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All Journal Ganendra: Majalah IPTEK Nuklir Jurnal Sains dan Teknologi Nuklir Indonesia (Indonesian Journal of Nuclear Science and Technology) Jurnal Ecolab
Diah Dwiana Lestiani
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Biochemistry, Genetics & Molecular Biology Computer Science & IT Energy Environmental Science Materials Science & Nanotechnology Mechanical Engineering Medicine & Pharmacology Physics Other

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Journal : Ganendra: Majalah IPTEK Nuklir

 1 
UJI INTERKOMPARASI METODE AAN DAN XRF UNTUK ANALISIS SAMPEL SEDIMEN IAEA INTER COMPARISON TEST OF NAA AND XRF METHOD FOR IAEA SEDIMENT SAMPLE ANALYSIS Syukria Kurniawati; Indah Kusmartini; Diah Dwiana Lestiani; Woro Yatu Niken Syahfitri
GANENDRA Majalah IPTEK Nuklir Volume 17 Nomor 1 Januari 2014
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Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (604.808 KB) | DOI: 10.17146/gnd.2014.17.1.1298

Abstract

Laboratorium Pusat Teknologi Nuklir Bahan dan Radiometri mengikuti kegiatan interkomparasi IAEA tahun 2011. Sampel uji yaitu sedimen dengan kode IAEA 457. Metode uji meliputi Analisis Aktivasi Neutron (AAN) dan X-Ray Fluorescence (XRF). Dilakukan perbandingan metode AAN dan XRF untuk mengevaluasi kinerja masing-masing metode dan mengetahui kesesuaian kedua metode tersebut dalam analisis unsur pada sampel interkomparasi IAEA. Evaluasi kinerja masing-masing metode dilakukan dengan uji akurasi dan perhitungan z-score sedangkan kesesuaian metode diuji dengan uji t-berpasangan. Hasil analisis sampel menggunakan AAN diidentifikasi enam unsur Al, Fe, Cr, Co, Mn dan Zn sedangkan XRF diidentifikasi delapan unsur Al, Fe, Cr, Co, Cu, Mn, Pb dan Zn. Hasil uji akurasi pada AAN, unsur Al dan Fe kurang memuaskan sedangkan pada XRF unsur Co memiliki hasil yang kurang baik. Hasil perhitungan z-score, hampir semua unsur memberikan hasil yang memuaskan kecuali Al menggunakan metode AAN. Uji t-berpasangan yang dilakukan pada hasil analisis sedimen menggunakan AAN dan XRF memberikan hasil t-hitung < t-tabel, artinya tidak ada perbedaan hasil analisis antara kedua metode. Hasil tersebut menunjukkan bahwa metode AAN dan XRF dapat saling melengkapi untuk analisis unsur pada sampel IAEA 457. Secara umum, kedua hasil analisis unsur menunjukkan kesesuaian yang baik sehingga memperkuat validitas hasil analisis sampel interkomparasi IAEA.
EVALUATION OF NAA LABORATORY RESULTS IN INTER-COMPARISON ON DETERMINATION OF TRACE ELEMENTS IN FOOD AND ENVIRONMENTAL SAMPLES Diah Dwiana Lestiani; Syukria Kurniawati; Natalia Adventini
GANENDRA Majalah IPTEK Nuklir Volume 15 Nomor 1 Januari 2012
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Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (157.655 KB) | DOI: 10.17146/gnd.2012.15.1.25

Abstract

Inter-comparison program is a good tool for improving quality and to enhance the accuracy and precision of theanalytical techniques. By participating in this program, laboratories could demonstrate their capability andensuring the quality of analysis results generated by analytical laboratories. The Neutron Activation Analysis(NAA) laboratory at National Nuclear Energy Agency of Indonesia (BATAN), Nuclear Technology Center forMaterials and Radiometry-PTNBR laboratory participated in inter-comparison tests organized by NAA workinggroup. Inter-comparison BATAN 2009 was the third inter-laboratory analysis test within that project. Theparticipating laboratories were asked to analyze for trace elements using neutron activation analysis as theprimary technique. Three materials were distributed to the participants representing foodstuff, and environmentalmaterial samples. Samples were irradiated in rabbit facility of G.A. Siwabessy reactor with neutron flux ~ 1013n.cm-2.s-1, and counted with HPGe detector of gamma spectrometry. Several trace elements in these sampleswere detected. The accuracy and precision evaluation based on International Atomic Energy Agency (IAEA)criteria was applied. In this paper the PTNBR NAA laboratory results is evaluated.Keywords: inter-comparison, neutron activation analysis, trace elements, foodstuff, environmental samples,NAA laboratory
Co-Authors Dyah Kumala Sari Esrom Hamonangan Esrom Hamonangan Panjaitan Hari Wahyudi Hernani Yulinawati Indah Kusmartini Indah Kusmartini Isa Ansyori Muhayatun Santoso Natalia Adventini Rita Mukhtar RITA RITA Susy Lahtiani Syukria Kurniawati Syukria Kurniawati Woro Yatu Niken Syahfitri