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All Journal Bulletin of Chemical Reaction Engineering & Catalysis Bulletin of Chemical Reaction Engineering & Catalysis
Ying Mei Zhou
School of Chemistry and Chemical Engineering, Xuzhou Institute of Technology, Xuzhou, Jiangsu 221111
Chemical Engineering, Chemistry & Bioengineering Chemistry

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Preparation of FeO(OH) Modified with Polyethylene Glycol and Its Catalytic Activity on the Reduction of Nitrobenzene with Hydrazine Hydrate Ke Ying Cai; Yu Sheng Liu; Ming Song; Ying Mei Zhou; Qing Liu; Xiao Hui Wang
Bulletin of Chemical Reaction Engineering & Catalysis 2016: BCREC Volume 11 Issue 3 Year 2016 (December 2016)
Publisher : Department of Chemical Engineering - Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (936.166 KB) | DOI: 10.9767/bcrec.11.3.576.363-368

Abstract

Iron oxyhydroxide was prepared by dropping ammonia water to Fe(NO3)3.9H2O dispersed in polyethylene glycol (PEG) 1000. The catalyst was characterized by X-ray powder diffraction, Fourier transform infrared spectroscopy and laser particle size analyzer. The results showed the catalyst modified with polyethylene glycol was amorphous. The addition of PEG during the preparation make the particle size of the catalyst was smaller and more uniform. The catalytic performance was tested in the reduction of nitroarenes to corresponding amines with hydrazine hydrate, and the catalyst showed excellent activity and stability. 
Reduction of Nitroarenes to Aromatic Amines with Sodium Borohydride in the Presence of Selenium and Actived Carbon Ke Ying Cai; Ying Mei Zhou
Bulletin of Chemical Reaction Engineering & Catalysis 2015: BCREC Volume 10 Issue 3 Year 2015 (December 2015)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.10.3.8512.275-280

Abstract

A selenium and actived carbon (AC) catalyst has been applied for the selective reduction of nitroarenes to their corresponding amines respectively using sodium borohydride (NaBH4) as a reducing source un-der mild conditions. Under the optimized conditions, efficient and selective reduction of nitroarenes into the corresponding aromatic amines occurred over a recyclable selenium catalyst. The catalyst can be easily recovered after catalytic reaction and readily reused for 4 cycles with consistent activity hence reduces the cost of the catalyst. Copyright © 2015 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).
Co-Authors Ke Ying Cai Ming Song Qing Liu Xiao Hui Wang Yu Sheng Liu