Fisitek : Jurnal Ilmu Fisika dan Teknologi
Vol 2, No 2 (2018)

SYNTHESIS OF RUTILE TIO2 NANOPARTICLES BY CO-PRECIPITATION METHOD

Nazaruddin Nasution (Program Studi Fisika Universitas Islam Negeri Sumatera Utara Medan)
Aida Fitri (Unknown)



Article Info

Publish Date
21 Nov 2018

Abstract

Abstract. The objective of this research is to produce rutile TiO2 nanoparticles by co-precipitation method and to determine its characterization using Scanning Electron Microscopy (SEM), Energy Dispersive X-ray Spectroscopy (EDS), X-ray Diffractometry (XRD), and Particle Size Analysis (PSA) methods. Synthesis of rutile TiO2 nanoparticles by co-precipitation method in this study was initiated by mixing 15% TiCl3 solution into distilled water while stirring at constant speed for some time. Then, pH is adjusted to 11-13 by dripping ammonia (NH4OH) solution while continuing to stir. The precipitate (white gel) is then dried in the oven and crushed to produce TiO2 powder. The morphology of the TiO2 particles obtained is spherical and tends to agglomerate. The average particle size of TiO2 produced is 192.2 nm. The EDS results show that the percentage of Ti mass in TiO2 particles is 59.52%. Based on XRD analysis, there are two phases formed namely anatase and rutile with a tetragonal crystal system.Keywords: Co-precipitation method, nanoparticles, and rutile.

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Journal Info

Abbrev

Fisitek

Publisher

Subject

Computer Science & IT Education Physics

Description

FISITEK: Jurnal Ilmu Fisika dan Teknologi is a peer-reviewed journal which covers all aspects of theoretical and practical research of physics and their use. FISITEK is published by Physics Department of Science and Technology Faculty, State Islamic University of Sumatera Utara Medan (Universitas ...