Rekayasa Mesin
Vol 11, No 3 (2020)

Produksi Biodiesel dari Dedak Padi dengan Metode In-Situ Dua Tahap Menggunakan Katalis Asam Sulfat dan CaO/Hydrotalcite

Mirzayanti, Yustia Wulandari (Unknown)
Alisa, Ayu (Unknown)
Sari, Devita (Unknown)



Article Info

Publish Date
31 Dec 2020

Abstract

In this study, biodiesel is made from rice bran vegetable oil. Biodiesel production was carried out by the in-situ method using two-sides using sulfuric acid catalysts and CaO/hydrotalcite. The solvent used was methanol as an oil component in the material and a reactant in the formation of FAME and n-hexane as a solvent to increase the yield of rice bran oil extraction. CaO/hydrotalcite to the yield of biodiesel produced and composition of biodiesel at the highest yield. As much as 50 grams of rice bran was put into a three-neck flask, then 50 ml of n-hexane were added. Next, 1 ml mixture of a sulfuric acid catalyst and 250 ml of methanol were added. Then, the mixture was reacted at 65º. Add stirring to 600 rpm for 90 minutes. Reheating after 90 minutes and a sample of 2.5 grams was taken for FFA testing. Next, the CaO/hydrotalcite catalyst in 10 ml of methanol with a mass variation of 1; 1,5; and 2 grams are added to the reaction flask. The mixture was reacted again at a temperature of 65 ºSuitably stirrings 600 rpm for 90 minutes. Based on the BET test results, the CaO/hydrotalcite catalyst surface area was 200.13 m2/g. The best results obtained on CaO/hydrotalcite catalysts were 2 grams with a biodiesel yield of 9.56%. In the highest biodiesel yield, the FAME component is preferred over the oleic acid methyl ester composition with an area of 35.09% at a retention time of 19.14 min.

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Journal Info

Abbrev

rm

Publisher

Subject

Mechanical Engineering

Description

Rekayasa Mesin is published by Mechanical Engineering Department, Faculty of Engineering, Brawijaya, Malang-East Java-Indonesia. Rekayasa Mesin is an open-access peer reviewed journal that mediates the dissemination of academicians, researchers, and practitioners in mechanical engineering. Rekayasa ...