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All Journal Jurnal Teknologi Bulletin of Chemical Reaction Engineering & Catalysis The Journal of Pure and Applied Chemistry Research Jurnal IPTEK Jurnal Litbang Industri Science and Physics Education Journal (SPEJ) Indonesian Mining Journal Prosiding Konferensi Nasional PKM-CSR Jurnal Rekayasa Kimia & Lingkungan Jurnal Pengabdian Masyarakat (JPM) Pinang Masak Bulletin of Chemical Reaction Engineering & Catalysis Indonesian Mining Journal
Lenny Marlinda
Universitas Jambi
Humanities Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Control & Systems Engineering Earth & Planetary Sciences Economics, Econometrics & Finance Education Electrical & Electronics Engineering Energy Engineering Environmental Science Industrial & Manufacturing Engineering Materials Science & Nanotechnology Mathematics Mechanical Engineering Medicine & Pharmacology Nursing Physics Public Health Social Sciences

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Journal : Bulletin of Chemical Reaction Engineering

 1 
Hydrocracking of Cerbera manghas Oil with Co-Ni/HZSM-5 as Double Promoted Catalyst Lenny Marlinda; Muhammad Al-Muttaqii; Ignatius Gunardi; Achmad Roesyadi; Danawati Hari Prajitno
Bulletin of Chemical Reaction Engineering & Catalysis 2017: BCREC Volume 12 Issue 2 Year 2017 (August 2017)
Publisher : Department of Chemical Engineering - Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (641.609 KB) | DOI: 10.9767/bcrec.12.2.496.167-184

Abstract

The effect of various reaction temperature on the hydrocracking of Cerbera manghas oil to produce a paraffin-rich mixture of hydrocarbons with Co-Ni/HZSM-5 as doubled promoted catalyst were studied. The Co-Ni/HZSM-5 catalyst with various metal loading and metal ratio was prepared by incipient wetness impregnation. The catalysts were characterized by XRD, AAS, and N2 adsorption-desorption. Surface area, pore diameter, and pore volume of catalysts decreased with the increasing of metals loading. The hydrocracking process was conducted under hydrogen initial pressure in batch reactor equipped with a mechanical stirrer. The reaction was carried out at a temperature of 300-375 oC for 2 h.  Depending on the experimental condition, the reaction pressure changed between 10 bar and 15 bar.   Several parameters were used to evaluate biofuel produced, including oxygen removal, hydrocarbon composition and gasoline/kerosene/diesel yields. Biofuel was analyzed by Fourier Transform Infrared Spectroscopic (FTIR) and gas chromatography-mass spectrometry (GC-MS). The composition of hydrocarbon compounds in liquid products was similar to the compounds in the gasoil sold in unit of Pertamina Gas Stations, namely pentadecane, hexadecane, heptadecane, octadecane, and nonadecane with different amounts for each biofuel produced at different reaction temperatures. However, isoparaffin compounds were not formed at all operating conditions. Pentadecane (n-C15) and heptadecane (n-C17) were the most abundant composition in gasoil when Co-Ni/HZSM-5 catalyst was used. Cerbera Manghas oil can be recommended as the source of non-edible vegetable oil to produce gasoil as an environmentally friendly transportation fuel. 
Hydrocracking of Non-edible Vegetable Oils with Co-Ni/HZSM-5 Catalyst to Gasoil Containing Aromatics Danawati Hari Prajitno; Achmad Roesyadi; Muhammad Al-Muttaqii; Lenny Marlinda
Bulletin of Chemical Reaction Engineering & Catalysis 2017: BCREC Volume 12 Issue 3 Year 2017 (December 2017)
Publisher : Department of Chemical Engineering - Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (134.117 KB) | DOI: 10.9767/bcrec.12.3.799.318-328

Abstract

Biofuel has been considered as one of the environmentally friendly energy sources to substitute fossil fuel derived from non-edible vegetable oil. This research aims to investigate the effect of the non-edible vegetable oil composition on a specific hydrocarbons distribution contained in biofuel and the aromatics formation through hydrocracking reaction with the Co-Ni/HZSM-5 catalyst. The formation of aromatics from non-edible vegetable oils, such as: Cerbera manghas, rubber seed, and sunan candlenut oils, containing saturated, mono- and polyunsaturated fatty acids is presented. The hydrocracking reaction was carried out in a pressure batch reactor, a reaction temperature of 350 oC for 2 h, reactor pressure of 15 bar after flowing H2 for 1 hour, and a catalyst/oil ratio of 1 g/200 mL. Liquid hydrocarbon product was analyzed by gas chromatography-mass spectrometry. Based on the GC-MS analysis, hydrocracking on three different oils indicated that polyunsaturated fatty acids were required to produce relatively high aromatics content. The sunan candlenut oil can be converted to gasoil range hydrocarbons containing a small amount of aromatic through hydrocracking reaction. Meanwhile, the aromatics in liquid product from hydrocracking of Cerbera manghas and rubber seed oils were not found. 
Co-Authors Achmad Roesyadi Danawati Hari Prajitno Diah Riski Gusti Edwin Permana Excel Emerlan Samiar Wasistha Ezra Bella Ramadhani Putri Heriyanti Ignatius Gunardi Indra Lasmana Tarigan Intan Lestari Ira Kusuma Dewi, Ira Kusuma Muhammad Al Muttaqii Muhammad Al Muttaqii Muhammad Al-Muttaqii Muhammad Al-Muttaqii Neviaty P Zamani Rahmi Rahmi Reni Desriyanti S.D. S. Murti Septina Is Heriyanti Sri Djangkung Sumbogo Murti Tri Utami Vemileza Putri Wahyudi Zahar Wahyudi Zahar Yoga Andika, Oel Taradepa, Adhitya Eko Bagus