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All Journal PROSIDING SEMINAR KIMIA Jurnal Kimia Mulawarman JURNAL ATOMIK
Alimuddin -
Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman
Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Energy Environmental Science

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TEST PHYTOCHEMICAL, TOXICITY AND ANTIBACTERIAL ACTIVITY FRACTION LEAF EXTRACT VARIOUS MAHANG (M acarang apruinosa (Miq.) Mull. Arg.) AGAINST Escherichia coli AND Staphylococcus aureus Mustafidah -; Chairul Saleh; Alimuddin -
PROSIDING SEMINAR KIMIA SEMINAR NASIONAL KIMIA 2014
Publisher : PROSIDING SEMINAR KIMIA

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Phytochemical, to xicity and antibacterial act ivity tests of total extract, fractions of n-heksana, ethyl acetate and ethanol-water fro m mahang leaf (Macaranga pruinosa (M.) M. A.) fro m KRUS (Kebun Raya Unmul Samarinda), East Kalimantan has been carried out. Based on the secondary metabolites phytochemical test of the (Macaranga pruinosa (M.) M. A.) leaf show that total extract is contain alkaloid and steroid. n-hexane fraction is contain alkaloid and steroid. Ethyl acetate fract ion is contain steroid. Ethanol-water fract ion is contain alkaloid and phenolic. Brine shrimp lethality test values obtained Lethal Concentration 50 % (LC 50 ) total extract 27,5036 ppm , n-heksana fraction 12,0773 pp m, ethyl acetate fraction 23719,2305 ppm and ethanol-water fraction 250,0384 ppm. Antibacteria act ivity test of extracts for Staphylococcus aureus bacteria (positive Gram) and Escherichia coli (negative Gram) minimum inhibitor consentration of 0-1 % (b/v) fro m ext ract fractions of n-heksana and fractions ethyl acetate for Staphylococcus aureus bacteria and fractions ethyl acetate for Escherichia coli bacteria.
PENENTUAN KUALITAS LEMAK PADA BAGIAN PERUT IKAN PATIN DJAMBAL (Pangasius djambal) Hamsinah -; Alimuddin -; Erwin -
PROSIDING SEMINAR KIMIA SEMINAR NASIONAL KIMIA 2013
Publisher : PROSIDING SEMINAR KIMIA

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The purpose of this research was to determine the quality of fat in the abdomen djambal patin fish, which includes parameters water content, free fatty acid, iodine number, peroxide number, and the physical characteristics of the fat which includes the melting and freezing. Each parameter in each sample were given treatment three replications. The method used to determine water content, free fatty acid, iodine number, peroxide number is method Open oven, alkalimetri titration and iodometric titration.The results for water content, free fatty acid, peroxide number and iodine number in each sample from the average of three repetitions was 4.4%, 0.0563%, 11.52 meq and 8.34. Based on these results it can be concluded that the water content and the peroxide number weren’t conform in Indonesian national standards, while the free fatty acid content and iodine number were conform in Indonesian national standards.
ANALISIS KAFEIN DALAM KOPI ROBUSTA (TORAJA) DAN KOPI ARABIKA (JAWA) DENGAN VARIASI SIKLUS PADA SOKLETASI Tria Annisa Rizky; Chairul Saleh; Alimuddin -
JURNAL KIMIA MULAWARMAN Vol 13 No 1 (2015)
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

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The research about analysis of caffeine content on coffee Robusta (Toraja) and coffee Arabika (Jawa) with cycle variations using spectrophotometer UV has been done. Coffee extract obtained throughsoxhletation with ethanol 96 % and variation cycles used is 3, 6, 9, 12 and 15, tested with spectrophotometer UV at a wavelength of 272 nm. The result of this research was obtained the caffeine content in coffee Robusta (Toraja) for 3, 6, 9, 12, 15 cycles consecutive is 1.439 mg/L, 2.158 mg/L, 2.695 mg/L, 2.887 mg/L and 3.700 mg/L. The caffeine content obtained coffee Arabika (Jawa) for 3, 6, 9, 12, 15 cycles consecutive is 0.474 mg/L, 0.478 mg/L, 1.056 mg/L, 1.540 mg/L and 1.926 mg/L respectively.Keywords: Coffee Robusta, Coffee Arabika, Ethanol 96 %, Soxhletation, Caffeine, Spectrophotometer UV
PEMANFAATAN ARANG AKTIF DARI KULIT DURIAN (Durio zibethinus L.) SEBAGAI ADSORBEN ION LOGAM KADMIUM (II) Marlinawati -; Bohari Yusuf; Alimuddin -
JURNAL KIMIA MULAWARMAN Vol 13 No 1 (2015)
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

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The research of adsorption cadmium (II) metal ions in the solution by activated carbon from durian peel has been done. Adsorption process is done by using a variation of pH (1, 2, 3, 4, 5 and 6), variation of contact time (15, 30, 45, 60, 75 dan 90 menit), variation of the concentration (20, 30, 40, 50 dan 60 mg/L). Analysis of metal ion concentration of cadmium (II) used by Atomic Absorption Spectrophotometer (AAS). The results of this research shows that the optimum condition was achieved at the pH value of 4 and the contact time of 60 minutes. Metal ion adsorption of cadmium (II) by activated carbon from durian’s peel at pH value of 4 and the contact time of 60 minutes can achieve 64,540%. Metal ion adsorption capacity of cadmium (II) adsorbed by activated carbon from durian’s peel can achieve 0,4951 mg/g.Keywords : Adsorption, Activated Carbon, Durian Peel, Metal Ions Cadmium (II)
DISTRIBUSI LOGAM TIMBAL (Pb) PADA TANAMAN WEDELIA (Wedelia trilobata (L.) Hitch) AKIBAT EMISI KENDARAAN BERMOTOR DI BEBERAPA JALAN KOTA SAMARINDA Amalia Saleha; Alimuddin -; Rahmat Gunawan
JURNAL KIMIA MULAWARMAN Vol 10 No 2 (2013)
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

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The research has done of "The distribution of lead (Pb) on wedelia plants contaminated by vehicular emission on several main road in samarinda”. This study aimed to determine the metal concentrations of lead in roots, flowers and leaves of plants wedelia at several locations in the city of Samarinda on PM Noor Street, Wahid Hasyim Street, Pahlawan Street, AW Syahrani Street, and Belatuk Street (control location) were the different traffic density and the treatment of leaching on levels of lead found in wedelia plants. The concentrations of lead metal on wedelia plants were measured using an Atomic Absorption Spectrophotometer (AAS) at a wavelength of 283.3 nm. The results showed that The highest levels of Pb obtained on PM Noor and lowest on Belatuk, were the traffic density is high concentration of lead is absorbed more than low traffic density. And the treatment of non-leaching and leaching concentrations obtained difference was not significant, indicating leaching did not significantly affect the concentration of Pb on plants.
PENURUNAN GARAM KLORIDA AIR LAUT DENGAN MEMANFAATKAN MODIFIKASI PATI DARI LIMBAH BONGGOL PISANG AMBON (Musa paradisiaca var sapientum) Aulia Husna Rabbani; Alimuddin -; Chairul Saleh
JURNAL KIMIA MULAWARMAN Vol 13 No 1 (2015)
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

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The research of desalination the sea water by utilization of the strach bump a “Pisang Ambon (Musa paradisiaca var sapientum)” modification has been done. Modification of starch bump “Pisang Ambon (Musa paradisiaca var sapientum)” had be a ability better than starch bump “Pisang Ambon (Musa paradisiaca var sapientum)” in the levels of chloride. The variation upon which to do to absorb chloride of sea water which are starch, starch been activated NaOH and starch acetate bump of a “Pisang Ambon (Musa paradisiaca var sapientum)”. Where The characteristic of the third ingredients were done by analysis FT-IR that showed the spectrum in the wavenumber of each of which are read the force –OH,C-H streaching, C-H bending, CO ester in the spectrum of starch and starch been activated with NaOH and then are read the ester C=O in the wave number of 1751,36/cm and C-O ester and forth on the wave number of 1234,44/cm to the full spectrum of starch acetate. The rendemen a modification of the starch was also shown the modified starch in the bump a “Pisang Ambon (Musa paradisiaca var sapientum)” then more starch obtained. And which after passed a sample of starch bumb “Pisang Ambon (Musa paradisiaca var sapientum)” wet sea water left in levels chloride 20.160,77 mg/L, in the starch bump “Pisang Ambon (Musa paradisiaca var sapientum)” dry sea water left in levels of chloride 19.783,23 mg/L, in the starch bump “Pisang Ambon (Musa paradisiaca var sapientum)” have been activated with NaOH wet sea water left in the levels of chloride 19.405,68 mg/L, in the starch bump “Pisang Ambon (Musa paradisiaca var sapientum)” have been activated with NaOH dry sea water left in levels of chloride 19.028,14 mg/L and in the starch acetat bump “Pisang Ambon (Musa paradisiaca var sapientum)” sea water left in levels of chloride 18.461,83 mg/L.Keywords: the water of the sea, salt chloride, spectrum FTIR, starch and modification of starch bump a Pisang Ambon (Musa paradisiaca var sapientum)
PREDIKSI PUNCAK KEMATANGAN BUAH NAGA MELALUI PENGUKURAN GULA REDUKSI DENGAN METODE NELSON-SOMOGYI Alimuddin -
JURNAL KIMIA MULAWARMAN Vol 9 No 2 (2012)
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

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Prediction of dragon fruit maturation peak by measuring reductor sugar with nelson-somogyi method have been done. Prediction was done by using three modes which are experimental result, regression model and first derivation. Age of the fruit which used in this research were 1, 3, 5 and 7 weeks old. Based on the result of this research can be concluded that maturation peak of dragon fruit happens at between 5 until 6 weeks old.Keywords: Dragon Fruit, Reductor Sugar and Nelson-Somogyi Method.
UJI FITOKIMIA DAN AKTIVITAS ANTIBAKTERI DARI TANAMAN MERKUBUNG (Macaranga gigantea (Rchb.f. & Zoll) Mull. Arg.) DENGAN EKSTRAK TOTAL, FRAKSI n-HEKSANA, ETIL ASETAT DAN ETANOL AIR TERHADAP BAKTERI Escherichia coli dan Staphylococcus aureus Azhar Seli Apriani; Chairul Saleh; Alimuddin -
JURNAL KIMIA MULAWARMAN Vol 12 No 1 (2014)
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

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Phytochemical tests, mortality of larvae shrimp (brine shrimp lethality test) and the antibacterial activity of theleaf merkubung (Macaranga gigantea Rchb.f. & Zoll.) With various factions has been conducted. Merkubung leafsamples were extracted with ethanol and concentrated by using rotary evaporator. The total extract was fractionatedwith n-hexane and ethyl acetate. The results of phytochemical compounds secondary metabolites merkubung leavesshowed that the total extract are contains alkaloids, phenolics and steroids. n-hexane fraction are containing alkaloids,flavonoids and steroids. Ethyl acetate faction are containing flavonoids and steroids. Ethanol-water faction is containingphenolic compounds. Shrimp larvae mortality trials showed mortality rates of larvae of Artemia salina (L) by usingSAS Probit analysis to determine the value of Lethal Concentration 50 % (LC50). The test shows that the most toxicfraction is the total extract with LC50 values of 459.8414 ppm. The test of antibacterial activity using paper disc methodand shows that the most active faction is the total extract with a MIC (Minimmum Inhibitor Concentration) of 1 % is6.5 mm diameter clear zone on Staphylococcus aureus (Gram positive) and 6.25 mm in the bacterium Escherichia coli(Gram negativ).Keywords : Macaranga gigantea Rchb.f. & Zoll., phytochemical test, Antibacteria activity test, LC50.
ANALISIS KANDUNGAN KAFEIN DALAM KOPI SUMATERA DAN KOPI FLORES DENGAN VARIASI SIKLUS MENGGUNAKAN SPEKTROFOTOMETER UV-VIS Nadhirah -; Alimuddin -; Chairul Saleh
JURNAL KIMIA MULAWARMAN Vol 13 No 1 (2015)
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

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The research about analysis of caffeine content on coffee Sumatera and coffee Flores with cycle variations using spectrophotometer UV-Vis has been done. Coffee extract obtained through soxhletation with ethanol 96% and variation cycles used is 3, 6, 9, 12 and 15. The extract obtained is dissolved in ethanol 96% and tested with spectrophotometer UV-Vis at a wavelength of 272 nm. The result obtained in this research is the caffeine content in coffee Sumatera for 3, 6, 9, 12, 15 cycles consecutive are 0.582 mg/L; 0.986 mg/L; 1.315 mg/L; 2.143 mg/L and 2.918 mg/L. While the caffeine content obtained coffee Flores for 3, 6, 9, 12, 15 cycles consecutive are 0.465 mg/L; 0.599 mg/L; 0.728 mg/L; 1.186 mg/L and 1.653 mg/L.Keywords : Coffee Sumatera, Coffee Flores, Ethanol 96%, Soxhletation, Caffeine, Spectrophotometer UV-Vis
UJI FITOKIMIA, TOKSISITAS DAN AKTIVITAS ANTIBAKTERI dari EKSTRAK BERBAGAI FRAKSI DAUN MAHANG (Macarang apruinosa (Miq.) Mull. Arg.) terhadap BAKTERI Escherichia coli dan Staphylococcus aureus Mustafidah -; Chairul Saleh; Alimuddin -
JURNAL KIMIA MULAWARMAN Vol 12 No 2 (2015)
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

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Phytochemical, toxicity and antibacterial activity tests of total extract, fractions of n-heksana, ethyl acetate and ethanol-water from mahang leaf (Macaranga pruinosa (M.) M. A.) from KRUS (Kebun Raya Unmul Samarinda), East Kalimantan has been carried out. Based on the secondary metabolites phytochemical test of the (Macaranga pruinosa (M.) M. A.) leaf show that total extract is contain alkaloid and steroid. n-hexane fraction is contain alkaloid and steroid. Ethyl acetate fraction is contain steroid. Ethanol-water fraction is contain alkaloid and phenolic. Brine shrimp lethality test values obtained Lethal Concentration 50 % (LC50) total extract 27,5036 ppm , n-heksana fraction 12,0773 ppm, ethyl acetate fraction 23719,2305 ppm and ethanol-water fraction 250,0384 ppm. Antibacteria activity test of extracts for Staphylococcus aureus bacteria (positive Gram) and Escherichia coli (negative Gram) minimum inhibitor consentration of 0-1 % (b/v) from extract fractions of n-heksana and fractions ethyl acetate for Staphylococcus aureus bacteria and fractions ethyl acetate for Escherichia coli bacteria.Keywords (Macaranga pruinosa (M.) M. A.), phytochemical test, Antibacteria activity test, LC 50 .
Co-Authors Agustinus Miu Albayssag Faisal Tanjung Amalia Saleha Aulia Husna Rabbani Azhar Seli Apriani Bohari Yusuf Chairul Saleh Daniel - Erwin Erwin Hamsinah - Indri Ayu Lestari Marlinawati - Mendriyani Pali Mustafidah - Mutia Wulandari Nadhirah - Rahmat Gunawan Roy Aditya Rudi Kartika, Rudi Saibun Sitorus Siti Hosniah Siti Nurliana Sugiarti - Tria Annisa Rizky Yogie Henry Payung