Bulletin of Chemical Reaction Engineering & Catalysis
2013: BCREC Volume 8 Issue 1 Year 2013 (June 2013)

Preparation and Characterization of Acid and Alkaline Treated Kaolin Clay

Sachin Kumar (Department of Chemical Engineering, National Institute of Technology, Rourkela-769008)
Achyut Kumar Panda (Department of Chemistry, School of Engineering and Technology, Bhubaneswar Campus, Centurion University of Technology and Management - 752050)
R. K. Singh (Department of Chemical Engineering, National Institute of Technology, Rourkela-769008)



Article Info

Publish Date
30 Jun 2013

Abstract

Kaolin was refluxed with HNO3, HCl, H3PO4, CH3COOH, and NaOH of 3M concentration at 110 °C for 4 hours followed by calcination at 550 °C for 2 hours. The physico-chemical characteristics of resulted leached kaolinite clay were studied by XRF, XRD, FTIR, TGA, DTA, SEM and N2 adsorption techniques. XRF and FTIR study indicate that acid treatment under reflux conditions lead to the removal of the octahedral Al3+ cations along with other impurities. XRD of acid treated clay shows that, the peak intensity was found to decrease. Extent of leaching of Al3+ ions is different for different acid/base treatment. The acid treatment increased the Si/Al ratio, surface area and pore volume of the clay. Thus, the treated kaolin clay can be used as promising adsorbent and catalyst supports. © 2013 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0)

Copyrights © 2013






Journal Info

Abbrev

bcrec

Publisher

Subject

Chemical Engineering, Chemistry & Bioengineering Chemistry

Description

Bulletin of Chemical Reaction Engineering & Catalysis, a reputable international journal, provides a forum for publishing the novel technologies related to the catalyst, catalysis, chemical reactor, kinetics, and chemical reaction engineering. Scientific articles dealing with the following topics in ...