The Journal of Pure and Applied Chemistry Research
Vol 10, No 2 (2021): Edition May-August 2021

Effect of Calcination Temperature on The Synthesis of Silica from Bagasse

Poedji Loekitowati Hariani (Universitas Sriwijaya)
Fahma Riyanti (Universitas Sriwijaya)
Desneli Desneli (Universitas Sriwijaya)
Fatma Fatma (Universitas Sriwijaya)
Sabila Yunita (Universitas Sriwijaya)
Muhammad Said (Universitas Sriwijaya)



Article Info

Publish Date
31 Aug 2021

Abstract

Bagasse is the solid waste derived from the sugar-making process. A large amount of silica in bagasse is a potential source of silica. In this study, extraction of silica from bagasse was carried out in the following steps: pretreatment of bagasse using HCl solution, followed by calcination at varying temperatures (700℃, 800℃, and 900℃) using a furnace. Furthermore, extraction using NaOH solution and precipitation using HCl. Silica characteristics were obtained using X-Ray Diffraction (XRD), Scanning Electron Microscopy-Electron Dispersive Spectrometry (SEM-EDS), and BET surface area. The results showed that calcination temperature affected the characteristics of the silica produced. The silica extracted at 700℃ produced an amorphous phase with a broad peak at an angle of 2θ = 20-24°. It contained the most considerable silica content and surface area, 42.46% and 796.89 cm2/g, respectively. The extracted silica had an average diameter of 5.67 mm and a pore volume of 1.184 cm3/g.

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Journal Info

Abbrev

jpacr

Publisher

Subject

Chemical Engineering, Chemistry & Bioengineering Chemistry Materials Science & Nanotechnology Medicine & Pharmacology

Description

The Journal of Pure and Applied Chemistry Research focuses in publishing research articles in the field of Chemistry and Applied Chemistry. The target is in exploring, investigating, and developing chemicals sources from local and/or Indonesian to increase the value. Scope of the journal is organic ...