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All Journal IPTEK The Journal for Technology and Science
Ahnaf, Ahnaf
Departemen Kimia Institut Teknologi Sepuluh Nopember
Computer Science & IT

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Synthesis and Characterization of Zeolitic Imidazolate Framework-8 (ZIF-8)/Al2O3 Composite Aulia, Wulan; Ahnaf, Ahnaf; Irianto, Mochammad Yusuf; Ediati, Ratna; Iqbal, Rendy Muhamad; Rachman, Rahadian Abdul; Martia, Ulva Tri Ita
IPTEK The Journal for Technology and Science Vol 31, No 1 (2020)
Publisher : IPTEK, LPPM, Institut Teknologi Sepuluh Nopember

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (929.525 KB) | DOI: 10.12962/j20882033.v31i1.5511

Abstract

Metal-organic framework (MOF) such as ZIF-8 is the tremendous porous material applied in many fields due to high specific surface area and excellent regularity of pores. One technique to improve the physical properties of ZIF-8 with the formation of a composite between a metal oxide and MOF. ZIF-8 and ZIF-8/Al2O3 were successfully synthesized by the solvothermal method with an Al variation of 19%, 38%, and 76%. The ZIF-8/Al2O3 were characterized by XRD, FTIR, SEM, and N2 Physisorption. The diffractogram shows that the appearing of ZIF-8’s peak on 2θ = 7.26; 10.41, 12.66, 16.41, and 17.95°. The morphological of ZIF-8 crystals had a cubic shape. Then the ZIF-8/Al2O3 had different shapes with ZIF-8. Based on the FTIR result, the Zn-N peak appears on 420 cm−1, which indicates the bonding between metal and organic ligand for ZIF-8/Al2O3 has an additional spike on 825 cm−1 due to the vibration of Al−O− Al.
Co-Authors Aulia, Wulan Iqbal, Rendy Muhamad Irianto, Mochammad Yusuf Martia, Ulva Tri Ita Rachman, Rahadian Abdul Ratna Ediati