PROSIDING SEMINAR KIMIA
Vol 1 No 1 (2022): Prosiding SNK 2022

SINTESIS DAN KARAKTERISASI MATERIAL SILIKA MESOPORI SBA-15 DENGAN ULTRASONIC ASSISTED SOL-GEL METHOD MENGGUNAKAN PELARUT ASAM ASETAT

Siti Sarah (Unknown)
RR Dirgarini Julia Nurlianti Subagyono (Unknown)
Veliyana Londong Allo (Unknown)



Article Info

Publish Date
12 Jul 2023

Abstract

Synthesis and characterization of mesoporous silica material SBA-15 with ultrasonic assisted sol-gel method using acetic acid solvent has been conducted. The mesoporous silica material SBA-15 was characterized by N2 adsorption/desorption Analysis, Small Angle X-Ray Diffraction (SAXRD), Scanning Electron Microscopy (SEM), Fourier Transform Infrared (FTIR). SBA-15 material resulted from the calcination method for template removal has a surface of 876 m2/g, a pore volume of 5,1 cm3/g and a pore diameter of 1,13 nm. The SAXRD pattern of SBA-15 showed three distinctive peaks with Miller indeces of 100, 110 and 200 respectively. The morphology of the SBA-15 material has the form of aggregate particles with a reguler cylindrical structure on the particles. Infrared spectra of SBA-15 showed the presence of functional groups, namely Si-O-Si, Si-OH and –OH. Keywords: Mesoporous silica, SBA-15, sonication

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