Jurnal Matematika & Sains
Vol 22 No 1 (2017)

Sintesis Nanokomposit -Fe2O3/SiO2 dengan Metode Salt-Assisted Spray Pyrolysis untuk Menurunkan Viskositas Minyak Berat

Anrokhi, Mohamad Samsul (Unknown)
Nuryadin, Bebeh Wahid (Unknown)
Abdullah, Mikrajuddin (Unknown)
Khairurrijal, Khairurrijal (Unknown)
Iskandar, Ferry (Unknown)



Article Info

Publish Date
22 Aug 2017

Abstract

A α-Fe2O3/SiO2 nanocomposite as aquathermolisys catalyst material at heavy oil has been synthesized and optimized by using  Salt-Assisted Spray Pyrolysis method. The α-Fe2O3/SiO2 nanocomposite is obtained by thermal decomposition from the precursor.  The precursor is made of FeCl3, SiO2 and NaCl and water as a solvent. Concentration of FeCl3, SiO2, and NaCl are 1:1:5 in order. the composition of SiO2 in the composite is 0%, 25% and 50% of total mass, respectively. the droplets were transported to the furnace reactor using air as a carrier gas with a fixed flow rate at 5 liter/min and the furnace’s temperature is 800 °C in order to get the pyrolysis reaction. The resulted powder is then characterized by using XRD, SEM and Chatalytic aquathermolysis test. The result of XRD characterization shows that crystal peaks of α-Fe2O3 has been formed. SEM result shows nanocomposite morphology of α-Fe2O3/SiO2 with circle particle form with average particle diametre of α-Fe2O3, SiO2 25% and SiO2 50% of total mass are 765 nm, 850 nm, and 746 nm, respectively. Catalytic Aquathermolysis test showed catalyst α-Fe2O3/SiO2 50%  has catalytic properties better than catalytic properties of α-Fe2O3/SiO2 and α-Fe2O3/SiO2 25%.

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