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Aminnudin, Aminnudin
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Energy Engineering Industrial & Manufacturing Engineering Materials Science & Nanotechnology Mechanical Engineering

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Effect of Addition Titanium Dioxide Nanoparticle on Properties of Pineapple Leaf Fiber Mediated TEMPO Oxidation Oxidation Ikrom, Muhamad; Suryanto, Heru; Fikri, Ahmad Atif; Aminnudin, Aminnudin; Maulana, Jibril; Fadillah, Faqih; Mito, Mohamed T; Masera, Kemal
Journal of Mechanical Engineering Science and Technology (JMEST) Vol 8, No 1 (2024)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um0168i12024p082

Abstract

Indonesia is an agricultural country with the potential to grow many plants as natural fiber sources. In order to improve its properties, natural fiber needs to be treated by applying nanomaterial so that it can compete with the characteristics of synthetic fibers. The study aims to determine the influence of adding titanium dioxide (TiO2) nanoparticles on pineapple leaf fiber (PALF) characteristics. The PALF was collected from the Subang plantation (Indonesia). The chemical treatment was carried out with pre-treatment using an alkalization process for 3 hours, and the oxidation process was carried out with TEMPO. TiO2 nanoparticle grafting was carried out by adding a silane solution with a ratio of 1:10 with alcohol. The characteristics of PALF were observed using XRD, FTIR, SEM, and tensile tests. The results show that the crystallinity of the PALF increased after TEMPO treatment. PALF form Si-O-C bond identified at a wavelength of 1158 cm-1 after silane treatment. Ti – O – Si functional groups were identified in the 660 cm-1 – 670 cm-1 wavelength range. In the fiber surface, agglomerated TiO2 nanoparticles are formed and increase with increasing TiO2 nanoparticle concentration. The tensile stress of treated PALF is increased by 125%, with the highest tensile strength of 1279.18 MPa, obtained by TiO2 nanoparticle concentration of 1.0%.
Effect of Grafting Nano-TiO2 on Sansevieria cylindrica Fiber Properties Wiguna, Chrisrulita Sekaradi; Suryanto, Heru; Aminnudin, Aminnudin; Binoj, Joseph Selvi; Ali, Alamry
Journal of Mechanical Engineering Science and Technology (JMEST) Vol 7, No 1 (2023)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um016v7i12023010

Abstract

Natural fibers, which are abundant, environmentally friendly, and biodegradable, are used as a replacement for synthetic fibers. The composite strength can be increased by treating the surfaces of natural fibers with suitable chemicals, which can also improve the interface interaction between fiber and matrix. Application of a coupling agent in chemical treatment is utilized to reinforce the bonding between fiber and matrix. The objective of the study is to determine the influence of silane concentration on the Sansevieria cylindrica fiber properties. The methods included fibers treatment using ethanol and coupling agent as dissolving and TiO2 with concentrations of 0 percent, 0.25 percent, 0.5 percent, 0.75 percent, and 1 percent. The mechanical strength testing was conducted through a single fiber test. Fiber morphology was observed using an electron microscope. FTIR analyzes the change in fiber chemical composition caused by TiO2 addition. As a result, the morphology of S. cylindrica fibers became rougher and showed a rougher surface after a silane concentration of 1 percent, but with the proper concentration, some fiber surfaces provided a good interface. Ti-O bonds are formed at a wavelength of 475 cm-1. The shift in a peak at 400–500 cm-1 indicates Ti-O-Ti group stretching vibrations believed to have originated from TiO2 particles. The mechanical strength increases as the concentration of TiO2 increases, with the highest fiber strength of 284.66 MPa observed at a TiO2 concentration of 1 percent. This represents a 26 percent higher tensile strength compared to the control specimen.
Characterization of Bacterial Nanocellulose - Graphite Nanoplatelets Composite Films Susilo, Bili Darnanto; Suryanto, Heru; Aminnudin, Aminnudin
Journal of Mechanical Engineering Science and Technology (JMEST) Vol 5, No 2 (2021)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um016v5i22021p145

Abstract

Bacterial cellulose  (BC) was synthesized from pineapple peel extract media with addition of fermentation agent bacteria Acetobacter xylinum. BC was disintegrated from the pellicle into bacterial nanocellulose (BNC) by using a high-pressure homogenizer (hph) machine, which has a three-dimensional woven nanofibrous network. The synthesis of composite films started when BNC, graphite nanoplatelets, and cetyltrimethylammonium bromide (CTAB) were homogenized using an ultrasonic homogenizer then baked on a glass mold at a temperature of 80 degrees Celcius for 14h. A scanning electron microscope (SEM) was used to analyze its morphology. X-Ray diffraction spectra were used to analyze the composite films structure. The functional groups of the composite films were analyzed using the FTIR spectrum. SEM micrograph shows that GNP was evenly distributed into BNC matrix after CTAB addition. GNPs are shown as flat and smooth flakes with sharp corners. Some peak corresponds O-H, C-H, C≡C, and CH3 stretching was identified by using FTIR spectroscopy at wavenumber 3379, 2893, 2135, and 1340 cm-1, respectively. XRD analysis shows that Crystalline Index (C.I) of BNC increases after 2.5 wt% addition of GNP. The presence of CTAB decreases C.I value of composite films. BNC/GNP composite films have the best mechanical properties with Young’s modulus about 77.01 ± 8.564.
Effect of Graphene Addition on Bacterial Cellulose-Based Nanocomposite Maulana, Jibril; Suryanto, Heru; Aminnudin, Aminnudin
Journal of Mechanical Engineering Science and Technology (JMEST) Vol 6, No 2 (2022)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um016v6i22022p107

Abstract

Bacterial cellulose (BC) is a widespread, low-cost biopolymer that has generally been produced from plants and biomass waste. A method for improving the range of applications for bacterial cellulose is adding graphene material. It has an outstanding feature that can increase the performance of nanocomposite materials. The research aims to observe the effect of graphene on the surface morphology, crystallinity, chemical bonding, and tensile strength of BC/CuO nanocomposite. For this study's synthesis, BC was synthesized by fermenting pineapple peel extract for 10 to 14 days. The produced BC was crushed, homogenized with a nano homogenizer machine, and filtered. Filtered BC, CuO, and graphene were added to obtain a solution, and the mixture was first stirred magnetically, followed by an ultrasonic homogenizer, and finally dried using a freeze-dry method to make a porous nanocomposite. According to SEM analysis, the addition of CuO and graphene can fill porosity nanocomposite. By XRD analysis, the addition of graphene reduces the crystallinity of BC/CuO. The FTIR data showed that adding graphene reduces hydrogen bonding and makes some Cu-O-C bonding. The tensile test has demonstrated that the tensile strength of BC-based nanocomposite with graphene reinforcement tends to decrease.
Analysis of Structure and Functional Group of Filament Product-Based PLA/Nanographite Nanocomposite Suryanto, Heru; Aminnudin, Aminnudin; Bintara, Redyarsa Dharma; Putra, Abyan Farras; Nashrullah, Fikri Munif; Binoj, Joseph Selvi; Panicker, Nithin
Journal of Mechanical Engineering Science and Technology (JMEST) Vol 7, No 2 (2023)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um016v7i22023p129

Abstract

In many polymer compounds, Polylactic Acid (PLA) is a polyalcohol material that has the most potential material which is potent for biological degradation. They have been applied as filaments in additive manufacturing. The PLA properties can be modified by adding nanomaterials such as graphite nanoplatelets. This study aims to obtain the characteristics of PLA-based filament nanocomposite with nanographite reinforcement. Methods include exploration research to obtain nanocomposite filament with PLA and 1% of nanographite. The mixing process of nanographite in PLA solution with chloroform solvent and then the extrusion process of nanocomposite using a single extruder. The product comparison before and after the extrusion process was analyzed using X-ray diffraction and Fourier Transform infrared. Diffractogram results indicate that the original PLA structure is amorphous, and after mixing using nanographite, peaks of nanographite appeared clearly. After the extrusion process, some peaks at 16.7° and 19.1° disappeared, but only a peak 26.6° appeared in the diffractogram. Extrusion makes the structure change. Functional group analysis confirms that some reactions occurred so that many peaks were removed, and several new peaks were observed. It indicates that the extrusion process of PLA/nanographite results in different structures and functional groups that indicate a change in its properties.
Effect of the Homogenization Process on Titanium Oxide-Reinforced Nanocellulose Composite Membranes Mahsuli, Taufiq; Larasati, Aisyah; Aminnudin, Aminnudin; Maulana, Jibril
Journal of Mechanical Engineering Science and Technology (JMEST) Vol 7, No 2 (2023)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um016v7i22023p137

Abstract

Indonesian pineapple production can reach 200 tons per day; however, pineapples generate a significant amount of waste. Pineapple peel waste can be used to make membranes. Composite membranes containing TiO2 have dense properties, low porosity, and increase the mechanical strength of the cellulose sheet. This research uses various ultrasonic homogenizers to homogenize the distribution of nanocellulose and TiO2 (50% and 100% power with 30, 60, and 90 minutes). The casting method is used to shape the membrane. The SEM test shows that the higher the power used and the longer the sonication time, the less agglomeration of about 1.63%/ cm2 and a thickness of 16.56 µm. Identification of X-ray diffraction (XRD) results shows that sonication treatment for too long causes the peak at an angle of 25o to disappear. The analysis revealed no new peaks in the diagram pictures that were found using Fourier Transform Infrared Spectroscopy (FTIR) to analyze the functional groups, but it is known that changes occur in the O-H bonds of cellulose and C=C. The 50% sample with a power of 60 minutes had the lowest roughness value of 1.008 µm. Furthermore, as the power and time on the sample are increased, the roughness increases.
The Effect of Heat Treatment to the Erosion Rate of Brass Composite Aminnudin, Aminnudin; Solichin, Solichin
Journal of Mechanical Engineering Science and Technology (JMEST) Vol 4, No 1 (2020)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um016v4i12020p037

Abstract

Brass composites can be improved their mechanical properties by the heat treatment process. The improvement of the mechanical properties of this technique is expected to increase the resistance of the composite to erosion that occurs in the environment of flow water. Brass composites used are composites with fly ash 5, 10, 15 and 20%. The heat treatment process was carried out using an electric furnace without protective gas. Composite heat up to 350°C and 400°C for 30 min. and quenching with water. Before and after the erosion test, the weight of the test specimen was weighed with analytical scales. The treatment process affects the tensile strength of brass composites. The heat treatment process of brass composites with 5% fly ash at 350 °C produces the highest tensile strength. Erosion rate testing on brass composites showed the lowest erosion rate occurred on brass composites with 5% fly ash and heat treatment at 350°C.
Co-Authors Ahmad Atif Fikri, Ahmad Atif Aisyah Larasati, Aisyah Ali, Alamry Binoj, Joseph Selvi Fadillah, Faqih Heru Suryanto Ikrom, Muhamad Mahsuli, Taufiq Masera, Kemal Maulana, Jibril Mito, Mohamed T Nashrullah, Fikri Munif Panicker, Nithin Putra, Abyan Farras Redyarsa Dharma Bintara Solichin Solichin Susilo, Bili Darnanto Wiguna, Chrisrulita Sekaradi