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All Journal al-Kimiya EduChemia (Jurnal Kimia dan Pendidikan)
Dori Fitria
Department of Chemistry, Faculty of Science and Technology, Universitas Islam Negeri Sulthan Thaha Saifuddin Jambi, Jambi 36361, Indonesia
Chemical Engineering, Chemistry & Bioengineering Chemistry Education Materials Science & Nanotechnology

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Green Synthesis and Characterization of Cinnamylideneacetophenone Compound Using Fe3O4 Magnetic as Catalyst Dori Fitria; Antonius Herry Cahyana; Agus Rimus Liandi
EduChemia (Jurnal Kimia dan Pendidikan) Vol 6, No 2 (2021)
Publisher : Department of Chemical Education Faculty of Teacher Training and Education Universitas Su

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (759.808 KB) | DOI: 10.30870/educhemia.v6i2.10412

Abstract

Cinnamaldehyde is a compound found in the skin of cinnamon plants which has various bioactivity. In this study, the compound cinnamaldehyde was modified with the help of Fe3O4 which was synthesized with the help of seaweed extract as a heterogeneous catalyst. Fe3O4-MNPs are synthesized using FeCl3 and Sargassum filipendula extracts as their natural reducing agents. The catalytic ability of Fe3O4 was evaluated in the reaction between cinnamaldehyde and aromatic ketone compounds synthesized by the reflux method. Structure Analysis and elucidation of the synthesized compounds were carried out by measuring the vibrations of the functional groups by FTIR, and the determination of H and C atoms by HNMR and CNMR analysis. The FTIR, proton and carbon NMR analysis have identified that the synthesized product was cinnamylideneacetophenone by the name 1,5-diphenylpyenta-2,4-dien-1-one. The optimum conditions were obtained at a catalyst concentration of 10% w/w for five hours with a yield of 36%. The yield of this reaction was better than the reaction without a catalyst.
Synthesis and Characterization of 1-(1-naphthyl)-5-phenyl-2,4-pentadien-1-one from trans-cinnamaldehyde and 1-acetonaphthone Dori Fitria; Bayu Ardiansah; Atia Balkis
al Kimiya: Jurnal Ilmu Kimia dan Terapan Vol 10, No 1 (2023): al Kimiya: Jurnal Ilmu Kimia dan Terapan
Publisher : Department of Chemistry, Faculty of Science and Technology, UIN Sunan Gunung Djati Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.15575/ak.v10i1.22896

Abstract

Chalcone analogues (1-(1-naphthyl)-5-phenyl-2,4-pentadiene-1-one) have been synthesized through an aldol condensation reaction between cinnamaldehyde and 1-acetylnaphthalene. The method used in this study is the stirrer method, with the reaction conducted at room temperature for 24 hours using a NaOH catalyst in H2O/ethanol (50%, v/v). The purity of the product was analyzed using thin-layer chromatography on silica gel plates with n-hexane: ethyl acetate (9:1) employed as the solvent. The resulting product obtained was 0.88 g with a yield of 61.97%. Structure Analysis and elucidation of the synthesized compounds were performed by measuring the vibrations of the functional groups using FTIR, LCMSMS analysis, and determining the 1H and 13C atoms by HNMR and CNMR analysis. The FTIR, LCMSMS, 1H, and 13C NMR analysis identified that the synthesized product as chalcone analogues, specifically 1-(1-naphthyl)-5-phenyl-2,4-pentadiene-1-one.
Co-Authors Agus Rimus Liandi Antonius Herry Cahyana Atia Balkis Bayu Ardiansah