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Yulinda Lestari
Pusat Penelitian Metalurgi dan Material - LIPI
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STUDI PENGARUH VARIASI SUHU PERLAKUAN PANAS TERHADAP STRUKTURMIKRO DAN KOROSIFITAS PADA PELAPISAN SS 410 MENGGUNAKAN KOMPOSIT Ni-P-NANO PARTIKEL Al2O3 Yulinda Lestari; Efendi Mabruri; Anne Zulfia Syahrial
Jurnal Sains Materi Indonesia Vol 18, No 3: APRIL 2017
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2017.18.3.4114

Abstract

Pelapisan material Stainless Steel 410 dengan komposit Ni-P-nano powder Al2O3 menggunakan metode electroless kodeposisi sangat tergantung pada tingkat penggabungan lapisan komposit tersebut antara matriks Ni-P dan penguat nano partikel Al2O3 Hal ini berpengaruh pada keunggulan sifat lapisan komposit seperti ketahanan korosi yang baik, laju deposisi yang cepat, keseragaman deposit yang dihasilkan dan ketahanan kimia yang baik. Pada penelitian ini, parameter yang divariasi adalah suhu perlakuan panas setelah proses electroless kodeposisi. Penelitian ini bertujuan untuk mengetahui fenomena strukturmikro, fasa dan kristalinitas, komposisi kimia dan distribusi unsur di permukaan coating, dan ketahanan korosi komposit coating Ni-P-nano partikel powder Al2O3. Substrat yang digunakan yaitu Stainless Steel 410 di-pretreatment untuk mengaktivasi permukaan, kemudian direndam dalam larutan yang terdiri dari nikel sulfat, natrium hypophosphite, ammonium sulfat, sodium asetat, lead asetat dan serbuk nano alumina. Substrat direndam selama 60 menit, dalam suhu proses 90±2 oC dengan kecepatan putaran 150 rpm. Karakterisasi sampel dilakukan menggunakan alat SEM-EDS, XRD, dan CMS. Dari hasil percobaan menunjukkan terdapat perbedaan visual permukaan substrat antara logam dasar, setelah proses electroless coating dan setelah perlakuan panas. Berdasarkan variabel percobaan, untuk suhu perlakuan panas yang optimum adalah 400 oC, dimana terbentuk strukturmikro dari nodular menjadi butiran yang lebih teratur dan merata serta memiliki ketahanan korosi yang paling baik.
EFFECT OF NICKEL PULSED ELECTRODEPOSITION PARAMETERS ON DEPOSIT MICROSTRUCTURE AND CORROTION RATE AISI 410 Agnes Stephani; Soesaptri Oediyani; Yulinda Lestari; Efendi Mabruri
Widyariset Vol 4, No 2 (2018): Widyariset
Publisher : Pusbindiklat - LIPI

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (776.158 KB) | DOI: 10.14203/widyariset.4.2.2018.143-152

Abstract

Nickel pulse electrodeposition is one of the coating methods that used to increase the corrosion resistance and improve the mechanical properties. In this study, nickel was used as the anode and martensitic stainless steel 410 was used as the cathode. The solution used in the method of nickel pulse electrodeposition include nickel sulfate, nickel chloride, and boric acid. Pulse electrodeposition parameters are variation of duty cycle of 70, 80, 90% and frequency variations valued at 0.1, 1, 10, and 20 kHz. Temperatures used in research nickel pulse electrodeposition at 50 ° C, with a current density of 15 A / dm² and 18 minutes. The Scanning Electron Microscopy analysis determine the microstructure and grain size changes after a nickel pulse electrodeposition. The polarization test determine optimum rate of corrosion when 90 % duty cycle and 20 kHz frequency.
EFFECT OF NICKEL PULSED ELECTRODEPOSITION PARAMETERS ON DEPOSIT MICROSTRUCTURE AND CORROTION RATE AISI 410 Agnes Stephani; Soesaptri Oediyani; Yulinda Lestari; Efendi Mabruri
Widyariset Vol 4, No 2 (2018): Widyariset
Publisher : Pusbindiklat - LIPI

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14203/widyariset.4.2.2018.143-152

Abstract

Nickel pulse electrodeposition is one of the coating methods that used to increase the corrosion resistance and improve the mechanical properties. In this study, nickel was used as the anode and martensitic stainless steel 410 was used as the cathode. The solution used in the method of nickel pulse electrodeposition include nickel sulfate, nickel chloride, and boric acid. Pulse electrodeposition parameters are variation of duty cycle of 70, 80, 90% and frequency variations valued at 0.1, 1, 10, and 20 kHz. Temperatures used in research nickel pulse electrodeposition at 50 ° C, with a current density of 15 A / dm² and 18 minutes. The Scanning Electron Microscopy analysis determine the microstructure and grain size changes after a nickel pulse electrodeposition. The polarization test determine optimum rate of corrosion when 90 % duty cycle and 20 kHz frequency.
Studi Pelapisan Komposit Ni-P-Nano Al2O3 Dengan Metode Electroless Co-Deposition [Study of Ni-P-Nano Al2O3 Composite Coating With Electroless Co-Deposition Methode] Yulinda Lestari; Effendi Mabruri; Anne Zulfia Syahrial
Metalurgi Vol 31, No 1 (2016): Metalurgi Vol. 31 No. 1 April 2016
Publisher : National Research and Innovation Agency (BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1358.178 KB) | DOI: 10.14203/metalurgi.v31i1.96

Abstract

The Ni-P-nano powder Al2O3 composite coating have been prepared by electroless codeposition method. It has advantage that the process does not require an electrode, fast deposition rate, good corrosion and wear resistance. In this study, the variable parameters are the addition of nano powder Al2O3 composition. The aim of this research is to determine microstructure phenomenon, phase and crystalinity, chemical composition and distribution on coating surface, and corrosivity Ni-P-nano powder Al2O3 composite coating.The substrate is used stainless steel 410. Substrates have been pre treated in order to activate the surface. Then, substrate immersed in solution that consisting of nickel sulfate, sodium hypophosphite, ammonium sulfate, sodium acetate, lead acetate and nano alumina powder. The substrate is immersed about 60 minutes at a 90±2 °C temperature with speed of 150 rpm. Sample characterization has done by SEM-EDS, XRD, and CMS. Results indicate there is a microstructure visual difference before and after electroless coating process.Based on variable experiment, the optimum nanopowder Al2O3 compositionis 10 gr/l which have given the best paticle distribution and most excellent corrosion resistance.AbstrakPelapisan material dengan komposit Ni-P-nano powder Al2O3 yang menggunakan metode electroless kodeposisi memiliki keunggulan yaitu prosesnya tidak membutuhkan elektroda, laju deposisi yang cepat danmemiliki ketahanan korosi dan ketahanan aus yang baik. Pada penelitian ini, parameter yang divariasikan adalah komposisi penambahan nano powder Al2O3. Penelitian ini bertujuan untuk mengetahui fenomena struktur mikro, fasa dan kristalinitas, komposisi kimia dan distribusi unsur di permukaan coating, danketahanan korosi komposit coating Ni-P-nano powder Al2O3. Substrat yang digunakan yaitu baja tahan karat 410 dilaku awal (pretreatment) untuk mengaktivasi permukaan, kemudian direndam dalam larutan yang terdiri dari nikel sulfat, natrium hypophosphite, ammonium sulfat, sodium asetat, lead asetat dan serbuk nano alumina. Substrat direndam selama 60 menit, dalam suhu proses 90±2 °C dengan kecepatan putaran 150 rpm. Karakterisasi sampel dilakukan menggunakan alat SEM-EDS (scanning electron microscopy-energy dispersive spectroscopy), XRD (x-ray diffraction), dan CMS (corrosion measurement system). Dari hasil percobaan menunjukkan terdapat perbedaan struktur mikro antara substrat logam dasar dan substrat setelahproses electroless coating. Berdasarkan variabel percobaan, untuk komposisi nano powder Al2O3 yang optimum adalah 10 gr/l karena memberikan distribusi partikel dan ketahanan korosi yang paling baik.
Pengaruh Rapat Arus dan Waktu Pelapisan Nikel pada AISI 410 dengan Metode Pulse Electrodeposition terhadap Strukturmikro dan Laju Korosi [The Influences of Current Density and Time on Microstructure and Corrosion Rate Nickel Coating in Aisi 410 by Pulse Electro Deposition Method] Rivaldo Ramadhana Saputra; Soesaptri Oediyani; Yulinda Lestari; Efendi Mabruri
Metalurgi Vol 32, No 2 (2017): Metalurgi Vol. 32 No. 2 Agustus 2017
Publisher : National Research and Innovation Agency (BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (312.31 KB) | DOI: 10.14203/metalurgi.v32i2.224

Abstract

Nickel plating process with pulse methods in AISI 410 electrodepostion has been done to reduce corrosion rate of this material in industrial applications i.e turbine blade that is often experienced corrosion problems. The coating process using nickel sulfate 250 g / l, boric acid 50 g / l and nickel chloride 45 g / l at temperature of 50-60 ° C with various of current densities for 10, 15, 20 and 25 A / dm² and time for coating process of 10, 15 and 20 minutes. Duty cylce used was 80% and the pulse frequency approximately around 100 Hz. Microstructure examined by using SEM-EDS (scanning electron microscopy-energy dispersive spectroscopy) to observe grain size and thickness of the nickel layer. Corrosion rate measured by using CMS (corrosion measurement system).  The results showed that increasing of current density and coating process would reduce grain size and corrosion rate in coating area. The corrosion rate is 0.00027 mmpy when the current density is 25 A / dm² and plating time is 20 minutes. AbstrakProses pelapisan nikel dengan metode pulse electrodepostion pada AISI 410 dilakukan untuk menurunkan laju korosi AISI 410 pada aplikasi industri, yaitu turbin blade yang sering mengalami masalah korosi. Proses pelapisan menggunakan larutan nickel sulphate 250 g/l, boric acid 50 g/l dan nickel chloride 45 g/l pada temperatur 50 – 60°C dengan variasi rapat arus 10, 15, 20 dan 25 A/dm² dan lamanya proses pelapisan 10, 15 dan 20 menit. Duty cylce yang digunakan adalah 80% dan frekuensi pulse 100 Hz. Pengujian struktur mikro dilakukan menggunakan SEM-EDAX untuk melihat ukuran butir dan ketebalan lapisan nikel yang terbentuk. Pengujian laju korosi dilakukan menggunakan alat CMS. Hasil penelitian menunjukkan bahwa semakin besar rapat arus dan semakin lama proses pelapisan maka ukuran butir yang tergambarkan dalam mikrostruktur lapisan semakin kecil dan laju korosi yang terukur semakin kecil. Laju korosi paling kecil adalah 0,00027 mmpy pada rapat arus 25 A/dm² dan waktu pelapisan 20 menit.
Co-Authors Agnes Stephani Anne Zulfia Efendi Mabruri Effendi Mabruri Rivaldo Ramadhana Saputra Soesaptri Oediyani