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All Journal The Journal of Pure and Applied Chemistry Research
Desneli Desneli
Universitas Sriwijaya
Chemical Engineering, Chemistry & Bioengineering Chemistry Materials Science & Nanotechnology Medicine & Pharmacology

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Effect of Calcination Temperature on The Synthesis of Silica from Bagasse Poedji Loekitowati Hariani; Fahma Riyanti; Desneli Desneli; Fatma Fatma; Sabila Yunita; Muhammad Said
The Journal of Pure and Applied Chemistry Research Vol 10, No 2 (2021): Edition May-August 2021
Publisher : Chemistry Department, The University of Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/ub.jpacr.2021.010.02.587

Abstract

Bagasse is the solid waste derived from the sugar-making process. A large amount of silica in bagasse is a potential source of silica. In this study, extraction of silica from bagasse was carried out in the following steps: pretreatment of bagasse using HCl solution, followed by calcination at varying temperatures (700℃, 800℃, and 900℃) using a furnace. Furthermore, extraction using NaOH solution and precipitation using HCl. Silica characteristics were obtained using X-Ray Diffraction (XRD), Scanning Electron Microscopy-Electron Dispersive Spectrometry (SEM-EDS), and BET surface area. The results showed that calcination temperature affected the characteristics of the silica produced. The silica extracted at 700℃ produced an amorphous phase with a broad peak at an angle of 2θ = 20-24°. It contained the most considerable silica content and surface area, 42.46% and 796.89 cm2/g, respectively. The extracted silica had an average diameter of 5.67 mm and a pore volume of 1.184 cm3/g.
Co-Authors Fahma Riyanti Fatma Muhammad Said Poedji Loekitowati Hariani Sabila Yunita