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All Journal Jurnal Bahan Alam Terbarukan PROSIDING SEMINAR KIMIA JURNAL ATOMIK
Teguh Wirawan, Teguh
Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman
Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Energy Environmental Science Materials Science & Nanotechnology

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ELEKTRODEKOLORISASI LIMBAH CAIR ZAT WARNA JINGGA DAN HIJAU DARI INDUSTRI SARUNG TENUN SAMARINDA MENGGUNAKAN ELEKTRODA PbO2/Pb Yulieta, Afifah Nur; Wirawan, Teguh; Panggabean, Aman Sentosa
PROSIDING SEMINAR KIMIA Vol 2 No 2 (2024): Prosiding SNKT III 2023
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

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Abstract

Electrodecolorization of liquid waste from Samarinda Seberang woven sarong industry using PbO2/Pb electrode was to reduce the dye content of Samarinda Seberang woven sarong waste by electrodecolorization method using lead (Pb) as cathode and lead dioxide (PbO2) as anode. Electrodecolorization of Direk orange and green dyes was carried out by varying the working potential, electrolyte concentration, time and dye concentration. The optimum condition of the Direk orange dye solution is using a working potential of 12 volts, 0.2 M Na2SO4 electrolyte concentration for 15 minutes and the Direk green dye solution is at a working potential of 10.5 volts, 0.2 M Na2SO4 electrolyte concentration for 15 minutes. The percentage of decolorization of the waste liquid sample of the Samarinda orange woven sarong industry using the PbO2/Pb electrode at the maximum condition is 99.58% and the percentage of decolorization of the waste liquid sample of the Samarinda green woven sarong industry using the PbO2/Pb electrode at the maximum condition is 98.46%. Keywords: Electrodecolorization, PbO2/Pb electrode, Na2SO4 electrolyte, Samarinda woven sarong industry waste.
Green Synthesis Of Silver Nanoparticles Using Ketapang Leaf Extract (Terminalia Catappa L.) Assisted By Ultrasound Syaima, Husna; Hindryawati, Noor; Hiyahara, Irfan Ashari; Wirawan, Teguh; Arief, M. Syaiful; Widodo, Nanang Tri; Ahmad, Atika Aulia; Maniam, Gaanty Pragas
Jurnal Bahan Alam Terbarukan Vol 12, No 2 (2023): December 2023 [Nationally Accredited Sinta 2]
Publisher : Universitas Negeri Semarang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.15294/jbat.v12i2.48809

Abstract

Green synthesis of silver nanoparticles using plants has been interesting in recent years. In the present study, the silver nanoparticles were synthesized using a bioreductor from ketapang leaf extract (Terminalia catappa L.) assisted by sonochemical methods. This green synthesis provides an economic, eco-friendly, and clean synthesis route for silver nanoparticles. Different concentrations of AgNO3 precursors (0.5; 1.0 and 1.5 mM) were initially reacted with ketapang leaf extract with PVA 1% solution as stabilizers that were sonicated for 30 minutes. Silver nanoparticle colloidal solutions were characterized using UV-Vis spectrophotometers, Particle Size Analyzers (PSA), and Transmission Electron Microscopes (TEM). Maximum absorption of silver nanoparticles was obtained at wavelength 420-450 nm. Based on UV data, the silver nanoparticles showed stability for up to 3 weeks. The XRD peaks indicated that the (111) crystallographic plane was more predominant than other planes. The average size of the silver nanoparticles was 79.7 nm from the PSA result. TEM imaging depicted that the nanoparticles were spherical. Finally, the result proved that the silver nanoparticles effectively removed the methylene blue up to 76.43% within optimum conditions (3 ppm of methylene blue, 15 minutes contact time, and 8% nanoparticle concentration).
ELEKTRODELOKALISASI ZAT WARNA LIMBAH CAIR SARUNG TENUN SAMARINDA MENGGUNAKAN ELEKTRODA PbO2/Cu Menono, Fera Friskaneke; Wirawan, Teguh; Panggabean, Aman Sentosa
JURNAL ATOMIK Vol 9 No 1 (2024)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v9i1.1361

Abstract

Electrodecolorization of Sarung Tenun Samarinda liquid waste dyestuff using PbO2/Cu electrode has been conducted. This study aims to reduce the level of dyes in Sarung Tenun Samarinda liquid waste samples by electrodecolorization method using lead dioxide (PbO2) electrode as anode and Copper (Cu) as cathode. Electrodecolorization was carried out by varying the working potential, Na2SO4 electrolyte concentration, time, and dye concentration in order to obtain optimum conditions for dye decolorization by electrolysis process. The concentration of the dye was determined by calculating the absorbance data obtained from measurements using a UV-Vis spectrophotometer. The results showed that the optimum conditions of electrodecolorization on orange dyes using PbO2/Cu electrodes were a working potential of 10.5 volts, 0.2 M Na2SO4 electrolyte concentration and a time of 20 minutes. In green dyes, the optimum conditions are working potential of 10.5 volts, electrolyte concentration of Na2SO4 0.1 M and time for 15 minutes. The percentage of decolorization of the orange Sarung Tenun Samarinda liquid waste sample using the PbO2/Cu electrode was 100% and in the green Sarung Tenun Samarinda liquid waste sample was 100%.
Adsorpsi Fenol oleh Arang Aktif Ampas Kopi Teraktivasi Fisik dan Kimia Nurfarizha, Harisma; Wirawan, Teguh; Widodo, Nanang Tri
JURNAL ATOMIK Vol 6 No 2 (2021)
Publisher : Jurusan Kimia FMIPA UNMUL

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Activated charcoal was prepared from coffee grounds using carbonization at 500⁰C as a physical activation and also by chemical activation using sulphuric acid. Chemical characterization of the activated charcoal was performed by Fourier Transform Infrared Spectroscopy. The optimum conditions for phenol adsorption was attained at pH 4 and 60 minutes of contact time. Adsorption isotherms from Freundlich
ADSORPSI ZAT WARNA TEKSTIL UNGU DARI AIR LIMBAH INDUSTRI RUMAH TANGGA SARUNG TENUN SAMARINDA SEBERANG DENGAN MENGGUNAKAN SERBUK KULIT BUAH LAI (DURIO KUTEJENSIS (HASSK.) BECC.) Oliviani, Nadira; Wirawan, Teguh; Sitorus, Saibun
JURNAL ATOMIK Vol 8 No 2 (2023)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

Pewarna tekstil termasuk senyawa yang sulit terurai secara alami, sehingga dapat berdampak negatif terhadap lingkungan perairan. Penelitian ini bertujuan untuk memanfaatkan kulit buah lai yang dibuat menjadi serbuk sebagai adsorben untuk menyerap zat warna tekstil ungu pada air limbah sarung tenun Samarinda Seberang. Tahap pertama dibuat dengan membilas bubuk kulit buah lai dengan air suling mendidih, kemudian dipanggang dan diayak dengan ayakan 60 mesh. Karakterisasi dilakukan dengan menggunakan Fourier Transform Infared (FTIR) dan Scanning Electron Microscopy (SEM). Kajian adsorpsi zat warna tekstil ungu oleh serbuk kulit buah lai dilakukan dengan variasi waktu, pH dan konsentrasi. Hasil karakterisasi dengan FTIR menunjukkan adanya CO, CH bending, C=C, C=O, CC alkena,Gugus CH dan berdasarkan hasil karakterisasi SEM serbuk cangkang lainnya memiliki permukaan yang berpori. Kondisi optimum adsorpsi zat warna tekstil ungu 100 ppm untuk 25 mL dengan berat adsorben 0,01 g terjadi pada waktu kontak 2,5 menit dan pH 9. Adsorpsi zat warna tekstil ungu mengikuti pola adsorpsi isoterm Langmuir dan memiliki kapasitas adsorpsi maksimum sebesar 1176 .0486 mg/g. Aplikasi pada sampel air limbah sarung tenun ungu Samarinda Seberang dengan konsentrasi 143,5 ppm sebanyak 25 mL dan menggunakan berat optimum 0,01 g, waktu 2,5 menit dan pH 9 diperoleh %Adsorpsi sebesar 72,0119%. 5 menit dan pH 9. Adsorpsi zat warna tekstil ungu mengikuti pola adsorpsi isoterm Langmuir dan memiliki kapasitas adsorpsi maksimum sebesar 1176 .0486 mg/g.Aplikasi pada sampel air limbah sarung tenun ungu Samarinda Seberang dengan konsentrasi 143,5 ppm sebanyak 25 mL dan menggunakan berat optimum 0,01 g, waktu 2,5 menit dan pH 9 diperoleh %Adsorpsi sebesar 72,0119%. 5 menit dan pH 9. Adsorpsi zat warna tekstil ungu mengikuti pola adsorpsi isoterm Langmuir dan memiliki kapasitas adsorpsi maksimum sebesar 1176 .0486 mg/g. Aplikasi pada sampel air limbah sarung tenun ungu Samarinda Seberang dengan konsentrasi 143,5 ppm sebanyak 25 mL dan menggunakan berat optimum 0,01 g, waktu 2,5 menit dan pH 9 diperoleh %Adsorpsi sebesar 72,0119%.
ADSORPSI FENOL MENGGUNAKAN ADSORBEN KOMPOSIT Fe3O4-ARANG AKTIF AMPAS KOPI Reknosari, Elen; Wirawan, Teguh; Koesnarpadi, Soerja
JURNAL ATOMIK Vol 6 No 2 (2021)
Publisher : Jurusan Kimia FMIPA UNMUL

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ABSTRAK Adsorpsi fenol menggunakan adsorben komposit Fe3O4-Arang aktif ampas kopi telah dilakukan. Adsorben komposit Fe3O4-Arang aktif ampas kopi disintesis dari FeSO4.7H2O dan FeCl3.6H2O dengan perbandingan 3:2 kemudian dikomposit dengan arang aktif ampas kopi. Adsorben komposit Fe3O4-Arang aktif ampas kopi dikarakterisasi dengan Fourier Transform Infared (FTIR) dan Scanning Electron Microscopy (SEM) serta dilakukan uji adsorpsi terhadap fenol. Hasil karakterisasi dengan Fourier Transform Infared (FTIR), muncul peak 1604,77 cm-1 menunjukkan adanya serapan C=O yang menyatakan bahwa ampas kopi telah membentuk zat karbon. Selain itu adsorben komposit Fe3O4-arang aktif ampas kopi muncul peak pada panjang gelombang 509,21 cm-1 yang merupakan gugus Fe-O menunjukkan bahwa nanopartikel Fe3O4 telah berhasil tercangkok pada struktur arang aktif. Kondisi optimum adsorpsi fenol menggunakan adsorben komposit Fe3O4-arang aktif ampas kopi adalah pada waktu kontak 30 menit dan pH 5. Kata kunci: Adsorpsi, Fenol, Magnetit, Arang Aktif, Ampas Kopi
Adsorption Of Dye From Household Industrial Wastewater Of Samarinda Seberang Weaving Gloves Using Adsorbent From Activated Charcoal Lai Fruit Powder (Durio Kutejensis (Hassk.) Becc.) Sari, Riska Alif Kartika; Wirawan, Teguh; Sitorus, Saibun
JURNAL ATOMIK Vol 9 No 1 (2024)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v9i1.1271

Abstract

Textile dyes include compounds that are difficult to decompose naturally. In the waters is a serious environmental problem because it can have a negative impact. This study aims to utilize lai fruit peel which is used as activated charcoal as an adsorbent to adsorb purple dyes in woven sarong waste water. The first stage of making activated charcoal is through carbonation in a furnace at 500oC for 30 minutes. Activation was carried out chemically by immersing it in 2 M H2SO4 solution for 24 hours. FTIR characterization of the resulting activated carbon was carried out to determine its functional groups and SEM characterization to determine its morphology. The results of FTIR characterization of activated carbon from lai fruit peel powder have functional groups -CO- and –OH, while SEM characterization of activated carbon from lai fruit peel powder is in the form of fibers with open pore surfaces that are spread on the surface and cavity walls of the activated charcoal of lai fruit peel powder. The adsorption process was carried out using the bath method and the concentration of the purple dye was determined using a UV-Vis spectrophotometer. The results showed that the adsorption of purple dye by activated charcoal was optimal at contact time of 1 minute and at pH 8. Adsorption of purple dye followed by the Freundlich adsorption pattern and had a maximum chemical adsorption capacity of 55.209 mg/g.
Co-Authors Ahmad, Atika Aulia Aman Sentosa Panggabean Arief, M. Syaiful Gaanty Pragas Maniam, Gaanty Pragas Hiyahara, Irfan Ashari Menono, Fera Friskaneke Nanang Tri Widodo Noor Hindryawati, Noor Nurfarizha, Harisma Oliviani, Nadira Reknosari, Elen Saibun Sitorus Sari, Riska Alif Kartika Soerja Koesnarpadi Syaima, Husna Yulieta, Afifah Nur