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All Journal Jurnal Keramik dan Gelas Indonesia Jurnal Keramik dan Gelas Indonesia
Irna Rosmayanti
Balai Besar Keramik
Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Electrical & Electronics Engineering Materials Science & Nanotechnology

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Synthesis and Characterization of Cetyl Piridinium Chloride Modified and Al2O3 Pillared Clay ferry arifiadi; Irna Rosmayanti; Herlina Damayanti; Hernawan Hernawan; Kristanto Wahyudi
Jurnal Keramik dan Gelas Indonesia Vol 29, No 2 (2020): Jurnal Keramik dan Gelas Indonesia
Publisher : Balai Besar Keramik

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32537/jkgi.v29i2.6673

Abstract

Bentonite is a mineral that is very abundant in Indonesia and has the potential to be developed, one of which is by adding intercalant to obtain a modified bentonite with the desired characteristics. In this study, the synthesis was carried out by the intercalation method by surfactant Cetyl pyridinium Chloride (CPC) with % weight variations and then followed by pillarization with aluminum polyoxo. Then the resulting solid phase is calcined at a temperature of 450oC. The results obtained were that bentonite with modified CPC and aluminum polyoxo had higher basal distance and surface area characteristics compared to natural bentonite and this increase was also proportional to the amount of CPC added before the pillarization process. The best modification value in the addition of CPC was 36% by weight with a basal distance of 16,8898 Å and a surface area of 276.478 m2 / g. From this research, it can be concluded that the addition of CPC and aluminum polyoxo to bentonite can increase the basal distance and its surface area. The added CPC concentration also has an effect on increasing the number of pillar cations that enter the bentonite so that the pillarization that occurs in bentonite is more and causes the characteristics of the bentonite to be better.
The Effect of Alkali Addition and Coating Time on Hydrophilic Properties of Antimocrobial Ceramic Tiles Irna Rosmayanti; Rizky Berliana Wijayanti; Eneng Maryani
Jurnal Keramik dan Gelas Indonesia Vol 28, No 2 (2019): Jurnal Keramik dan Gelas Indonesia
Publisher : Balai Besar Keramik

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32537/jkgi.v28i2.5759

Abstract

Antimicrobial glaze is used for sanitation needs in special environments such as hospitals or schools. Antimicrobial properties of TiO2 involve photocatalytic activity on  inorganic material. A hydrophilic surface, with contact angle value <65o, is resulted by those activity. In this study, polished tile coating was done using TiO2 material which had been prepared through a dissolving process in sulfuric acid followed by gel formation with addition of 2 types of alkali, ammonia and ammonium bicarbonate. The TiO2 gel formed was dispersed in aquadest and then coated on the surface of the tile by dip coating with various deposition time (3 hours, 6 hours and 53 hours). ANOVA test results represent that both main effect of alkali type and coating time, and interaction effect of these variable produce significant effects on contact angles. Addition of ammonium bicarbonate produce better hydrophilic surface on the tile than addition of ammonia. The longer coating time will increase hydrophilic characteristic of the surface.
Synthesis and Characterization of Cetyl Piridinium Chloride Modified and Al2O3 Pillared Clay ferry arifiadi; Irna Rosmayanti; Herlina Damayanti; Hernawan Hernawan; Kristanto Wahyudi
Jurnal Keramik dan Gelas Indonesia Vol 29, No 2 (2020): Jurnal Keramik dan Gelas Indonesia
Publisher : Balai Besar Keramik

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32537/jkgi.v29i2.6673

Abstract

Bentonite is a mineral that is very abundant in Indonesia and has the potential to be developed, one of which is by adding intercalant to obtain a modified bentonite with the desired characteristics. In this study, the synthesis was carried out by the intercalation method by surfactant Cetyl pyridinium Chloride (CPC) with % weight variations and then followed by pillarization with aluminum polyoxo. Then the resulting solid phase is calcined at a temperature of 450oC. The results obtained were that bentonite with modified CPC and aluminum polyoxo had higher basal distance and surface area characteristics compared to natural bentonite and this increase was also proportional to the amount of CPC added before the pillarization process. The best modification value in the addition of CPC was 36% by weight with a basal distance of 16,8898 Å and a surface area of 276.478 m2 / g. From this research, it can be concluded that the addition of CPC and aluminum polyoxo to bentonite can increase the basal distance and its surface area. The added CPC concentration also has an effect on increasing the number of pillar cations that enter the bentonite so that the pillarization that occurs in bentonite is more and causes the characteristics of the bentonite to be better.
The Effect of Alkali Addition and Coating Time on Hydrophilic Properties of Antimocrobial Ceramic Tiles Irna Rosmayanti; Rizky Berliana Wijayanti; Eneng Maryani
Jurnal Keramik dan Gelas Indonesia Vol 28, No 2 (2019): Jurnal Keramik dan Gelas Indonesia
Publisher : Balai Besar Keramik

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32537/jkgi.v28i2.5759

Abstract

Antimicrobial glaze is used for sanitation needs in special environments such as hospitals or schools. Antimicrobial properties of TiO2 involve photocatalytic activity on  inorganic material. A hydrophilic surface, with contact angle value <65o, is resulted by those activity. In this study, polished tile coating was done using TiO2 material which had been prepared through a dissolving process in sulfuric acid followed by gel formation with addition of 2 types of alkali, ammonia and ammonium bicarbonate. The TiO2 gel formed was dispersed in aquadest and then coated on the surface of the tile by dip coating with various deposition time (3 hours, 6 hours and 53 hours). ANOVA test results represent that both main effect of alkali type and coating time, and interaction effect of these variable produce significant effects on contact angles. Addition of ammonium bicarbonate produce better hydrophilic surface on the tile than addition of ammonia. The longer coating time will increase hydrophilic characteristic of the surface.
Co-Authors Eneng Maryani ferry arifiadi Herlina Damayanti Hernawan Hernawan Kristanto Wahyudi Rizky Berliana Wijayanti