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Maulana, Jibril
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Energy Engineering Industrial & Manufacturing Engineering Materials Science & Nanotechnology Mechanical Engineering

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Journal : Journal of Mechanical Engineering Science and Technology

 1 
Effect of Addition Titanium Dioxide Nanoparticle on Properties of Pineapple Leaf Fiber Mediated TEMPO Oxidation Oxidation Ikrom, Muhamad; Suryanto, Heru; Fikri, Ahmad Atif; Aminnudin, Aminnudin; Maulana, Jibril; Fadillah, Faqih; Mito, Mohamed T; Masera, Kemal
Journal of Mechanical Engineering Science and Technology (JMEST) Vol 8, No 1 (2024)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um0168i12024p082

Abstract

Indonesia is an agricultural country with the potential to grow many plants as natural fiber sources. In order to improve its properties, natural fiber needs to be treated by applying nanomaterial so that it can compete with the characteristics of synthetic fibers. The study aims to determine the influence of adding titanium dioxide (TiO2) nanoparticles on pineapple leaf fiber (PALF) characteristics. The PALF was collected from the Subang plantation (Indonesia). The chemical treatment was carried out with pre-treatment using an alkalization process for 3 hours, and the oxidation process was carried out with TEMPO. TiO2 nanoparticle grafting was carried out by adding a silane solution with a ratio of 1:10 with alcohol. The characteristics of PALF were observed using XRD, FTIR, SEM, and tensile tests. The results show that the crystallinity of the PALF increased after TEMPO treatment. PALF form Si-O-C bond identified at a wavelength of 1158 cm-1 after silane treatment. Ti – O – Si functional groups were identified in the 660 cm-1 – 670 cm-1 wavelength range. In the fiber surface, agglomerated TiO2 nanoparticles are formed and increase with increasing TiO2 nanoparticle concentration. The tensile stress of treated PALF is increased by 125%, with the highest tensile strength of 1279.18 MPa, obtained by TiO2 nanoparticle concentration of 1.0%.
Mechanical Properties of Corner Lap-45 Types Joined Using Friction Stir Welding Setiawan, Widia; Santoso, Nugroho; Winarto, Felixianus Eko Wismo; Krisnaputra, Radhian; Mandala, Wirawan Widya; Maulana, Jibril
Journal of Mechanical Engineering Science and Technology (JMEST) Vol 8, No 1 (2024)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um016v8i12024p178

Abstract

Solid welding has always been concerned with probe design, pins, and joint strength. Many researchers have conducted studies on joints, such as butt joints, lap joints, and T joints, but the results show low strength. This study analyzes the mechanical properties of a new design of a 90o angle joint joined by friction stir welding. This study connected aluminum 6061 using the friction stir welding method using a rectifying jig and a probe with EMS 45 material. The corner joint designs used corner-lap 45 with feed rate as independent variables in 6, 8, 10, 15, and 30 mm/min and dependent variable probe rotation speed at 1000 rpm and shoulder pressure in 584 kg. The results show low feed rates create chips and fish fins on the advancing side, and microstructure test results at low feed rates (6-15 mm/min) indicate the presence of interface bonding. The hardness value of the stir zone also shows an insignificant increase. In the tensile test results, the tensile strength decreases from the base metal value, which then the tensile strength increases along with the increase in feed rate up to a feed rate of 15 mm/min and decreases again at a feed rate of 30 mm/min.
Effect of Graphene Addition on Bacterial Cellulose-Based Nanocomposite Maulana, Jibril; Suryanto, Heru; Aminnudin, Aminnudin
Journal of Mechanical Engineering Science and Technology (JMEST) Vol 6, No 2 (2022)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um016v6i22022p107

Abstract

Bacterial cellulose (BC) is a widespread, low-cost biopolymer that has generally been produced from plants and biomass waste. A method for improving the range of applications for bacterial cellulose is adding graphene material. It has an outstanding feature that can increase the performance of nanocomposite materials. The research aims to observe the effect of graphene on the surface morphology, crystallinity, chemical bonding, and tensile strength of BC/CuO nanocomposite. For this study's synthesis, BC was synthesized by fermenting pineapple peel extract for 10 to 14 days. The produced BC was crushed, homogenized with a nano homogenizer machine, and filtered. Filtered BC, CuO, and graphene were added to obtain a solution, and the mixture was first stirred magnetically, followed by an ultrasonic homogenizer, and finally dried using a freeze-dry method to make a porous nanocomposite. According to SEM analysis, the addition of CuO and graphene can fill porosity nanocomposite. By XRD analysis, the addition of graphene reduces the crystallinity of BC/CuO. The FTIR data showed that adding graphene reduces hydrogen bonding and makes some Cu-O-C bonding. The tensile test has demonstrated that the tensile strength of BC-based nanocomposite with graphene reinforcement tends to decrease.
Effect of the Homogenization Process on Titanium Oxide-Reinforced Nanocellulose Composite Membranes Mahsuli, Taufiq; Larasati, Aisyah; Aminnudin, Aminnudin; Maulana, Jibril
Journal of Mechanical Engineering Science and Technology (JMEST) Vol 7, No 2 (2023)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um016v7i22023p137

Abstract

Indonesian pineapple production can reach 200 tons per day; however, pineapples generate a significant amount of waste. Pineapple peel waste can be used to make membranes. Composite membranes containing TiO2 have dense properties, low porosity, and increase the mechanical strength of the cellulose sheet. This research uses various ultrasonic homogenizers to homogenize the distribution of nanocellulose and TiO2 (50% and 100% power with 30, 60, and 90 minutes). The casting method is used to shape the membrane. The SEM test shows that the higher the power used and the longer the sonication time, the less agglomeration of about 1.63%/ cm2 and a thickness of 16.56 µm. Identification of X-ray diffraction (XRD) results shows that sonication treatment for too long causes the peak at an angle of 25o to disappear. The analysis revealed no new peaks in the diagram pictures that were found using Fourier Transform Infrared Spectroscopy (FTIR) to analyze the functional groups, but it is known that changes occur in the O-H bonds of cellulose and C=C. The 50% sample with a power of 60 minutes had the lowest roughness value of 1.008 µm. Furthermore, as the power and time on the sample are increased, the roughness increases.
Co-Authors Ahmad Atif Fikri, Ahmad Atif Aisyah Larasati, Aisyah Aminnudin, Aminnudin Fadillah, Faqih Heru Suryanto Ikrom, Muhamad Krisnaputra, Radhian Mahsuli, Taufiq Mandala, Wirawan Widya Masera, Kemal Mito, Mohamed T Nugroho Santoso Setiawan, Widia Winarto, Felixianus Eko Wismo