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All Journal JURNAL KIMIA SAINS DAN APLIKASI
Muhammad Rizki Kurniawan
Study Program of Medical Laboratory Technology, Faculty of Science and Technology, Binawan University Jakarta
Chemical Engineering, Chemistry & Bioengineering Chemistry Engineering

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Direct Investigation of Synthesis of Gold Nanoparticles Using Polyscias scutellaria Leaf Extract in the Hexane-Water System Using the Centrifugal Liquid Membrane-Spectrophotometry Method Muhammad Rizki Kurniawan; Aji Humaedi; Ahmad Fitra Ritonga
Jurnal Kimia Sains dan Aplikasi Vol 23, No 7 (2020): Volume 23 Issue 7 Year 2020
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (2495.316 KB) | DOI: 10.14710/jksa.23.7.255-260

Abstract

The Centrifugal liquid Membrane (CLM) method, which provides an ultra-thin two-phase liquid membrane system in a rotating glass cell, was successfully applied to Green Synthesis from Polyscias scutellaria (PS) capped gold nanoparticles (AuNPs-PS) using a Mangkokan leaf (Polyscias scutellaria) extract as a reducing agent and stabilizer in the hexane-water system. PS extract in hexane fraction as the organic phase has a UV absorption spectrum at the maximum wavelength, λmax of 220 nm, while the precursor of HAuCl4 solution as an aqueous phase has an λmax of 214 nm. Investigation of AuNPs-PS formation was carried out at various concentrations of Mangkokan leaf extract concentration; i.e., 0.001 0.003; 0.005; 0.007 and 0.009%, while the reaction was carried out at various rotational speeds of 5,000-9,000 rpm. The formation and stability of AuNPs-PS were observed from the phenomenon of surface plasmon resonance (SPR) and absorbance changes as measured by a UV-Vis spectrophotometer. The results of measurements using CLM-Spectrophotometry shows the formation of AuNPs-PS in the hexane-water system at λmax of 534 nm.
Co-Authors Humaedi, Aji Ritonga, Ahmad Fitra