Jurnal Sains Materi Indonesia
Vol 12, No 2: FEBRUARI 2011

PHASE TRANSITION IN Fe3O4 /Fe2O3 NANOCOMPOSITES BY SINTERING PROCESS

Muhammad Ghufron (Dept. of Physics, Fac. of Math. and Natural Sciences-Sepuluh November Institute of Tech. Surabaya Kampus ITS Sukolilo, Surabaya 60111, Indonesia)
Malik Anjelh Baqiya (Dept. of Physics, Fac. of Math. and Natural Sciences-Sepuluh November Institute of Tech. Surabaya Kampus ITS Sukolilo, Surabaya 60111, Indonesia)
Mashuri Mashuri (Dept. of Physics, Fac. of Math. and Natural Sciences-Sepuluh November Institute of Tech. Surabaya Kampus ITS Sukolilo, Surabaya 60111, Indonesia)
Triwikantoro Triwikantoro (Dept. of Physics, Fac. of Math. and Natural Sciences-Sepuluh November Institute of Tech. Surabaya Kampus ITS Sukolilo, Surabaya 60111, Indonesia)
Darminto Darminto (Dept. of Physics, Fac. of Math. and Natural Sciences-Sepuluh November Institute of Tech. Surabaya Kampus ITS Sukolilo, Surabaya 60111, Indonesia)



Article Info

Publish Date
15 Oct 2018

Abstract

PHASE TRANSITION IN Fe3O4/Fe2O3 NANOCOMPOSITES BY SINTERING PROCESS. Fe3O4 powders have been successfully produced by using coprecipitation method. The characterization using X-Ray Diffraction method resulted in the size of Fe3O4 powders of 9.1 ± 0.3 nm. Samples were then formed into pellete and powders. Heat treatment at temperature 600 oC of powder samples for 1 hour and 2 hours give maghemite and hematite phases, but heat treatment at temperature 700-800 oC for 1 hour, 2 hours and 3 hours give only one phase namely hematite. Heat treatment at temperature 600 oC, 700 oC and 800 oC of pelletes for 1 hour, 2 hours and 3 hours give also only one phase which is hematite. Quantitative analysis using MAUD program resulted in Fe3O4/Fe2O3 composites with changing crystal size at increasing temperature.

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Journal Info

Abbrev

jsmi

Publisher

Subject

Materials Science & Nanotechnology

Description

Jurnal Sains Materi Indonesia (Indonesian Journal of Materials Science), diterbitkan oleh Pusat Teknologi Bahan Industri Nuklir - BATAN. Terbit pertama kali: Oktober 1999, frekuensi terbit: empat ...