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All Journal Chemistry Indonesian Journal of Chemical Research
Dwi Rasy Mujiyanti
Chemistry Study Program, Mathematic and Natural Sciences Faculty, Lambung Mangkurat University, Banjarbaru, Indonesia
Biochemistry, Genetics & Molecular Biology Chemistry Engineering Environmental Science

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Silica Content Analysis of Rice Husks Siam Unus from South Kalimantan Dwi Rasy Mujiyanti; Dahlena Ariyani; Muna Lisa
Indonesian Journal of Chemical Research Vol 9 No 2 (2021): Edition for September 2021
Publisher : Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam, Universitas Pattimura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30598//ijcr.2020.9-muj

Abstract

Research on the analysis of rice husk content of Siam Unus with various NaOH concentrations (1.0 M; 1.5 M; 2.0 M; 2.5 M; 3.0 M) has been done. This study aims to obtain data on the effect of variations in NaOH concentration on the purity of the silica extract from Siam Unus rice husks and silica characterization of Siam Unus rice husks using Fourier Transform Infra-Red (FTIR) and X-ray fluorescence spectrometry (XRF). The results showed that the combustion of rice husks at 200 °C as the optimum temperature for 1 hour followed by combustion at 600 °C for 4 hours produces grayish-white rice husks with a yield is 20.70%. Silica functional group characterization showed that silanol (Si-OH) and siloxane (Si-O-Si) as dominant functional groups. The result of composition characterization using XRF showed that SiO2 is the dominant compound with the highest percentage of SiO2 is 1.5 M NaOH extract at 42.80%.
Study Effect of Chitosan-Epichlorohydrin Macropore Beads on Decreasing the Value of Total Dissolved Solid (TDS) and Dyes in Sasirangan Liquid Waste Treatment Dahlena Ariyani; Nabila Khairiyatul Hilma; Umi Baroroh Lili Utami; Uripto Trisno Santoso; Dwi Rasy Mujiyanti
Indonesian Journal of Chemical Research Vol 11 No 1 (2023): Edition for May 2023
Publisher : Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam, Universitas Pattimura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30598//ijcr.2023.11-muj

Abstract

Sasirangan liquid waste contains contaminants that are quite dangerous, characterized by high values of total dissolved solids and dyestuffs. This study aims to determine the effect of dose and pH on chitosan-epichlorohydrin macropore beads. The parameters of the measured waste are total dissolved solids and dyestuffs. The process of absorption of sasirangan liquid waste characterizes by FTIR. The results showed that chitosan-epichlorohydrin beads that interacted with sasirangan liquid waste had optimum results at a chitosan dose of 600 mL/L, with a decrease in the total value of dissolved solid by 2161 mg/L and a decrease in dye by 84.78%. Chitosan-epichlorohydrin beads at pH against total dissolved solid gave optimum results at pH 7 with a reduction in the total dissolved solid value of 2269 mg/L, while pH against dyestuffs gave optimum results at pH 3 with a decrease of 94.09%. The interaction between chitosan and chitosan-epichlorohydrin beads occurred a shift in wave numbers from 943 cm-1 to 932 cm-1 showing the C-O-C group and the chitosan-epichlorohydrin beads spectra with waste at wave numbers 3013-3618 cm-1 to 3007-3631 cm-1 the O-H vibration group overlapped the N-H vibration and showed the result that the beads Chitosan-epichlorohydrin/adsorb sasirangan liquid waste.
Co-Authors Dahlena Ariyani Muna Lisa Nabila Khairiyatul Hilma Umi Baroroh Lili Utami Uripto Trisno Santoso