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INDONESIA
Indonesian Journal of Pure and Applied Chemistry
Published by Universitas Tanjungpura
ISSN : 26208571     EISSN : 2620858X     DOI : -
Core Subject : Science,
Biochemistry, Genetics & Molecular Biology Chemistry
Indonesian Journal of Pure and Applied Chemistry (IJoPAC) was first established in 2018 as a scientific journal that accommodates researchers and education practitioners to publish scientific work and research results which are the results of experiments or literature studies in the field of chemistry. Publications are carried out periodically with three issues (January-April, May-August, September-December) in one volume per year. Published scientific work can be in the form of original articles, short communications and review results covering the fields of Physical chemistry, Organic chemistry, Analytical chemistry, Inorganic chemistry, Biochemistry / Biological Chemistry, Applied Chemistry. Focus and Scope of Indonesian Journal of Pure and Applied Chemistry covering the fields : Physical chemistry Organic chemistry Analytical chemistry Inorganic chemistry Biochemistry/Biological Chemistry Applied Chemistry
Arjuna Subject : Kimia(semua kategori) - Kimia (Lain-Lain)
Articles 5 Documents
 1 
Search results for , issue "Vol 3, No 3 (2020)" : 5 Documents clear
KARAKTERISASI KOMPONEN DESTILAT MINYAK SEREH WANGI (Cymbopogon nardus l. Rendle) DARI KECAMATAN KUALA BEHE KABUPATEN LANDAK Omarta Omarta; Afghani Jayuska; Imelda Hotmarisi Silalahi
Indonesian Journal of Pure and Applied Chemistry Vol 3, No 3 (2020)
Publisher : Tanjungpura University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (483.822 KB) | DOI: 10.26418/indonesian.v3i3.44155

Abstract

Tanaman Sereh Wangi (Cymbopogon nardus l. Rendle) merupakan tanaman dari famili Poaceae yang telah lama dikenal sebagai penghasil minyak atsiri. Pemanfaatan minyak atsiri sereh wangi telah banyak diteliti sebagai pestisida nabati. Penelitian ini bertujuan untuk mengetahui persen rendemen minyak sereh wangi dan mengetahui pengaruh variasi suhu dan waktu fraksinasi terhadap komposisi senyawa yang terkandung dalam minyak sereh wangi. Minyak sereh wangi yang digunakan berwarna kuning pucat jernih dengan dengan berat jenis 0,8662 gram. Hasil identifikasi GC-MS menunjukkan bahwa minyak sereh wangi sebelum didestilasi mengandung 10 puncak senyawa dengan 3 puncak senyawa mayor berdasarkan  area dominan yaitu alpha-pinene 79,07%; beta-ocimene 8,80%; dan sitronelal 6,42 %. Hasil fraksi minyak setelah didestilasi yaitu pada destilat pertama luas area alpha-pinene 90,38%; beta-ocimene 5,42%; dan sitronelal 0,47%. Destilat kedua alpha-pinene 88,11%; beta-ocimene 6,88%; dan sitronelal 0,63%. Destilat ketiga alpha-pinene 84,37%; beta-ocimene 9,40%; dan sitronelal 0,98%
PENGARUH VARIASI KOMPOSISI SELULOSA JERAMI PADI DAN LIMBAH BOTOL PLASTIK POLIETILEN TEREFTALAT (PET) TERHADAP KARAKTERISTIK BIODEGRADABLE PLASTIC Hanna Sjafarina; Intan Syahbanu; Nurlina Nurlina
Indonesian Journal of Pure and Applied Chemistry Vol 3, No 3 (2020)
Publisher : Tanjungpura University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (953.052 KB) | DOI: 10.26418/indonesian.v3i3.44154

Abstract

Research on the effect of variations in the composition of rice straw cellulose on the characteristics of biodegradable PET-Cellulose plastic. The purpose of this study is to explain the effect of the composition of rice straw cellulose and PET on the characteristics of biodegradable plastic made from composite of rice straw cellulose and PET. This research was conducted  in several stages, the isolation of cellulose from rice straw, recycling PET from mineral water bottle,  mixing cellulose and PET, then testing the characteristics, the DTA-TGA thermal characteristic test, and degradation test with the soil burial test method. . In the thermal characteristics test there was a decrease in weight in samples with composition PET: cellulose 90:10; 60:40; and 50:50 each with 0.719; 0.710; 0.581 mg in the temperature range 38.30-68.32 ° C, 40.72-68.17 ° C, 41.45-80.40 ° C, while in the samples 80:20 and 70:30 there was no decrease in weight the temperature. In the sample 90:10; 80:20; 70:30; 60:40 and 50; 50 there is a decrease in weight each of 4,045; 3,909; 3,464; 2,760 and 3,205 mg at temperatures 328, 16-430.65 ° C, 362.05-442.15 ° C, 349.96-439.82 ° C, 388.29-446.70 ° C, and 325.39-420.79 ° C. The degradation test using soil burial test method obtained percent weight loss in samples with PET composition: 70:30 cellulose which was 38.24%.
SINTESIS DAN TRANSISI ELEKTRONIK KOMPLEKS TEMBAGA (II)-KLOROFIL Imelda Hotmarisi Silalahi; Julan Julan; Muhammad Yusprianto; Rudiyansyah Rudiyansyah
Indonesian Journal of Pure and Applied Chemistry Vol 3, No 3 (2020)
Publisher : Tanjungpura University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (701.392 KB) | DOI: 10.26418/indonesian.v3i3.44149

Abstract

The copper (II)-chlorophyll complex was prepared from the reaction between the chlorophyll isolated from cassava leaves and the metal ion precursor, CuSO4.5H2O in methanol under reflux for four hours. The FTIR spectra of the reaction product compared to the chlorophyll spectra show an indication of a complexation through metal coordination with the N atom from the phyrol ring replacing the magnesium (II) ion in chlorophyll.This assumption is drawn based on changes on FTIR spectra, i.e. vibration absorption originating from the CN and NH groups in the porphyrin ring and the appearance of the distinctive vibration band of nitrogen-metal bonds which is annotated as Cu-N groups at 599.88 cm-1. Another sign is the change in the OH and CO vibration bands which imply changes in aggregate properties that occur through inter-molecular interactions due to the introduction of copper (II) metal into the chlorophyll structure. The formation of copper (II)-chlorophyll compounds is also shown from the results of atomic absorption spectroscopy by recording copper metal in the product and reducing magnesium metal concentration. UV-vis spectra of chlorophyll in methanol show a characteristic band in the dark area (Soret band) at a maximum wavelength of 404 nm and the visible area (Q band) with the strongest intensity at 665 nm. These peaks appear to shift hypsochromically in the copper (II)-chlorophyll compound to 397 nm and 650 nm with higher absorptivity, indicating a change in the electronic transition of the chlorophyll after coordinating with the copper (II) ion. A new peak at 411 nm was also observed which is suggested to indicate that the copper (II) -chlorophyll complex is in an octahedral geometry in the aggregate coordinated via nitrogen atoms in the phyrol ring in place of the magnesium (II) ion.
ANALISIS NATRIUM DODESILBENZENA SULFONAT DALAM IKAN LELE SECARA MASERASI DAN SPEKTROFOTOMETRI UV-VIS MENGGUNAKAN METILEN BIRU Kahar Muzakar; Adhitasari Suratman; Roto Roto
Indonesian Journal of Pure and Applied Chemistry Vol 3, No 3 (2020)
Publisher : Tanjungpura University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (357.509 KB) | DOI: 10.26418/indonesian.v3i3.44150

Abstract

Method validation of sodium dodecylbenzene sulfonate (SDBS) analysis in catfish by maceration and UV-Vis spectrophotometry using methylene blue active substances (MBAS) method was performed. The first stage of this research was method validation comprising correlation coefficient, sensitivity, Limit of Detection (LOD), Limit of Quantitation (LOQ), precision, and accuracy. The extraction of SDBS by maceration with methanol for 16 h and analysis by UV-Vis spectrophotometry using MBAS were performed. Then, this method was applied to analyze SDBS in catfish. The results of validation of SDBS analysis in cultivated catfish give correlation coefficient 0.9944, sensitivity 10.57 × 104 L mol-1 cm-1, LOD 0.01776 mg/L, LOQ 0.05922 mg/L, precision 0.1351-1.300 %, and accuracy 87.64-90.01 %, respectively. The SDBS concentrations in fish increase with the increase in the SDBS concentration in cultivating water. Bioconcentration Factor (BCF) values were inversely proportional to the concentration of SDBS in the cultivating water. The concentrations of SDBS on catfish, tilapia, and carp in traditional markets were 5.719-8.162; 5.180-6.548; and 2.973-5.874 mg/kg, respectively. In general, analysis method of SDBS in catfish by maceration and UV-Vis spectrophotometry with MBAS show a good result and can be used as a routine analysis in fish.
EKSTRAKK UMBI BAWANG DAYAK (Eleutherine palmifolia (L.) Merr.) SEBAGAI PEREDUKSI ION PERAK DALAM SINTESIS NANOPARTIKEL PERAK Normaningsih Rahayu; Gusrizal Gusrizal; Nurlina Nurlina
Indonesian Journal of Pure and Applied Chemistry Vol 3, No 3 (2020)
Publisher : Tanjungpura University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (937.878 KB) | DOI: 10.26418/indonesian.v3i3.44151

Abstract

Silver nanoparticles (AgNPs) are one of the best plasmonic candidates that have been used in Surface Plasmon Resonance (SPR)-based nanosensors for the detection of metallic ions. In this research, AgNPs were prepared by the method using Eleutherine palmifolia (L.) Merr root ethanol extract. Silver nanoparticles were synthesized by reduction of silver nitrate with Eleutherine palmifolia (L.) Merr. Tuber extract (concentration of extract = 0,01%, pH = 11, volume ratio 1:1) in the boiling water bath for 90 minutes. The formation of silver nanoparticles was indicated by the appearance of yellow color and monitored using a UV-Visible spectrophotometer. The spectra showed the maximum peak at 401-405 nm. The resulted silver nanoparticles with the size of 10-20 nm were stable at least for 16 weeks.

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