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All Journal Ganendra: Majalah IPTEK Nuklir Indonesian Journal of Chemistry
Wafda, Hakimul
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Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Other

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SINTESIS PADUAN BARU BAJA OXIDE DISPERSION STRENGTHENED (ODS) FERITIK Fe-Cr-Al-W-Ti-Zr DENGAN DISPERSOID Y2O3 SEBAGAI KANDIDAT MATERIAL CLADDING ELEMEN BAKAR REAKTOR NUKLIR DENGAN METODE MEKANOSINTESIS Wafda, Hakimul; Prajitno, Djoko Hadi; Mustari, Asrili Pramutadi Andi; Roswita, Fahma
GANENDRA Majalah IPTEK Nuklir Volume 26 Nomor 2, 2023
Publisher : Website

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/gnd.2023.6856

Abstract

Bahan struktur merupakan salah satu kunci penting dalam penelitian reaktor nuklir generasi keempat. Sejak peristiwa kecelakaan di pembangkit listrik tenaga nuklir Fukushima–Daiichi, telah terjadi peningkatan pengembangan Accident Tolerant Fuel (ATF) Cladding atau kelongsong bahan bakar toleran kecelakaan untuk menghindari kecelakaan reaktor air ringan. Maka dari itu Inovasi perekayasaan ATF merupakan salah satu kegiatan dalam litbang material maju yang sedang banyak dikembangkan. Kandidat material yang paling menjanjikan untuk ATF cladding adalah Baja yang diperkuat dengan dispersi oksida (ODS). Dalam penelitian ini baja ODS feritik Fe-Cr-Al-W-Ti-Zr-Y2O3 disintesis dengan metode mekanosintesis menggunakan alat planetary ball mill (PBM) dengan variasi komposisi Zr sebesar 0%, 0.5%, 1%, dan 1.5%. Mekanosintesis dilakukan selama 8 jam dengan menggunakan bola stainless steel. Perbandingan berat antara sampel dengan bola adalah 1:10. Kemudian dilakukan karakterisasi menggunakan mikroskop optik, XRD, dan SEM-EDS. Hasil observasi menunjukkan homogenitas yang baik pada bahan hasil sintesis.
High Temperature Oxidation Behavior of ODS Ferritic Stainless Steel Fe-16Cr-4Al-1Ni-0.4Y2O3 Wafda, Hakimul; Prajitno, Djoko Hadi; Basuki, Eddy Agus; Syafiq, Ahmad; Widiawati, Nina; Andi Mustari, Asril Pramutadi
Indonesian Journal of Chemistry Vol 24, No 5 (2024)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ijc.95284

Abstract

This study investigates the isothermic oxidation behavior of the new ODS alloy Fe-16Cr-4Al-1Ni-0.4Y2O3 (% by weight) at 700, 800 and 900 °C, with exposure times of 5, 20, 50, and 100 h at each temperature. The purpose is to obtain new data on its high-temperature parabolic oxidation constant for assessing oxidation resistance. The methods used include isothermal oxidation testing, XRD, SEM-EDS characterization, and analysis of oxidation kinetics by monitoring changes in oxide thickness using microscopy and SEM-EDS. The oxide products formed on the sample surface are Fe2O3, Fe3O4, AlFe2O4, and (Fe,Cr)2O3. Al and Cr oxides are located under the dominant Fe oxide layer on the surface of the sample. The oxidation test results showed that the most protective sample was obtained at a temperature of 700 °C for 100 h with an oxide thickness of 263.99 μm. The kinetics analysis correlates strongly with the parabolic equation (R2 ≈ 1). The oxidation rate constants at temperatures of 700, 800, and 900 °C were 681.76, 2957.5, and 12300 μm2 h−1, respectively. The activation energy required by the oxidation reaction in this alloy is 136.5 kJ mol−1. This research enhances understanding and potential applications of the Fe-16Cr-4Al-1Ni-0.4Y2O3 alloy in high-temperature environments.
Co-Authors Ahmad Syafiq Andi Mustari, Asril Pramutadi Basuki, Eddy Agus Djoko Hadi Prajitno Mustari, Asrili Pramutadi Andi Roswita, Fahma Widiawati, Nina