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Irdoni HS
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Pengaruh Komposisi Katalis H-Zeolit Dan Kecepatan Pengadukan Pada Sintesa Plastisizer Butil Oleat Rinanda, Wahyu Okta; HS, Irdoni; Nirwana, Nirwana
Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains Vol 2, No 2 (2015): Wisuda Oktober Tahun 2015
Publisher : Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains

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Abstract

Oil palm commodity has a strategic role in the national economy. In the development of the palm oil industry, the necessary diversification of oil palm products needed by using the esterification reaction. One of the products of the oil palm which on development now is a fatty acid alkyl esters. Products that include the type of fatty acid alkyl ester is plasticizer. In this study, the plasticizer is synthesized by esterification of oleic acid and butanol, using activated natural zeolite catalysts. This research aims to study the influence of H-Zeolite catalyst composition and stirring speed on synthesis plasticizer butyl oleate, and determining the characteristics of the plasticizer butyl oleate which generated through analysis of test products. The process is using the variation of H-Zeolite catalyst composition (12.5%, 15%, 17.5%) based on oleic acid and stirring speed (175 rpm, 200 rpm, 225 rpm), with a fixed variable, the reaction temperature of 1100 C, the process time is 6 hours and the reaction molar ratio of 1: 9. From the analysis of the results showed that the esterification of H-Zeolite catalyst composition and stirring speed affects the conversion of the resulting products. The best operating conditions obtained in this study is the H-Zeolite catalyst composition of 17.5% and a stirring speed of 200 rpm which produces a reaction conversion of 74.50%. Characteristics plasticizer generated in this study is consistent with the characteristics of commercial plasticizers which Viscosity (200 C) 8.62 to 9.07 mPa.s and Specific Gravity (200 C) from 0.886 to 0.901.Keywords: Butyl Oleate, Esterification, H-Zeolite and Plasticizer
Pengaruh Rasio Molar Dan Komposisi Katalis H-Zeolit Pada Pembuatan Plastisizer Dari Minyak Limbah Ikan Patin dengan Butanadiol Sari, Novita Aprilia Maya; HS, Irdoni; Nirwana, Nirwana
Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains Vol 2, No 1 (2015): Wisuda Februari Tahun 2015
Publisher : Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains

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Catfish waste can be processed into fat or fish oil that can be used as a source of raw material for plasticizers with the trans-esterification reaction. Transesterification reaction is a reaction between oils (triglycerides) with the alcohol that produces Fatty acid alkyl esters. Products that include the type of fatty acid alkyl ester is a plasticizer. Plasticizer additive compound that is added to hard or rigid resin can improve the flexibility and workability. In this study, the plasticizer is synthesized by transesterification of waste oil catfish and butanediol, using natural zeolite catalyst activated. The process is done with a variety of molar ratio (1: 2, 1: 4, and 1: 6) and H-zeolite catalyst composition (10%, 15%, and 20%) of waste oil based ikana catfish, with a fixed variable reaction temperature 145- 1500C, stirring speed of 200 rpm and reaction time of 6 hours. From the analysis of the results shows that the transesterification and the molar ratio of H-zeolite catalyst composition affects the conversion of the resulting product. The highest operating conditions obtained in this study is the molar ratio of 1: 4 and H-zeolite catalyst composition of 15% which resulted in the conversion reaction of 25.35%. Characteristics plasticizer generated in this study are Viscosity (200 C) 0.910 mPa.s and Specific Gravity (200 C) 0.918.   Keywords: Plasticizer, Trans-esterification, Waste Oil Catfish, Butanediol, H-Zeolite
Pengaruh Waktu Reaksi Dan Rasio Molar Terhadap Asam Oleat Dengan Butanol Pada Sintesa Plastisizer Butil Oleat Selly, Mers; Nirwana, Nirwana; HS, Irdoni
Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains Vol 2, No 1 (2015): Wisuda Februari Tahun 2015
Publisher : Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains

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Abstract

The amount of palm oil feedstock in Indonesia, encourages the development of palm oil industry product diversification. One alternative for providing value-added palm oil by esterification of oleic acid is contained in palm oil became known as butyl oleate plasticizers. Plasticizer is an additive compound added to polymer to improve flexibility and workabilitas. Step of this research is the preparation of H-zeolite catalysts and synthesis of the plasticizer butyl oleate esterification using natural zeolite catalysts are activated to H-zeolites with varying reaction time (6, 9 and 12 hours) and the molar ratio of oleic acid and butanol (1: 6 , 1: 9 and 1:12) with the permanent variable stirring speed of 200 rpm, temperature of 108-112 ° C and catalyst-based as much as 15% oleic acid. From the test results showed that the reaction time and the molar ratio of the plasticizer effect on the synthesis of butyl oleate. Obtained value of 0.862 specific gravity and viscosity of 8.39 mPa by showing that the specific gravity and viscosity plasticizer produced meets the standards of commercial plasitisizer namely 0.862 to 0.928 and from 8.2 to 9.4. The highest achievement in this research was 76.73% with a molar ratio of 1:12 for 12 hours process.Keywords: Esterification, H-zeolites, Oils, Plasticizers
Pengaruh Penambahan Zat Aditif (Calcium Hypochlorite) Terhadap Coolant Properties (Viscosity) Minyak Sawit Skp, Buma Gempa; Masnur, Dedy; HS, Irdoni
Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains Vol 1, No 2 (2014): Wisuda Oktober Tahun 2014
Publisher : Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains

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Abstract

Cutting fluid (coolant) are required in the machining processes. Most of cutting fluid are from mineral oil, and they are as unrenewable resource, therefore look for alternative resources ofmineral oil, which derived from vegetables oil. Palm oil have potency based of cutting fluid, however of coolant properties increased additive. This research want investigate effect ofadditive on phiysical properties of coolant. The method on mixture combining palm oil and additive (calcium hypochlorite) are conducted take of three proportion (95:5), (90:10), (85:15), the results from mixture the tested physical properties of viscosity at 40oC and 100oC of temperature. The results acknowledge the addition of (calcium hypochlorite) with palm oileffects on phiysical properties of coolant, the greater the percentage of calcium hypochlorite viscosity increased.Keywords: Cutting fluid (coolant), palm oil, additive, calcium hypochlorite, physical properties.
Pemanfaatan Teknologi Elektrokoagulasi Untuk Pengolahan Limbah Cair Industri Tahu Menggunakan Elektroda Al-Al Dengan Variabel Jarak Elektroda Dan Kuat Arus Sinaga, Hendriyanto; Amri, Idral; HS, Irdoni
Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains Vol 6 (2019): Edisi 1 Januari s/d Juni 2019
Publisher : Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains

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Tofu factories located in Sigunggung Subdistrict, Pekanbaru, produce 0.9 to 1 m3 of liquid waste every day, and are immediately disposed of without going through the processing process so that they pollute the environment. The analysis shows that the liquid waste is not in accordance with Permen LH No. 5 2014. In this study the electrocoagulation method was used to reduce COD, BOD, TSS and neutralize pH. By varying the current strength, electrode distance and time the results obtained as follows: (1) the effective variation of electrode distance is 2 cm current strength of 0.6 A at 60 minutes can reduce the COD concentration to 76.36%, BOD 72, 83%, TSS 85.16% and pH to 6.31. (2) effective variation of current strength is 0.6 A distance of 2 cm at 60 minutes can reduce COD concentration to 72.90%, BOD 71.69%, TSS 83.83% and pH to 6.13. The results of the research obtained are in accordance with Permen LH No.5 2014.Keywords : electrocoagulation, TSS, COD, BOD, pH
Pemanfaatan Green Coke Sebagai Bahan Bakar Padat Yulia, Indri; HS, Irdoni; Bahruddin, Bahruddin
Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains Vol 4, No 2 (2017): Wisuda Oktober Tahun 2017
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The need for alternative energy sources keep increasing, green coke is a byproduct from refenery unit that has a high heating value, so it is potential to be used as an alternative fuel. The purpose of this experiment was to study the green coke briquetting process, studied the effect of the pressing pressure against the produced briquettes, and determine the effect of operating conditions on the heating value and the resulting compressive strength. Green coke used in this experiment was tested fors carbon content, then do briquetting by adding starch with the composition ratio of green coke to starch (95:5, 90:10, and 85:15 %weight) and the variation of pressure (120, 150, 180 Kg/cm2), with response of heating value and compressive strength, the response data obtained were processed using Respone Surface Methodology (RSM) using Design Expert application. The pressing pressure and the ratio of green coke has a significant effect on the heating value and compressive strength. Highest heating value obtained in the comparison of green coke composition: adhesive 95: 5 and the pressing pressure of 180 kg / cm2 with a calorific value of 37685.4 Kj / Kg, and a compressive strength of 4.72 kg / cm2Keywords : alternative energy, compressive strength, heating value, starch.
Pengaruh Kadar Filler Mikrokristalin Selulosa Dan Plasticizer Gliserol Terhadap Sifat Dan Morfologi Bioplastik Berbasis Pati Sagu Hendri, Zwilla Oktoriana; HS, Irdoni; Bahruddin, Bahruddin
Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains Vol 4, No 2 (2017): Wisuda Oktober Tahun 2017
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Bioplastic is one of alternative solution to change comercial plastic that can be dangerous to environment. Bioplastic can make degradation become easier. One of potential raw materialis sago because it has a highest starch component. The general aims of this research are the study of impact Microcrystalline cellulose filler and plasticizer glycerol to mechanicalproperties and morphology of bioplastic. The synthesis method is casting of starch, water, filler and plasticizer with composisition of filler is (4-12 % b/b), composisition of plasticizer (10–22 % b/b), and composisition of water (100-150 ml). The analysis of bioplastic is tensile strenght, elongation, modulus young, hidrophobicity (water uptake), biodegradation, SEM (Scanning Electron Microscopy), and design expert v.10.0.1 trial version. The most react variable is the composition of filler, followed by plastcizer glycerol and water ratio. The best process condition is bioplastic with composisition filler 12 %b/b, plasticizer 10 % b/b, andwater compotition 100 ml with the value is tensile strenght 14,21 Mpa, elongation 36,91%, water uptake 36,91%, and biodegradation 34,43%. Micrograf analysis shows that fillerdistribution is not equally on sago starch matrices and stil has a clod.Keywords : bioplastic, casting, filler, plasticizer, water uptake
Pengaruh Kadar Filler ZnO, Plasticizer Gliserol Dan Nisbah Air Terhadap Sifat Dan Morfologi Bioplastik Berbasis Pati Sagu Syahputra, Annur Fauzi; Bahruddin, Bahruddin; HS, Irdoni
Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains Vol 4, No 2 (2017): Wisuda Oktober Tahun 2017
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The need of plastic as plastic bags, food or goods packaging progressively increasing. Bioplastics is one alternative to conventional plastics that are harmful to the environment.one of the ingredients that can be used as bioplastics is starch, but starch-based bioplastics are still lacking at the mechanical properties. The purpose of this study was to determine thecharacteristics of sago starch, determine the effect of water ratio, the composition of the ZnO filler and plasticizer glycerol on mechanical properties and morphology of bioplastics. Sagostarch was tested for the composition of amylose and amylopectin, while the bioplastics is tested for mechanical properties such as tensile strength (tensile strenght), elongation, wateruptake, biodegradation, and dispersion of the filler through SEM (Scanning Electron Microscopy) and analyzed using Response Surface Methodology (RSM) , Significance levelused in this study is 0.05 so that the most significant variables can be determined from pvalue value of <0.05 and a lack of fit> 0.05, which indicates that the model according to theresearch results. The factors that most significantly influence all responses are ZnO filler composition and followed by the plasticizer and water ratio. Best results are obtained on thecomposition of 15% filler, plasticizer 10% and the ratio of water 100 ml with a tensile strength of 15.484 MPa, elongation 2.691%, water uptake 28%, and 22.12% biodegradation.Key Words : bioplastics, filler ZnO, glycerol, starch, biodegradation
Pengaruh Variasi Komposisi Aditif PEG Terhadap Kinerja Membran CA Al-Fitri, Mahriandhanie Chika; Pinem, Jhon Armedi; HS, Irdoni
Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains Vol 7 (2020): Edisi 2 Juli s/d Desember 2020
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The membrane is defined as a selective and semipermeable thin layer between two phases, namely the feed phase and the permeate phase. The purpose of this study is to make cellulose acetate from pineapple leaves, make cellulose acetate membrane with variations in the composition of PEG additives, and study the effect of PEG additive composition on the characteristics of cellulose acetate membranes produced. The methodology in this research is isolation of cellulose from pineapple leaves, synthesis of cellulose acetate from pineapple leaf fibers, synthesis of cellulose acetate membrane, pre-treatment of pulp and paper industry wastewater, and characterization of cellulose acetate membrane. The variation in the composition of the additives Polyethylene Glycol (PEG) used is 5, 10, 15 % w/w. Pulp and paper industrial wastewater treatment using cellulose acetate membrane is carried out with a variation of 2 bar operating pressure. The highest value of flux was obtained on membranes with a composition of PEG 15% w/w that is 39.922 L/m2.hour. The highest value of the rejection of COD, BOD5 and TSS parameters were obtained from the membrane with a PEG composition of 5% w/w, that are 67.13%; 76.45% and 74.42%. Keywords: membrane, polyethylene glycol (PEG), cellulose acetate
Pengaruh Komposisi Pelepah Sawit Terhadap Sifat Dan Morfologi Wood Plastic Composite Fauzi, Iwan; Bahruddin, Bahruddin; HS, Irdoni
Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains Vol 3, No 2 (2016): Wisuda Oktober Tahun 2016
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The availability of palm frond has a potential to use for decrease utilization of woods directly. One application is the wood plastic composite (WPC). Research on the WPC is still growing which aimsto continue to get better quality of product. The objective of this research was to determine the effect of palm frond composition to properties and the morphology of wood plastic composite(WPC). The Composition of palm frond measured at - 40 ~ +80 as the filler and the polypropylene as the matrix is 30:70 which mix with additive 2% and Maleic Anhydride Polypropylene (MAPP) 5%. Palm frond prepared using oxalic acid, potassium hydroxide, sodium hydroxide and hydrogen peroxide at a temperature of 120oC with 15 minutes immersion time. Filler mixing process, matrix, and the additive use Labo Plastomill internal mixer at a temperature of 170oC and the rotor speed at 80 rpm. Tests include cellulose test while the mechanical properties testing are tensile strength and flexural strength, and physical properties include density, water absorption and thickness swelling. Morphology test used the electron microscopy scanning with amagnification of 100 and 500 times. The results showed that the type of preparation has a relatively significant influence. Best WPC material is used oxalic acid mixture at a temperature of 120oC with19,214 MPa tensile strength, flexural strength of 43 639 MPa, density 0974 gr / cm3, 0.32% water absorption and thickness swelling 1.42%.Keyword: filler, palm frond, wood plastic composite
Co-Authors ADITYA NUGRAHA Ahmad Fadli Al-Fitri, Mahriandhanie Chika Amri, Idral Anugerah Rifaldi Ardiana, Amalia Bahruddin Bahruddin Bahruddin Bramansyah Riswanda Buma Gempa Skp, Buma Gempa Chairul Chairul David Hamonangan Dedy Masnur, Dedy Fernando S Sihotang Geo Rayfandy Hendri, Zwilla Oktoriana Idral Amri Inka Novela Jhon Armedi Pinem Joni Miharyono Mers Selly Mudinillah, Adam Muhammad Rivai Nirwana Nirwana Nirwana, Nirwana Nirwana, Nirwana Novita Aprilia Maya Sari, Novita Aprilia Maya Nurul Aini Thaibil Fadhly Rahmad Agung Yanuardhi Rio Andika Sinaga, Hendriyanto Syahputra, Annur Fauzi Ummy Aisyah Rochaeni Wahyu Okta Rinanda, Wahyu Okta Wira Bima Stevent Sembiring Yulia, Indri Yustinawati Yustinawati