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All Journal Bulletin of Chemical Reaction Engineering & Catalysis Bulletin of Chemical Reaction Engineering & Catalysis
Manal Afham Toma
Department of Chemical Engineering, University of Technology, Baghdad
Chemical Engineering, Chemistry & Bioengineering Chemistry

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The Effect of Solvent-Modification on the Physicochemical Properties of ZnO Nanoparticles Synthesized by Sol-Gel Method Zainab Yousif Shnain; Manal Afham Toma; Basheer A. Abdulhussein; Najat J. Saleh; Mohammed Ibrahim; Nerran Manuel; Abbner Mahmood
Bulletin of Chemical Reaction Engineering & Catalysis 2022: BCREC Volume 17 Issue 1 Year 2022 (March 2022)
Publisher : Department of Chemical Engineering - Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.17.1.12345.46-52

Abstract

This study investigated the solvent effect on the synthesis of Zinc Oxide (ZnO) nanoparticle using sol-gel method. Zinc acetate dihydrate and oxalic acid were used as a chemical precursor for the synthesis of the ZnO nanoparticle considering the effects of various solvents. The effect of using water, propanol, or ethanol as solvent during the synthesis were examined. The resultant gel in the aqueous and organic moderate solvent was thermally cracked into ZnO nanoparticles at 450 °C under atmospheric pressure. The results showed that the solvent type has a significant effect on the morphology and particles size of the ZnO nanoparticles synthesized. Atomic Force Microscopy (AFM) was used to investigate the microstructure of the nanoparticles. The crystalline and chemical structure of the prepared ZnO nanoparticle were studied by X-ray diffraction (XRD) and Fourier Transform Infrared spectroscopy (FTIR). The average diameter of nano-size particles obtained for ethanol, propanol and water are 79.55 nm, 83.86 nm and 85.59 nm, respectively. ZnO particles showed higher degree of crystalline in water compared to other solvents under current investigation. Copyright © 2021 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). 
The Effect of Solvent-Modification on the Physicochemical Properties of ZnO Nanoparticles Synthesized by Sol-Gel Method Zainab Yousif Shnain; Manal Afham Toma; Basheer A. Abdulhussein; Najat J. Saleh; Mohammed Ibrahim; Nerran Manuel; Abbner Mahmood
Bulletin of Chemical Reaction Engineering & Catalysis 2022: BCREC Volume 17 Issue 1 Year 2022 (March 2022)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.17.1.12345.46-52

Abstract

This study investigated the solvent effect on the synthesis of Zinc Oxide (ZnO) nanoparticle using sol-gel method. Zinc acetate dihydrate and oxalic acid were used as a chemical precursor for the synthesis of the ZnO nanoparticle considering the effects of various solvents. The effect of using water, propanol, or ethanol as solvent during the synthesis were examined. The resultant gel in the aqueous and organic moderate solvent was thermally cracked into ZnO nanoparticles at 450 °C under atmospheric pressure. The results showed that the solvent type has a significant effect on the morphology and particles size of the ZnO nanoparticles synthesized. Atomic Force Microscopy (AFM) was used to investigate the microstructure of the nanoparticles. The crystalline and chemical structure of the prepared ZnO nanoparticle were studied by X-ray diffraction (XRD) and Fourier Transform Infrared spectroscopy (FTIR). The average diameter of nano-size particles obtained for ethanol, propanol and water are 79.55 nm, 83.86 nm and 85.59 nm, respectively. ZnO particles showed higher degree of crystalline in water compared to other solvents under current investigation. Copyright © 2021 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). 
Co-Authors Abbner Mahmood Basheer A. Abdulhussein Mohammed Ibrahim Najat J. Saleh Nerran Manuel Zainab Yousif Shnain