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Jurnal Akademika Kimia

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Published by Universitas Tadulako

ISSN : 23026030 EISSN : 24775185 DOI : https://doi.org/10.22487/

Core Subject : Science, Education,

Chemistry Education

Jurnal Akademika Kimia is an electronic open-access journal that aims to publish the latest research results in the area of chemistry education and pure chemistry from academicians, professionals, and other practitioners at all levels of chemistry education. The journal coverage includes the following: current trends of professional chemistry education, educational technology, teacher education, educational science, learning assessment, learning models, and development of learning materials, as well as pure chemistry including organic chemistry, inorganic chemistry, analytical chemistry, physical chemistry, biochemistry and other chemistry fields such as environmental chemistry, that emphasis on a broad description of the general methods and processes for the synthesis, modification, and characterization of chemical materials.

Arjuna Subject : Kimia(semua kategori) - Kimia (Lain-Lain)

Articles 10 Documents

Search results for , issue "Vol. 11 No. 1 (2022)" : 10 Documents clear

Analysis of Student’s Creative Thinking Ability on Colloid Material Siti Arma; Supriadi Supriadi
Jurnal Akademika Kimia Vol. 11 No. 1 (2022)
Publisher : Universitas Tadulako

This study aimed to describe students' creative thinking skills in Colloid material in class XI SMA Negeri 7 Palu. The type of this research was descriptive quantitative. The research sample consisted of 30 students. The data collected were in the form of test results for the ability to think creatively, which were obtained through giving essay questions as many as five items that expert validators had validated. The results of every item were on average 74.4% of fluency, while flexibility, elaboration, and originality, respectively, were 75.83%, 53.76%, 61.66%, and 47.5%. Based on the analysis of the four indicators above, it can be found that the students' creative thinking ability on colloid material in class XI SMA Negeri 7 Palu was in the medium category. Students need to be accustomed to working on questions that can require them to think creatively during learning to develop their ability in creative thinking and connect theory with everyday life.

Development of Hollow Fiber Liquid Phase Microextraction Method for Determination of Diazinon Residues in Vegetable Samples Eviomitta R. Amanda; Yanuardi Raharjo; Usreg S. Handajani
Jurnal Akademika Kimia Vol. 11 No. 1 (2022)
Publisher : Universitas Tadulako

An extraction method based on a combination of hollow fiber liquid-phase microextraction with high-performance liquid chromatography diode array detector (HF-LPME HPLC-DAD) has been developed and demonstrated to analyze pesticide residues in vegetables. This study aims to determine the optimum extraction conditions and validation performance of this method. Diazinon pesticide was selected as the target model analyte. HF-LPME is performed by stacking microliter organic solvent droplets through an HPLC syringe coated with polypropylene hollow fiber by directly dipping it into the sample solution and stirring it during the extraction process. Finally, the organic solvent was put into an HPLC syringe at the end of the extraction. Then, it was injected into the HPLC-DAD at the wavelength of 247 nm. Several important extraction parameters have been optimized. The optimization results showed the type of organic solvent of n-hexane, the length of the hollow fiber of 1.5 cm, the volume of the sample solution of 20 mL, and the stirring speed of 600 rpm. The validation performance obtained a limit of detection (LoD) of 0.10 mgL-1, limit of quantification (LoQ) of 0.33 mgL-1, percent recoveries of 99.88%, a coefficient of variation of 3% (n=15), and the enrichment factor of 19,982 times. Under optimal conditions, the developed method was applied to extract diazinon in vegetable matrix samples using the spiking method. Mustard green was selected as a model matrix sample. From the research, the percentage recoveries of diazinon obtained in the mustard green matrix sample are 98.80% - 100.41%.

Flavonoid Compounds of the Catechin from Wungu (Graptophyllum pictum (L.) Griff) Leaves and the Sun Protecting Factor Value Masyita Masyita; Endah Sayekti; Nurlina Nurlina
Jurnal Akademika Kimia Vol. 11 No. 1 (2022)
Publisher : Universitas Tadulako

The flavonoid content in wungu (Graptophyllum pictum (L.) Griff.) leaves has the potential as a sunscreen. The study aims to identify isolates of flavonoid compounds from wungu leaves and determine the SPF value. Steps are followed by extraction, fractionation, phytochemical test, separation by chromatography, identification, and SPF test. Extraction was carried out with methanol, followed by fractionation with n-hexane and dichloromethane. Dichloromethane fraction was chosen to proceed to the separation step because the results of the phytochemical test showed a vigorous color intensity for the content of flavonoids. The isolate (3.6 mg; dark green; amorphous; mp. 132-136 °C) was identified using a UV-Vis spectrophotometer using methanol as a solvent with a shift reagent NaOH, AlCl3, and a mixture of concentrated AlCl3 and HCl. Based on the UV-Vis spectra, the isolate was predicted to be flavonoid compounds belonging to the catechin group, which have a hydroxyl group at positions C-3, C-7, and do not have an ortho-hydroxy group in ring B. The SPF value of the isolate of 2.3244 at 100 ppm was determined in vitro and calculated by the Qian equation. Therefore, isolate was categorized as sunscreens that provided minimal protection

Analysis Redox Reaction on Zinc-Coating Thickness Test in Metal Processing Industry of Small and Medium Enterprises Gatot Triyanto; Ricky R. Saputro; Chepi Reynaldir; Khoirudin Khoirudin; Sukarman Sukarman
Jurnal Akademika Kimia Vol. 11 No. 1 (2022)
Publisher : Universitas Tadulako

This study discusses the implementation of redox reactions on the thickness test of the galvanized (zinc-coated) layer using the JIS-H-0401 standard to help Small and Medium Enterprises (SMEs) industries. Some of the finished products go through the galvanizing process in the metal processing industry. Quality constraints, especially related to the thickness of the galvanic (zinc-coated) layer, have become an object that is less controlled because of the limitations of the test equipment used. This research uses an experimental method applied to one of its products: a flat washer with SPCC material and a thickness of about 2.20 mm. SPCC - SD material is classified as low carbon steel based on its carbon content. 5-unit flat washers were identified with sample codes A, B, C, D, and E. Flat washers have an internal diameter of 22.65 - 22.7 mm. In comparison, the outer diameter is between 43.75 - 43.80. The redox reaction process uses HCl (hydrochloric acid) with a concentration of 1 M, which is diluted with water (H2O). The zinc thickness test results show that the flat washer has an average thickness of 10.52 microns with a minimum and maximum thickness variation of 10.66 -10.72 microns.

The Effect of Surfactants on Separation of Light Rare Earth Metals using Emulsion Liquid Membrane Method: Review Dwi Ratna Setiani; Afifah R. Widianti; Fauzia Salsabila; Anni Anggraeni; Husein H. Bahti; Uji Pratomo
Jurnal Akademika Kimia Vol. 11 No. 1 (2022)
Publisher : Universitas Tadulako

Rare earth metals (REM) are scarce elements and are only found in the form of complex compounds of phosphate and carbonate. REM consists of 17 elements classified into light REM, medium REM, and heavy REM. This article is focused on lightweight REM, which is widely applied in various industrial fields. Many REM applications are increasing the demand for high-purity and bulk REMs. However, REM has almost the same physical and chemical properties, making it difficult to separate. Therefore, the separation of REM is interesting to study with various methods, one of which is Emulsion Liquid Membrane (ELM). ELM is developing a solvent extraction method involving three phases: the external phase, the internal phase, and the membrane phase. The key to the success of ELM lies in the stability of the emulsion, which is very dependent on the type and concentration of surfactants, so in the ELM process, it is necessary to choose the right concentration and type of surfactant. Therefore, this article was made to know the effect of surfactants such as span-80, span-85, and T154 in separating light REM using the ELM method.

Application of Cooperative Learning Jigsaw Model to Improve Student's Learning Achievement in Chemistry Learning Sitti Rahmawati; Detris Poba; Magfirah Magfirah; Kusrini Burase
Jurnal Akademika Kimia Vol. 11 No. 1 (2022)
Publisher : Universitas Tadulako

This study aims to improve student achievement in learning chemistry in class X MIA4 at SMA Negeri 1 Palu by applying the Jigsaw Cooperative Learning Model. The Classroom Action Research (CAR) problem can be formulated as follows: Is the Jigsaw Cooperative Learning Model application able to improve student achievement in learning chemistry in class X MIA4 SMAN 1 Palu? CAR is carried out with the following stages to answer the problem: 1. Planning, 2. Implementation. 3. Observation, and 4. Evaluation and Reflection. The study results can be explained as follows several fundamental aspects of learning were successfully improved by applying the Jigsaw Cooperative Learning Model. Such as student activity in collaboration and in completing worksheets independently, actively asking and answering questions, and making students feel happy and enthusiastic. Likewise, the average evaluation of each cycle showed that the % completeness increased. In cycle one, action one was 73.8%, action two 85.5%, and activity three 92.9% increased in cycle two, the average from three actions to 98.0%. It can be concluded that the application of the Jigsaw Cooperative Learning Model can improve student achievement in class X MIA4 SMA Negeri 1.

Synthesis and Characterization of Activated Carbon from Waste Compedak Fruit (Artocarpus Champeden) Activated H3PO4 as Adsorbent of Methylene Blue Catherina Bijang; Matheis F. J. D. P. Tanasale; Dewi Sri; Tahril Tahril; Thamrin Azis
Jurnal Akademika Kimia Vol. 11 No. 1 (2022)
Publisher : Universitas Tadulako

Synthesis of activated carbon from cempedak peel waste is carried out to utilize biomass waste. This study aimed to synthesize and characterize activated carbon from cempedak peel waste. The synthesis was carried out by chemical activation using phosphoric acid with a dry impregnation ratio of 1:4 (g sample:g H3PO4). Samples impregnated for 24 hours were then heated at 250℃—and then calcined at 350℃ and 450℃. The XRD and FTIR characterization results indicated that the activated carbon obtained had an amorphous structure and the activated carbon obtained had hydroxyl, carbonyl, and carboxylic groups. Activated carbon with the highest yield was obtained at a temperature of 350, namely 43%. The results of determining the water content of activated carbon obtained are 8.36% at 350 0C and 7.1% at 450 ℃. The value of water content and ash content of activated carbon from the skin of this cempedak fruit has met the Indonesian National Standard (SNI 06-3730-1995). The best-activated carbon yield was at a calcination temperature of 450, with the percentage of adsorption efficiency on methylene blue of 98.88%.

Development of Chemistry’s Learning Module Oriented Local Wisdom of Central Sulawesi for High School in Basic Acid Solution Materials Hety E. Panambulo; Ratman Ratman; Nurida Nurida
Jurnal Akademika Kimia Vol. 11 No. 1 (2022)
Publisher : Universitas Tadulako

Development research has been carried out to produce a high school chemistry learning module that oriented Central Sulawesi’s local wisdom in acid-base solutions. This research was conducted using research and development (R&D) methods. The goal of this study was to ascertain the validity and applicability of the developed learning modules. Development of the learning module is expected to be used by teachers as users and for students in their independent learning, increasing the understanding of concepts and getting to know local wisdom in the Central Sulawesi region. The validity of the learning module was determined by a validation test conducted by specialists in the topic, medium, and user. In contrast, the practicality of the learning module was determined by the outcomes of the module's implementation by students. The validation results showed that the average score of the material expert of 2,66 was categorized as “valid,” the average score of the media expert was 3,29 with the category “valid,” and the average score of the user was 3,53 with the category “valid.” The results implementation of learning modules using students' response questionnaires obtained respectively, a percentage of 29% of students responded was “very practical,” 64,4% of students responded war “practical,” 6% of students responded was “impractical,” and 0% of students respond was “very impractical.” Based on these results, it can be concluded that the development module was “valid” and “practical” in using the learning process.

Application of CORE Learning Model with Molymod-Assisted on Hydrocarbon Material to Improve the Students’ Learning Outcomes Gleryl F. Novemly; Mery Napitupulu; Ijirana Ijirana
Jurnal Akademika Kimia Vol. 11 No. 1 (2022)
Publisher : Universitas Tadulako

This study aimed to describe the improvement of learning outcomes by applying the learning model of Connecting, Organizing, Reflecting, Extending (CORE) with molymod-assisted hydrocarbon material of class X students of SMA Labschool UNTAD Palu. This type of research was experimental designs with one group pretest-posttest design. This study used 2 classes, namely class XA as replication class 1 (n = 26) and class XB as replication class 2 (n = 27). The students' learning outcomes were affective, psychomotor, and cognitive aspects. In replication class 1, the value of student learning outcomes was 71.37, while in replication class 2 was 66.00. The data analysis results showed increased student learning outcomes after using the Molymod-assisted CORE learning model in both classes. So it can be concluded that applying the Molymod-assisted CORE learning model on hydrocarbon materials can improve student learning outcomes for class X SMA LABSCHOOL UNTAD Palu.

Antioxidant Activity Test of Ethanol Extract of Ripe and Young Cocoa Pods (Theobroma Cacao L.) Andriana Andriana; Minarni R. Jura
Jurnal Akademika Kimia Vol. 11 No. 1 (2022)
Publisher : Universitas Tadulako

Antioxidant activity test of Ethanol Extract of Ripe and Young Cocoa Pod Skin (Theobroma Cacao L.) with DPPH (1,1-diphenyl-2-picrylhydrazyl) using UV-Vis spectrophotometer has been carried out. This study aimed to determine the IC50 value of the ethanol extract of ripe cocoa pods and young cocoa pods (Theobroma Cacao L.). The mature and young cocoa pods were extracted using absolute ethanol solvent and tested for their antioxidant activity using DPPH (1,1-diphenyl-2-picrylhydrazyl). The concentration variations used in the ethanol extract of ripe cocoa pods and young cocoa (Theobroma Cacao L.) were 20 ppm, 40 ppm, 60 ppm, and 80 ppm. The results showed that the IC50 values of the ethanol extract of ripe and young cocoa pods were 76.094 ppm and 91.884 ppm, respectively. Meanwhile, the IC50 value of vitamin C compared was 63.519 ppm. Based on the IC50 value data above, it can be seen that the antioxidant activity of the ethanol extract of young cocoa pods and ripe cocoa pods are potent antioxidants.

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Daud K. Walanda

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walanda@gmail.com

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+6281245207927

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jak.untad@gmail.com

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Program Studi Pendidikan Kimia-FKIP Universitas Tadulako Jl. Soekarno-Hatta Km.9, Palu-Indonesia 94119

Location
Kota palu,

Sulawesi tengah

INDONESIA

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Home Page

OAI Link

Editorial Team

Contact

Reviewer

Google Scholar

Contact Name Daud K. Walanda

Contact Email walanda@gmail.com

Phone +6281245207927

Journal Mail Official jak.untad@gmail.com

Editorial Address Program Studi Pendidikan Kimia-FKIP Universitas Tadulako Jl. Soekarno-Hatta Km.9, Palu-Indonesia 94119

Location Kota palu, Sulawesi tengah INDONESIA

Abstract

Abstract

Abstract

Abstract

Abstract

Abstract

Abstract

Abstract

Abstract

Abstract

Contact Name
Daud K. Walanda

Contact Email
walanda@gmail.com

Phone
+6281245207927

Journal Mail Official
jak.untad@gmail.com

Editorial Address
Program Studi Pendidikan Kimia-FKIP Universitas Tadulako Jl. Soekarno-Hatta Km.9, Palu-Indonesia 94119

Location
Kota palu,

Sulawesi tengah

INDONESIA