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All Journal Program Kreativitas Mahasiswa - Penelitian Alchemy Jurnal Penelitian Kimia
Ganjar Fadillah, Ganjar
Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam, Universitas Sebelas Maret
Chemical Engineering, Chemistry & Bioengineering Energy Environmental Science Materials Science & Nanotechnology

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EFFECTIVENESS OF GELATIN EXTRACTED FROM CHICKEN CLAWS AS A NATURAL PRESERVATIVES FOR BEEF AND FISH Fadillah, Ganjar; Kusuma, Pramudita Putri; Saraswati, Teguh Endah
Alchemy Jurnal Penelitian Kimia Vol 10, No 2 (2014)
Publisher : Alchemy Jurnal Penelitian Kimia

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Abstract

Gelatin has been successfully extracted from chicken claws by acid hydrolysis method through four major stages of degreasing, demineralization, extraction and drying. The yield of extracted gelatin obtained from wet chicken claws was about 6.21% (w/w). The effectiveness of gelatin as preservative applied in beef and fish was physically, chemically and microbiologically studied by organoleptic analysis, peroxide test, bacteria inhibition test and number calculation, respectively. Organoleptic analysis by hedonic test shows there were significant differences for color and texture parameters between gelatin-coated samples and control samples at concentrations of 1:1 (w/w). Peroxide number analysis by iodometry indicates the use of gelatin in the preservation of meat and fish decreased the oxidation number. The result of inhibition test againts Staphylococcus aureus bacteria shows the gelatin concentration of 20% provided greatest halo zone diameter (inhibitory region) as 19.44±2.11 mm. The colony bacteria test shows the use of gelatin potentially inhibited the growth of bacteria up to 75%. Overall, the results conclude that gelatin extracted from chicken claws has the potential activities as a natural preservative for beef and fish. 
PERANAN ZEOLIT NANOPORI TERMODIFIKASI SEBAGAI MATERIAL PENGONTROL PELEPASAN PUPUK UREA Hidayat, Rahmat; Fadillah, Ganjar; Chasanah, Uswatul; Wahyuningsih, Sayekti
Program Kreativitas Mahasiswa - Penelitian PKM-P 2014
Publisher : Ditlitabmas, Ditjen DIKTI, Kemdikbud RI

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Abstract

Effectiveness of catalyst zeolite nanoporous as a slow release fertilizer of nitrogen from urea has been researched. In this study, natural zeolite was activated by HF 1%  with a calsination temperature at 120oC and the surface of zeolite was modified by aminopropyltrimethoxysilane (APTMS) 5%. Zeolite activation was characterized by X-ray diffraction spectroscopy (XRD) and Surface Area Analyzer (SAA) while the modified zeolite was characterized by infrared spectroscopy (FTIR), Surface Area Analyzer (SAA) and UV-Vis spectroscopy. The results of the material characterization of zeolite-APTMS obtained size pore of 7,74 nm with a maximum adsorption capacity of urea was 3.668 mg/g. Slow release urea test  from zeolite-APTMS performed by observing the absorbance of the urea at a wavelength of 195 nm with a variation of time 0, 5,10,20,40,60,80,100 and 120 minutes The test of fertilizers in the soil is directly done by observing changes pH and release of NH4+ in the incubation time of 14 days. The results show that urea without zeolite will be released 100% in the 120 minute and zeolite-APTMS aqueous solution at minute 120 only released about 56,24%. While the application of fertilizers in the soil is directly obtained that urea with zeolite having a pH decrease slowly compared to urea without zeolite. It is addressed that the zeolite-APTMS potentially be developed as a release control material of nitrogen from urea is caused due to the ability of the zeolite to absorb urea-APTMS temporarily in the pore and hydrogen bonding interactions between the urea and N-H from APTMS. Keywords:  zeolite, zeolite-APTMS, urea, slow release fertilizer
Co-Authors Pramudita Putri Kusuma, Pramudita Putri Rahmat Hidayat Sayekti Wahyuningsih Teguh Endah Saraswati Uswatul Chasanah, Uswatul