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Anneza Astriet
Chemistry Department, FMIPA Universitas Syiah Kuala Darussalam- 23111,Banda Aceh Indonesia
Agriculture, Biological Sciences & Forestry Astronomy Biochemistry, Genetics & Molecular Biology Chemistry Earth & Planetary Sciences Energy Immunology & microbiology Neuroscience Physics

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PREPARATION OF INORGANIC CATALYST BASED HEMATITE (a-Fe2O3) COMPOUND EXTRACTED FROM ACEH IRON ORE MINERAL AND ITS CATALYTIC ACTIVITY ON TRANSESTERIFICATION OF COCONUT OIL Muliadi Ramli; Anneza Astriet; T. Banta Darmawan; Saiful Saiful; Susilawati Susilawati; Nasrullah Idris
Jurnal Natural Volume 19, Number 1, February 2019
Publisher : Universitas Syiah Kuala

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (289.745 KB) | DOI: 10.24815/jn.v19i1.12855

Abstract

Hematite (Fe2O3) was successfully extracted from the Aceh iron ore mineral by precipitation method with employing sulphuricacid (H2SO4) as chemical agent.  Furthermore, the extracted hematite was modified with sodium metal (K), namely it doped with NaOH of 5% and 10% (w/w), respectively. Based on the characterization results using XRD and SEM- EDS proved that modified catalyst (Na2O/Fe2O3) with their homogeneous size were resulted while the hematite (Fe2O3) particles was dopped withNaOH at its low concentration of (5% wt/wt), however while doping with the higher concentration of NaOH (10% w/w), agglomeration was taken place among the catalyst particles in which decreasing the surface area of the modified catalysts. Finally, the modified catalyst (Na2O/Fe2O3) was successfully applied as an inorganic catalyst on transesterification of coconut oil and methanol (T = 55 – 60oC, 2 h)for forming methyl esters asbiodiesel compounds. 
PREPARATION OF INORGANIC CATALYST BASED HEMATITE (a-Fe2O3) COMPOUND EXTRACTED FROM ACEH IRON ORE MINERAL AND ITS CATALYTIC ACTIVITY ON TRANSESTERIFICATION OF COCONUT OIL Muliadi Ramli; Anneza Astriet; T. Banta Darmawan; Saiful Saiful; Susilawati Susilawati; Nasrullah Idris
Jurnal Natural Volume 19, Number 1, February 2019
Publisher : Universitas Syiah Kuala

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24815/jn.v19i1.12855

Abstract

Hematite (Fe2O3) was successfully extracted from the Aceh iron ore mineral by precipitation method with employing sulphuricacid (H2SO4) as chemical agent.  Furthermore, the extracted hematite was modified with sodium metal (K), namely it doped with NaOH of 5% and 10% (w/w), respectively. Based on the characterization results using XRD and SEM- EDS proved that modified catalyst (Na2O/Fe2O3) with their homogeneous size were resulted while the hematite (Fe2O3) particles was dopped withNaOH at its low concentration of (5% wt/wt), however while doping with the higher concentration of NaOH (10% w/w), agglomeration was taken place among the catalyst particles in which decreasing the surface area of the modified catalysts. Finally, the modified catalyst (Na2O/Fe2O3) was successfully applied as an inorganic catalyst on transesterification of coconut oil and methanol (T = 55 – 60oC, 2 h)for forming methyl esters asbiodiesel compounds. 
Co-Authors Muliadi Ramli Nasrullah Idris Saiful Saiful Susilawati Susilawati T. Banta Darmawan