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All Journal Jurnal Penelitian Pendidikan IPA (JPPIPA) Jurnal Pijar MIPA
Dedy Suhendra
University of Mataram
Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Education Materials Science & Nanotechnology Mathematics Physics

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Optimasi Sintesis Asam Lemak Etanolamida Berbasis Minyak Ketapang Menggunakan Response Surface Methodology Lilik Indriani; Erin Ryantin Gunawan; Dedy Suhendra
Jurnal Pijar Mipa Vol. 16 No. 2 (2021): Maret 2021
Publisher : Department of Mathematics and Science Education, Faculty of Teacher Training and Education, University of Mataram. Jurnal Pijar MIPA colaborates with Perkumpulan Pendidik IPA Indonesia Wilayah Nusa Tenggara Barat

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (15.812 KB) | DOI: 10.29303/jpm.v16i2.2265

Abstract

Telah dilakukan optimasi sintesis asam lemak etanolamida berbasis minyak ketapang (Terminalia catappa L) menggunakan Response Surface Methodology (RSM). Asam lemak etanolamida adalah surfaktan yang banyak dibutuhkan pada industri farmasi. Sintesis asam lemak etanolamida dilakukan dengan mereaksikan minyak ketapang dan etanolamina sebagai substrat menggunakan katalis Lipozyme TL.IM. Penelitian ini bertujuan untuk mengamati interaksi antar variabel yang dapat mempengaruhi kondisi optimum dan hasil reaksi. Beberapa variabel yang dimaksud yaitu waktu reaksi, suhu reaksi, molar rasio substrat dan jumlah enzim. Metode RSM yang digunakan terdapat dalam perangkat lunak Design Expert v.7. Hasil penelitian menunjukkan model untuk mendapatkan kondisi yang optimal adalah model quadratic (p-value 0.0048/signifikan), lack of fit (p-value 0.3827 /non signifikan) dan nilai R-squared sebesar 0,7953. Kondisi optimum yang dihasilkan yaitu waktu reaksi 1,50 jam, suhu reaksi 38,10 °C, molar ratio minyak : etanolamina (1 : 20,52) gram/mol dan jumlah enzim 0.16 gram dengan prediksi dan aktual persen hasil asam lemak etanolamida secara berturut-turut sebesar 60,02 dan 64,00 %.
Utilization Of Moringa Seed Oil Fatty Acids for Azelaic Acid Base Stock Production Sri Seno Handayani; Erin Ryantin Gunawan; Dedy Suhendra; Murniati Murniati; Dhony Hermanto; Liliek Karnila
Jurnal Penelitian Pendidikan IPA Vol. 8 No. 5 (2022): November
Publisher : Postgraduate, University of Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/jppipa.v8i5.1964

Abstract

Moringa (Moringa oleifera L.) is a plant belonging to the moringaceae family. Moringa seeds contain oil which can be used as a raw material for making azelaic acid. Azelaic acid is used as an anti-acne in the pharmaceutical and cosmetic industries. Azelaic acid can be obtained from the oxidation process of fatty acids in moringa seed oil using potassium permanganate as an oxidizing agent. The resulting azelaic acid is in the form of white crystals with a conversion percentage of 72.17%. The results of the FT-IR characterization showed the formation of azelaic acid characterized by widening of the hydroxyl group at 3448.46 cm-1 followed by a shift of the ester group at absorption of 1633.46 cm-1. The ester bond is strengthened at a wavelength of 1115.95 cm-1.
Co-Authors Dhony Hermanto Erin Ryantin Gunawan Liliek Karnila Lilik Indriani Murniati Murniati Sri Seno Handayani