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All Journal JURNAL ILMIAH PENDIDIKAN FISIKA AL BIRUNI Indonesian Journal of Science and Technology
Ngurah Made Dharma Putra
Universitas Negeri Semarang
Computer Science & IT Earth & Planetary Sciences Education Electrical & Electronics Engineering Environmental Science Physics

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Structure, morphology, and optical properties of ZnO:Mg thin film prepared by sol-gel spin coating method Budi Astuti; Putut Marwoto; Azizah Zhafirah; Nur Hamid; Didik Aryanto; Sugianto Sugianto; Sulhadi Sulhadi; Ngurah Made Dharma Putra; Fianti Fianti
Jurnal Ilmiah Pendidikan Fisika Al-Biruni Vol 10, No 2 (2021): Jurnal Ilmiah Pendidikan Fisika Al-Biruni
Publisher : Universitas Islam Negeri Raden Intan Lampung, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (206.917 KB) | DOI: 10.24042/jipfalbiruni.v10i2.7239

Abstract

This research was conducted to analyze the Mg doping concentration effect on the structure, morphology, and optical properties of ZnO thin film prepared using the sol gel spin coating method. The Mg concentration was varied in the mole fraction of 1%, 3%, and 5%. Firstly, ZnO: Mg solution was dropped on a substrate and grown with a rotating speed of 3000 rpm and then annealed at 500 °C for 2 hours. The characterization of thin films' structure, morphology, and optical properties was done using XRD, FESEM, EDX, and UV-VIS spectrophotometer. XRD result showed a polycrystalline structure with three dominant peaks of (100), (002), and (101) plane, hexagonal wurtzite structures. Furthermore, the crystallite size was increased with the increase of Mg doping. FESEM results showed that the 5% ZnO: Mg thin film was the densest and least void from other films. In addition, the results of UV-Vis-NIR analysis showed the highest absorption value at a wavelength of 360-370 nm. The bandgap energy increased at 1% and 3% Mg doping samples but decreased by 5% Mg doping comes from the excess of oxygen in thin film with 5% Mg doping.
Synthesis, Characterization, and Electrochemical Performance of Reduced Graphene Oxide-Metal (Cu,Zn)-Oxide Materials Sugianto Sugianto; Ngurah Made Dharma Putra; Endah F. Rahayu; Wahyu B. Widayatno; Cherly Firdharini; Slamet Priyono; Didik Aryanto
Indonesian Journal of Science and Technology Vol 8, No 2 (2023): (ONLINE FIRST) IJOST: September 2023
Publisher : Universitas Pendidikan Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17509/ijost.v8i2.56065

Abstract

The reduced graphene oxide (rGO) and metal (Cu,Zn)-oxide composites were prepared using a one-step hydrothermal technique. The role of (Cu,Zn)-oxide on the physical and electrochemical properties of the composite was investigated. The composite consists of various shapes of ZnO nanoflowers and micro-spheres, as well as Cu-oxide nanoflakes and octahedron-like shapes. The (Cu,Zn)-oxides were formed in between the rGO layers and observed in the rGO-ZnO, rGO-CuO, and rGO-CuO-ZnO composites. The presence of ZnO, CuO, and rGO within the composite structure is also confirmed by the analyses of crystal structure, microstructure, and surface functional groups. Some excess impurities remaining from the surfactant give considerable differences in the electrochemical performance of the composites. The specific capacitance values of the rGO, rGO-ZnO, rGO-CuO, rGO-(0.5CuO-0.5ZnO), and rGO-(0.25CuO-0.75ZnO) composites are 9.32, 58.53, 54.14, 25.21, and 69.27 F/g, respectively. The formation ofa double metal-oxide structure as well as their insertion into the rGO sheet can significantly improve the electrochemical properties of the supercapacitor.
Structure, morphology, and optical properties of ZnO:Mg thin film prepared by sol-gel spin coating method Budi Astuti; Putut Marwoto; Azizah Zhafirah; Nur Hamid; Didik Aryanto; Sugianto Sugianto; Sulhadi Sulhadi; Ngurah Made Dharma Putra; Fianti Fianti
Jurnal Ilmiah Pendidikan Fisika Al-Biruni Vol 10, No 2 (2021): Jurnal Ilmiah Pendidikan Fisika Al-Biruni
Publisher : Universitas Islam Negeri Raden Intan Lampung, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24042/jipfalbiruni.v10i2.7239

Abstract

This research was conducted to analyze the Mg doping concentration effect on the structure, morphology, and optical properties of ZnO thin film prepared using the sol gel spin coating method. The Mg concentration was varied in the mole fraction of 1%, 3%, and 5%. Firstly, ZnO: Mg solution was dropped on a substrate and grown with a rotating speed of 3000 rpm and then annealed at 500 °C for 2 hours. The characterization of thin films' structure, morphology, and optical properties was done using XRD, FESEM, EDX, and UV-VIS spectrophotometer. XRD result showed a polycrystalline structure with three dominant peaks of (100), (002), and (101) plane, hexagonal wurtzite structures. Furthermore, the crystallite size was increased with the increase of Mg doping. FESEM results showed that the 5% ZnO: Mg thin film was the densest and least void from other films. In addition, the results of UV-Vis-NIR analysis showed the highest absorption value at a wavelength of 360-370 nm. The bandgap energy increased at 1% and 3% Mg doping samples but decreased by 5% Mg doping comes from the excess of oxygen in thin film with 5% Mg doping.
Co-Authors Azizah Zhafirah Budi Astuti Cherly Firdharini Didik Aryanto Didik Aryanto Endah F. Rahayu Fianti Fianti, Fianti Nur Hamid Putut Marwoto S Sulhadi Slamet Priyono Sugianto - Wahyu B. Widayatno