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All Journal JURNAL KIMIA SAINS DAN APLIKASI BioWallacea Journal of Biological Research JURNAL SAINS KOVALEN: Jurnal Riset Kimia Jurnal Progres Kimia Sains ALCHEMY Jurnal Penelitian Kimia SELAPARANG: Jurnal Pengabdian Masyarakat Berkemajuan Hydrogen: Jurnal Kependidikan Kimia Jurnal Pengabdian UNDIKMA Hydrogen: Jurnal Kependidikan Kimia Indonesian Journal of Animal Agricultural Science (IJAAS) Jurnal Pengabdian Masyarakat Ilmu Terapan (JPMIT) Jurnal Pijar MIPA Makara Journal of Science
La Ode Kadidae, La Ode
Department Of Chemistry, Faculty Of Mathematics And Natural Sciences, Halu Oleo University, Kendari, Indonesia|Halu Oleo University|Indonesia
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Journal : JURNAL KIMIA SAINS DAN APLIKASI

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Synthesis of Dansyl Cyclen and Preliminary Study of Its Fluorescent Properties La Ode Kadidae; Ruslin Ruslin; Thamrin Azis; La Aba; Laode Abdul Kadir
Jurnal Kimia Sains dan Aplikasi Vol 25, No 2 (2022): Volume 25 Issue 2 Year 2022
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (831.263 KB) | DOI: 10.14710/jksa.25.2.63-70

Abstract

The synthesis of a dansyl cyclen-based compound as a potential chemical sensor has been carried out. The initial study of its fluorescent properties has also been conducted. This study aims to synthesize a cyclen-based compound comprising three identical pendant arms and another different arm carrying a dansyl fluorophore. Producing these heterogenous pendant arms, a-three pendant arm cyclen 9 was reacted with dansyl aziridine 10. The synthesis products were characterized using 1H NMR, 13C NMR, IR, and elemental analysis. In addition, a Fluorescent Spectrophotometer has been used to assess the fluorescent intensity changes of the synthetic ligand in a range of pH 2–13 and when it was titrated with some metal ions. Based on the results of characterization with 13C NMR for compound 2 and additional characterization with IR and elemental analysis for its hydrochloric form 11, it is wisely said that the proposed compound has been successfully synthesized, giving 66% yield as viscous brown oil 2. Moreover, the fluorescent property showed that the higher the pH employed, the higher the fluorescent intensity observed. Meanwhile, the addition of some cationic metals revealed that cadmium (II) gave the highest increase in the fluorescent intensities among other cationic metals.
Co-Authors Aden Mula Pratiwi Alimin Amal Astam Astam, Amal C Bijang Dian Permana, Dian Faariu, Nur Mala Herdi Budiman Ida Usman Ida Usman Ida Usman Ilimu, Edi Imran Jamili Jamili Kadir, Laode Abdul La Aba La Ode Abd Kadir La Ode Adi Parman Rudia La Ode Adi Parman Rudia Laily Nurliana Laily Nurliana Laily Nurliana Laily Nurliana Laily Nurliana Laode Abdul Kadir Laode Abdul Kadir M. Jahiding M. Jahiding Mashuni Mashuni Mashuni Pallawagau Muh. Aksan Dermawan Muh. Natsir Muksar Muksar Nohong Nugrawaty, Andi Laila Nur Arfa Yanti Ramadhan, L.O.A.N. Ruslan Ruslan Ruslin Ruslin Ruslin Ruslin Rustam Musta Setyawati, Arini Sunarti Sunarti Suriana Suriana THAMRIN AZIS Wa Ode Harlis Wahyu Ahwarul Asis Waode Sukmawati Arsyad