crystallite size of gold nanoparticles is 15.47 nm.

Copyrights © 2018






Journal Info

Abbrev

jsmi

Publisher

Subject

Materials Science & Nanotechnology

Description

Jurnal Sains Materi Indonesia (Indonesian Journal of Materials Science), diterbitkan oleh Pusat Teknologi Bahan Industri Nuklir - BATAN. Terbit pertama kali: Oktober 1999, frekuensi terbit: empat ...