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Characterization of Glucosamine Nano Particles from Chitosan Using Ultrasonicators and Ball Milling Methods Bhatara Ayi Meata; Ginanjar Pratama; Rifki Prayoga Aditia; Afifah Nurazizatul Hasanah; Dini Surilayani; Sakinah Haryati; Aris Munandar
Jurnal Perikanan dan Kelautan Vol 11, No 2 (2021)
Publisher : JURNAL PERIKANAN DAN KELAUTAN

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33512/jpk.v11i2.12886

Abstract

Oral consumption of glucosamine hydrochloride can worsen side effects in the human body, so the development of nanoparticles from glucosamine hydrochloride is needed as a topical preparation in treating osteoarthritis. This study aims to determine the differences in the characteristics of nanoparticles from shrimp shell glucosamine made ultrasonic and ball milling. For the production of glucosamine from shrimp shells, the acid hydrolysis method was used using 37% HCL solution, then washed with IPA solution until glucosamine powder was formed, then the yield and FTIR tests were carried out. Preparation of glucosamine nanoparticles using the ultrasonic method, namely glucosamine with a 37% HCl mixture sonicated using an ultrasonicator, and another method using a ball mill to fission glucosamine to obtain powdered glucosamine nanoparticles. The powder obtained from the two methods was then characterized using a scanning electron microscope (SEM) to determine the morphological condition of the solid. The results of the glucosamine test obtained a yield of 83.65%, and the absorption pattern of the Fourier transform infrared (FTIR) spectrum showed 99.82% so that it met the quality standards proving that glucosamine hydrolysis was successful. The powder characterization obtained by SEM aims to determine the size characteristics of the glucosamine nanoparticles obtained. The resulting powder nanoparticles are yellow-white. The SEM photo results show the morphology of the particles with an uneven surface. The results of the Scanning Electron Microscope (SEM) test showed that the particle size of glucosamine by ultrasonic and ball milling methods were 83.56 nm and 61.16 nm, respectively.
Effect of Substitution Kurisi Fish (Nemipterus sp.) for Milk Fish Satay Production Bhatara Ayi Meata; Dwi Mulyani; Sakinah Haryati; Aris Munandar; Ginanjar Pratama; Rifki Prayoga Aditia; Afifah Nurazizatul Hasanah; Devi Faustine Elvina Nuryadin
Leuit (Journal of Local Food Security) Vol 4, No 1 (2023)
Publisher : Pusat Unggulan Iptek Ketahanan Pangan Universitas Sultan Ageng Tirtayasa

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.37818/leuit.v4i1.19641

Abstract

Milkfish satay is a traditional fishery product originating from the Serang area, Banten Province. The main problem with milkfish satay is that the raw material for milkfish is very expensive. Innovation in making milkfish satay can be done by substituting meat from other fish. The purpose of this study was to determine the best formulation of milkfish satay with a combination of milkfish and kurisi fish, and to determine the nutritional content of milkfish satay with a combination of milkfish and kurisi fish. Determination of the best formulation of milkfish satay with the addition of kurisi fish and determining its nutritional value. The formulations tested in the main research were A(100% DB + 0% DK), B(75% DB + 25% DK), C(50% DB + 50% DK), D(25% DB + 75% DK) , E(0% DB + 100% DK). This study was analyzed by organoleptic tests (appearance, color, taste, aroma and texture), proximate (protein, fat, water and ash), microbiology (TPC). Microbiological data were analyzed by means of one-way ANOVA and the organoleptic test was carried out by the Kruskal-Wallis test. If significantly different results were obtained, then Duncan's further test was carried out.