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All Journal Journal of Engineering and Technological Sciences Jurnal Ilmiah Arena Tekstil Padjadjaran Journal of Dentistry Mesin
Bambang Sunendar
Advance Material Processing, Teknik Fisika Institut Teknologi Bandung
Biochemistry, Genetics & Molecular Biology Dentistry Engineering Health Professions Immunology & microbiology Industrial & Manufacturing Engineering Mechanical Engineering Medicine & Pharmacology Public Health

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On the Development of a Nomogram for Alkali Activated Fly Ash Material (AAFAM) Mixtures Simatupang, Partogi H.; Imran, Iswandi; Pane, Ivindra; Sunendar, Bambang
Journal of Engineering and Technological Sciences Vol 47, No 3 (2015)
Publisher : ITB Journal Publisher, LPPM ITB

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (821.159 KB) | DOI: 10.5614/j.eng.technol.sci.2015.47.3.1

Abstract

Alkali activated fly ash material (AAFAM) has become the most promising material to substitute materials based on ordinary Portland cement (OPC). However, there is no available nomogram for AAFAM mixtures. In contrast, there are many rational methods available in the literature to make paste, mortar and concrete with OPC based materials, such as Monteiro-Helene’s nomogram, which uses Abram’s law, Lyse’s law and Molinari’s law. This paper presents a study to construct such a nomogram for AAFAM mixtures by first conducting experiments on the  paste and mortar phases. The procedure of Monteiro-Helene’s nomogram was adopted in this formulation. The first step in this direction was to find a close relationship between the strength and paste composition of the material that can be used as a substitute for Abram’s law. The second step  was  to construct the equivalent  of  Lyse’s and Molinari’s relationships by varying the sand and fly ash contents. The results show that it is possible to make a nomogram for AAFAM mixtures such as the one for OPC based materials. Class F fly ash and its mortar phase were used to construct the nomogram. In addition, the  mortar  samples  that were  used to build the nomogram had similar solidification products according to their microscopic characteristics.
PENGGUNAAN TiO2 PARTIKEL NANO HASIL SINTESIS BERBASIS AIR MENGGUNAKAN METODA SOL-GEL PADA BAHAN KAPAS SEBAGAI APLIKASI UNTUK TEKSTIL ANTI UV Komalasari, Maya; Sunendar, Bambang
Arena Tekstil Vol 28, No 1 (2013)
Publisher : Arena Tekstil

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (2135.385 KB)

Abstract

Partikel nano TiO2 berbasis air dengan pH basa telah berhasil disintesis dengan menggunakan metode sol-gel dan diimobilisasi pada kain kapas dengan menggunakan kitosan sebagai zat pengikat silang. Sintesis dilakukan  dengan prekursor TiCl4 pada konsentrasi 0,3 M, 0,5 M dan 1 M, dan menggunakan templat kanji dengan proses kalsinasi pada suhu 500˚C selama 2 jam. Partikel nano TiO2 diaplikasikan ke kain kapas dengan metoda pad-dry-cure dan menggunakan kitosan sebagai crosslinking agent. Berdasarkan hasil Scanning Electron Microscope (SEM),diketahui bahwa morfologi partikel TiO2 berbentuk spherical dengan ukuran nano (kurang dari 100 nm). Karakterisasi X-Ray Diffraction (XRD) menunjukkan adanya tiga tipe struktur kristal utama, yaitu (100), (101) dan (102) dengan fasa kristal yang terbentuk adalah anatase dan rutile. Pada karakterisasi menggunakan SEM terhadap serbuk dari TiO2 yang telah diaplikasikan ke permukaan kain kapas, terlihat adanya imobilisasi partikel nano TiO2 melalui ikatan hidrogen silang dengan kitosan pada kain kapas. Hasil analisa tersebut kemudian dikonfirmasi dengan FTIR (Fourier Transform Infra Red) yang hasilnya memperlihatkan puncak serapan pada bilangan gelombang 3495 cm-1, 2546 cm-1, dan 511 cm-1,  yang masing-masing diasumsikan sebagai adanya vibrasi gugus fungsi O-H, N-H dan Ti-O-Ti. Hasil SEM menunjukkan pula bahwa kristal nano yang terbentuk diantaranya adalah fasa rutile , yang berdasarkan literatur terbukti dapatberfungsi sebagai anti UV.
Evaluation on the Temperature and Calcination Time During Sol-gel Coating of TiO2 on Iron Foam substrate Ramdan, Raden Dadan; Haris, Luqman; Hermawan, Hendra; Sunendar, Bambang
Mesin Vol 26, No 1 (2017)
Publisher : Mesin

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1966.381 KB) | DOI: 10.5614/MESIN.2017.26.1.1

Abstract

Iron foam is iron based material which is widely applied due to its unique properties. However since corrosion is also a problem for this material, coating with innert material is required in enhancing its applications. In the present research, TiO2 coating is performed on iron foam suface by sol-gel dipping method. Focus is given on the study of the effect of calcinations temperature and time on the coating characteristics. TiCl4 is used as the precursor with concentration of 0.3 M, added with 1M HCl solution and chitosan soluation with concentration of 1%. Calcination is performed at temperature of 400, 500 dan 600oC and calcinations time of 1 and 3 hours inside controlled gas furnace using nitrogen atmosphere. Scanning Electron Microscopy (SEM) and Energy Dispersive Spectroscopy (EDS) characterization data shows that TiO2 particles form on the iron foam substrate. SEM characterization on the sample heated at 400oC and heating time of 1 hour shows the formation of nano particle titania (0.06 μm) which is homogeneously distributed with less agglomeration than others and considered as the best sample in the present research. As the temperature and time of calcinations increase, more inhomogeneous particle distribution and bigger particles form.
Hardness evaluation of dental composites fabricated from the uniform size and well-distributed zirconia-alumina-silica fillers with sol-gel technique Hakim, Muhammad Lukman Nur; Hasratiningsih, Zulia; Djustiana, Nina; Sunendar, Bambang; Faza, Yanwar
Padjadjaran Journal of Dentistry Vol 30, No 2 (2018): July
Publisher : Faculty of Dentistry Universitas Padjadjaran, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (433.347 KB) | DOI: 10.24198/pjd.vol30no2.18319

Abstract

Introduction: Several factor limits of services of dental composite have triggered further improvement. ZrO2-Al2O3-SiO2 system as filler of dental composite had been developed with sol-gel technique. Ultrasonic homogeniser were reported to change the particle size ditribution or shape. Unifom size and distribution of particle is believed to help define the behavior of hardness properties. Methods: The study was an laboratory experimental design. Filler ZrO2-Al2O3-SiO2 system were developed via sol-gel methods. Post calcination process, filler were immerse in ethanol and applied with ultrasonic homogeniser, with various amplitude i.e 50 rpm, 60 rpm and 80 rpm then named sample A, B, and C. XRD, SEM anda PSA were used to characterize of filler system. Subsequent filler were used to fabricate dental composite then evaluate the hardness value using micro-hardness tester. One–way ANOVA was used to analysis the statistical result of hardness value. Results: XRD pattern of three sample were similar in which tetragonal zirconia was prominent (57-61 %) followed by monoclinic zirconia (24-25%) and amorphous (15-17 %). While, SEM and PSA characterization showed amplitude 50 rpm (sample A) produce more uniform size and well-distributed particle filler than the others. In contrary, sample B and C showed higher peak in PSA results. It means there was dominating of filler with particular size.  However, the hardness value did not show significant differences between those filler (p>0,05). Conclusion: Dental composite that contain of different uniformity and distribution of filler ZrO2-Al2O3-SiO2 system has no significantly differences of hardness value.
Co-Authors Hakim, Muhammad Lukman Nur Haris, Luqman Hermawan, Hendra Iswandi Imran Ivindra Pane Maya Komalasari, Maya Nina Djustiana Partogi H. Simatupang, Partogi H. Ramdan, Raden Dadan Yanwar Faza Zulia Hasratiningsih, Zulia