The Journal of Pure and Applied Chemistry Research
Vol 10, No 1 (2021): Edition January-April 2021

The Effect of Temperature Synthesis on the Plate-Like Particle of Bi4Ti3O12 Obtained by Single Molten NaCl Salt

Sheley Marela (Department of Chemistry, Faculty Science and Technology, Universitas Islam Negeri Maulana Malik Ibrahim Malang)
Nur Aini (Department of Chemistry, Faculty Science and Technology, Universitas Islam Negeri Maulana Malik Ibrahim Malang)
Arie Hardian (Department of Chemistry, Universitas Jenderal Ahmad Yani, Cimahi, Indonesia)
Veinardi Suendo (Division of Inorganic and Physical Chemistry, Faculty Mathematics and Natural Sciences, Institut Teknologi Bandung, Jl. Ganesha 10, Bandung 40132, Indonesia Research Center for Nanosciences and Nanotechnology, Institut Teknologi Bandung, Jl. Ganesha )
Anton Prasetyo (Department of Chemistry, Faculty Science and Technology, Universitas Islam Negeri Maulana Malik Ibrahim Malang)

Article Info

Publish Date
08 Apr 2021

Abstract

Three-layer Aurivillius compound bismuth titanate (Bi4Ti3O12) is well known for having interesting properties such as ferroelectric and photocatalyst. Many researchers reported that the unique plate-like shaped particle affecting ferroelectric and photocatalyst properties. The molten salt synthesis is the common simple method to obtain that unique morphology. In this research, Bi4Ti3O12 was synthesized using single molten salt NaCl at various temperatures, which is 800, 850, 900, and 950 oC. X-Ray Diffraction data showed that all obtained Bi4Ti3O12 have a B2cb space group with no impurities detected. The Raman spectra shows the characteristic vibration modes of Bi4Ti3O12 at 62, 117, 228, 269, 332, 364, 536, 851 cm-1. The plate-like shaped particle was confirmed by SEM analysis. Based on SEM images, the size of the particle increased along with the synthesis temperature, which is due to the thermal effect on grain growth.

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Journal Info
The Journal of Pure and Applied Chemistry Research
Website

Abbrev

jpacr

Publisher

Universitas Brawijaya

Subject

Chemical Engineering, Chemistry & Bioengineering Chemistry Materials Science & Nanotechnology Medicine & Pharmacology

Description

The Journal of Pure and Applied Chemistry Research focuses in publishing research articles in the field of Chemistry and Applied Chemistry. The target is in exploring, investigating, and developing chemicals sources from local and/or Indonesian to increase the value. Scope of the journal is organic ...