Article Per Year (5 Year)
p-Index From 2019 - 2024
0
P-Index
This Author published in this journals
All Journal The Journal of Pure and Applied Chemistry Research
Fika Anjana
Department of Chemical Engineering, Institute Technology Sepuluh Nopember, Surabaya
Chemical Engineering, Chemistry & Bioengineering Chemistry Materials Science & Nanotechnology Medicine & Pharmacology

Published : 1 Documents Claim Missing Document
Claim Missing Document
Check
Articles

Found 1 Documents
Search

 1 
Temperature Effect of Crystalinity in Cellulose Nanocrystal from Oil Palm Empty Fruit Bunch (OPEFB) using Sonication-Hydrothermal Methods Zulnazri Zulnazri; Fika Anjana; Achmad Roesyadi
The Journal of Pure and Applied Chemistry Research Vol 6, No 1 (2017): Edition of January - April 2017
Publisher : Chemistry Department, The University of Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (925.99 KB) | DOI: 10.21776/ub.jpacr.2017.006.01.296

Abstract

Production of cellulose nanocrystals (CNCs) from cellulose of oil palm empty fruit bunches (OPEFB) have been done. The delignification of OPEFB was mixed with 17,5% NaOH and carried out in the three-neck flask with refluxed for 2 hour at 80oC. Further the suspension was bleached with NaOCl 2% for 1 hour at 70oC. Then, to produce CNCs, Cellulose was firstly sonicated for 30 minutes at 40oC. After that cellulose was hydrolized at hydrothermal reactor for 0,1,2,3,4,5, hours at 110 and 120oC respectively. After filtration and washing, CNCs was analyzed by X-Ray Diffraction and the result shows that the grade of the highest CNCs crystalinity at consentration of HCL 2 M at a temperature of 110oC with reaction time of 2 hours is equal to 75.87%.  It can be concluded that sonication-hydrothermal can increase the grade of crystalinity of cellulose nanocrystal.
Co-Authors Achmad Roesyadi Zulnazri Zulnazri