Jurnal Teknologi Industri Pertanian
Vol. 34 No. 2 (2024): Jurnal Teknologi Industri Pertanian

SYNTHESIS OF RESIDUAL OIL FROM SPENT BLEACHING EARTH (SBE) INTO BIODIESEL USING MICROWAVE REACTOR

Haryo Tejo Prakoso (Indonesian Oil Palm Research Institute, Jl. Taman Kencana 1, Bogor 16128, Indonesia)
Azzahra Salsabila Syifa Mawardanti (Chemical Engineering Department, Faculty of Engineering, Universitas Brawijaya, Malang, Jawa Timur 65145, Indonesia)
Azizatul Maftuhah (Chemical Engineering Department, Faculty of Engineering, Universitas Brawijaya, Malang, Jawa Timur 65145, Indonesia)
Firda Dimawarnita (Indonesian Oil Palm Research Institute, Jl. Taman Kencana 1, Bogor 16128, Indonesia)
Yora Faramitha (Indonesian Oil Palm Research Institute, Jl. Taman Kencana 1, Bogor 16128, Indonesia E-mail: haryotejoprakoso@gmail.com)
Bambang Poerwadi (Chemical Engineering Department, Faculty of Engineering, Universitas Brawijaya, Malang, Jawa Timur 65145, Indonesia)



Article Info

Publish Date
02 Sep 2024

Abstract

Spent bleaching earth (SBE) is a waste from the crude palm oil CPO refining process which contains high oil content, around 20-30%. There are several methods to reduce SBE oil content, one of which is the solvent extraction method. SBE residual oil can be utilized as a raw material for biodiesel. This research aims to determine the mass ratio of SBE and solvent, the optimal temperature for extracting residual oil from SBE, and the potential of residual oil from SBE to be used as biodiesel using a microwave reactor. Residual oil extraction was carried out at varying mass ratios of SBE and solvent (1:2, 1:4, and 1:6) and varying temperatures (26, 40, and 50°C). The treated residual oil was esterified and subjected to transesterification reaction with 15% methanol and 1% KOH for 10 minutes at 60°C using a microwave reactor. The optimal extraction result for residual oil was at a 1:4 ratio and 26°C with a yield of 19.12%. There is also an increase in surface area in deoiled-SBE. The conversion of residual oil from SBE into biodiesel yielded 33.53% with a conversion value of 45.28% and a FAME content of 92.97%. The characteristics of the produced biodiesel meet the Indonesian National Standard (SNI) for biodiesel with density of 0.8674 g/cm3 and viscosity of 5.69 mm2/s. Keywords: extraction, fatty acid, transesterification, yield

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Journal Info

Abbrev

jurnaltin

Publisher

Subject

Agriculture, Biological Sciences & Forestry Engineering Industrial & Manufacturing Engineering

Description

The development of science and technology in agriculture, has been instrumental in increasing the production of various agricultural commodities. But climate change is also uncertain world led to decreased agricultural productivity. World energy crisis resulted in higher prices of agricultural ...