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All Journal International Journal of Advances in Applied Sciences Fullerene Journal of Chemistry
Dinar Rachmadika Baharintasari
Universitas Negeri Malang
Chemistry Earth & Planetary Sciences Environmental Science Materials Science & Nanotechnology Mathematics Physics

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Analisis Kandungan Mineral Pasir Pantai Bajul Mati Kabupaten Malang Menggunakan XRF dan XRD Sumari Sumari; Yana Fajar Prakasa; Muhammad Roy Asrori; Dinar Rachmadika Baharintasari
Jurnal Kimia Fullerene Vol 5 No 2 (2020): Fullerene Journal of Chemistry
Publisher : Fakultas Matematika dan Ilmu Pengetahuan Alam

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.37033/fjc.v5i2.154

Abstract

Mineral exploration in Indonesia has not been evenly distributed, so a study with title analysis of the sand mineral content of Bajul Mati Malang Regency was carried out using XRF and XRD. The aims of this study to determine the percentage of mineral that containing in the sand of Bajul Mati beach in Malang Regency. The instruments used XRF and XRD where the samples were placed in a sample holder and irradiated with X-rays then. The result of analysis of mineral content and metal oxide in Bajul Mati beach sand showed that the beach sand of Bajul Mati has the big potential to be used as a base for making nanomaterials. The results of analysis of XRF showed that the content of SiO2 was 46.7% and the results of analysis of XRD showed that the SiO2 mineral has the quartz phased. Bajul Mati beach sand has the potential to be a source of mineral material.
Sono-hydrolysis of banana stem midrib using HY-zeolite from natural sand-based silica as a catalyst Sumari Sumari; Aman Santoso; Muhammad Roy Asrori; Yana Fajar Prakasa; Dinar Rachmadika Baharintasari
International Journal of Advances in Applied Sciences Vol 11, No 4: December 2022
Publisher : Institute of Advanced Engineering and Science

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (395.964 KB) | DOI: 10.11591/ijaas.v11.i4.pp306-311

Abstract

Banana stem midrib has the potential as a glucose source through catalytic hydrolysis assisted by ultrasonic (sono-hydrolysis). Besides, natural sand-based silica is the potential as raw material for zeolite synthesis. The purpose of the study was to do two things: i) characterize HY-zeolite made from natural sand-based silica and ii) determine whether HY-zeolite is effective for sono-hydrolysis of banana stem midrib. There was a total of four processes that were carried out, including i) the extraction of silica, ii) the synthesis of HY zeolite, iii) the hydrolysis process, and iv) the glucose content test. The results of the study were gained two things: i) The findings of X-ray fluorescence (XRF), X-ray diffraction (XRD), scanning electron microscopy (SEM), and Fourier transform infrared (FTIR) on HY-zeolite are 2.3 Si/Al, obtained 2 theta and d-spacing data similarities for HY-zeolite, and formed T-O-T, O-T-O (T=Si/Al), and Si-OH groups respectively; and ii) HY-zeolite with ultrasonic was effective for hydrolyzing cellulose into glucose at maximum temperature and time, 55 °C and 6 hours.
Silica extract from Malang beach sand via leaching and sol-gel methods Sumari Sumari; Muhammad Roy Asrori; Yana Fajar Prakasa; Dinar Rachmadika Baharintasari; Aman Santoso
International Journal of Advances in Applied Sciences Vol 12, No 1: March 2023
Publisher : Institute of Advanced Engineering and Science

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.11591/ijaas.v12.i1.pp74-81

Abstract

Many silica minerals are found in beach sands. One of its beach sands is in Bajul Mati beach sand which contains high silica. The silica can be extracted using existing methods, but it is less environmentally friendly. In this research, the extracting process of silica from the sand of Bajul Mati beach (South of Java-Indonesia) has been carried out through a method that is low-cost and more environmentally friendly. The purpose of this study was to characterize extracted silica with instrumentation results and economic analysis. The method of extracting silica from beach sand was via leaching and sol-gel methods: i) leaching with 7M HCl,ii) the formation of clear sodium silicate solution (Na2O.SiO2),iii) sol-gel: sodium silicate solution titrated with oxalic acid (H2C2O4) 1 M until pH 6 was obtained and silicite Si(OH)4 was formed, and iv) characterization with X-ray fluorescence (XRF), X-ray diffraction (XRD), Fourier transform infrared (FTIR), and scanning electron microscopy (SEM) with economic analysis. The result showed that extracted silica has a cristobalite structure based on XRD analysis. The purity of silica (% Wt Si) reached 93.9% based on XRF analysis. FTIR analysis has identified silanol, siloxic, and siloxane groups. The SEM analysis shows that silica (SiO2) particles tend to form agglomerations about ∼1 μm. In addition, economic analysis results showed that this method will support implementation in the future, so silica has been produced by this developed method.
Co-Authors Aman Santoso Muhammad Roy Asrori Sumari Sumari Yana Fajar Prakasa