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J Stuart Grossert
Department of Chemistry, Dalhousie University, Halifax, Nova Scotia
Chemical Engineering, Chemistry & Bioengineering Chemistry

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SYNTHESIS OF SAFRYL KETONE FROM SAFROLE Hanoch J Sohilait; Hardjono Sastrohamidjojo; Sabirin Matsjeh; J Stuart Grossert
Indonesian Journal of Chemistry Vol 4, No 1 (2004)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (45.071 KB) | DOI: 10.22146/ijc.21874

Abstract

Synthesis of safryl ketone from safrole has been achieved through conversion of allyl group to secondary alcohol, followed by oxidation with PCC-Al2O3. The oxymecuration-demercuration reaction of safrole with HgSO4-NaBH4 yields safryl alcohol (66.38%) and the oxidation of safryl alcohol with PCC-Al2O3 yields safryl ketone (62.92%). The structure elucidation of these products was conducted using Fourier Transformed Infra Red Spectroscopy (FTIR), Proton-Nuclear Magnetic Resonance (1H-NMR) and Mass Spectroscopy (MS).
Co-Authors Hanoch J Sohilait Hardjono Sastrohamidjojo Sabirin Matsjeh