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The Effect of Surfactant Characteristics on IFT to Improve Oil Recovery in Tempino Light Oil Field Indonesia Swadesi, Boni; Marhaendrajana, Taufan; Mucharam, Leksono; Siregar, H.P. Septoratno
Journal of Engineering and Technological Sciences Vol 47, No 3 (2015)
Publisher : ITB Journal Publisher, LPPM ITB

Water injection has been employed in the Tempino oil field since 1996. The current oil recovery factor is 35% of OOIP. Even though the pressure is still high, the oil production rate has declined rapidly and the water cut is approaching 89%. In order to mobilizeÂ theÂ oil from theÂ reservoirÂ more effectively, surfactant flooding is one of the solutions that can reduce residual oil saturation. Interaction between crude oil and compatible surfactant generates microemulsion,Â as an indication of low interfacial tension. Hence the oil is expected to move out of the pore throat easily. In this research, thirty types of surfactantsÂ were evaluated. The hydrophilicÂ lipophilicÂ balance (HLB)Â was calculated andÂ theÂ interfacial tension (IFT)Â with theÂ reservoir fluidÂ was measured. HLB criteria were established as an indicator of low IFT, which was then tested for Berea core flooding. The results indicate that an HLB between approximately 2.7 and 3.1 (on Daviesâ Scale) or greater than 11.5 (on Griffinâs Scale) givesÂ low IFTÂ (~10-3 dynes/cm).Â This characteristicÂ is possesed by surfactantÂ ethoxyÂ carboxylateÂ with aÂ linear hydrophobic structure.Â This surfactant produces a high incremental oil recovery according to Berea core flood tests. The AN2NS and AN3 surfactants recovered 90% and 86% of OOIP respectively.

Surfactant-Polymer Coreflood Simulation and Uncertainty Analysis Derived from Laboratory Study Hakiki, Farizal; Maharsi, Dara Ayuda; Marhaendrajana, Taufan
Journal of Engineering and Technological Sciences Vol 47, No 6 (2015)
Publisher : ITB Journal Publisher, LPPM ITB

This paper presents a numerical simulation study on coreflood scale derived from a laboratory study conducted on light oil and water-wet sandstone samples from fields at Tempino and Kenali Asam, Sumatra, Indonesia. A rigorous laboratory study prompted a specified surfactant type among dozens of screened samples, i.e. AN3NS and AN2NS-M for Kenali Asam and Tempino, respectively. The coreflood scale numerical simulation study was performed using a commercial simulator, on the basis of the results from the laboratory study, at a constant temperature of 68Â°C, 0.3 cc/min injection rate and under 120 psia confining pressure. To get better recovery, the cores were tested using surfactant and polymer in a blended mode, containing 0.03% w/w polymer diluted in each field brine, which accommodated around 8000 ppm salinity. The most significant variable in the multiphase flow is the relative permeability curve, which is affected by interfacial tension (IFT) during waterflooding and surfactant-polymer (SP) flooding. This study shows that relative permeability will be shifted at ultra-low IFT (10-3 to 10-4 mN/m). This shifting phenomenon is governed by the interpolation parameter set, which implicitly represents the capillary number. Further work in matching the numerical results to the coreflood was conducted by changing the interpolation parameters.

Wettability Alteration Induced by Surface Roughening During Low Salinity Waterflooding Marhaendrajana, Taufan; Ridwan, Muhammad Ghifari; Kamil, Maulana Insan; Permadi, Pudji
Journal of Engineering and Technological Sciences Vol 50, No 5 (2018)
Publisher : ITB Journal Publisher, LPPM ITB

Wettability alteration during low salinity waterflooding (LSW) is expected to be one of the prominent reasons for enhanced oil recovery. However, the underlying mechanisms of improved oil recovery in sandstone during LSW are not entirely clear. Thus, a series of experiments was carried out to investigate the underlying mechanisms that drive the wettability alteration. FTIR spectroscopy was combined with thermogravimetric analysis to quantify the amount of adsorbed hydrocarbon components in sandstone with various clay contents. Afterward, the time-dependent contact angle in fabricated sandstone substrate (RMS roughness 9.911.31) was observed with various clay and brine contents to monitor the wettability alteration during LSW. The existence of divalent ions (Ca2+ and Mg2+) was found to stabilize the sandstone and prevent it from swelling. Surprisingly, with the presence of divalent ions, the rate of contact angle change was insignificant (, even though a reduction of divalent ions occurred and the rate of contact angle change with the sole presence of NaCl was notably altered (. Furthermore, the presence of higher clay content showed an increased contact angle alteration. We propose that these phenomena are partially driven by macroscopic phenomena of clay swelling, which leads to surface roughening and enhances the water-wetness.

The Effect of Surfactant Characteristics on IFT to Improve Oil Recovery in Tempino Light Oil Field Indonesia Boni Swadesi; Taufan Marhaendrajana; Leksono Mucharam; H.P. Septoratno Siregar
Journal of Engineering and Technological Sciences Vol. 47 No. 3 (2015)
Publisher : Institute for Research and Community Services, Institut Teknologi Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.5614/j.eng.technol.sci.2015.47.3.2

Water injection has been employed in the Tempino oil field since 1996. The current oil recovery factor is 35% of OOIP. Even though the pressure is still high, the oil production rate has declined rapidly and the water cut is approaching 89%. In order to mobilize the oil from the reservoir more effectively, surfactant flooding is one of the solutions that can reduce residual oil saturation. Interaction between crude oil and compatible surfactant generates microemulsion, as an indication of low interfacial tension. Hence the oil is expected to move out of the pore throat easily. In this research, thirty types of surfactants were evaluated. The hydrophilic lipophilic balance (HLB) was calculated and the interfacial tension (IFT) with the reservoir fluid was measured. HLB criteria were established as an indicator of low IFT, which was then tested for Berea core flooding. The results indicate that an HLB between approximately 2.7 and 3.1 (on Davies' Scale) or greater than 11.5 (on Griffin's Scale) gives low IFT (~10-3 dynes/cm). This characteristic is possesed by surfactant ethoxy carboxylate with a linear hydrophobic structure. This surfactant produces a high incremental oil recovery according to Berea core flood tests. The AN2NS and AN3 surfactants recovered 90% and 86% of OOIP respectively.

Surfactant-Polymer Coreflood Simulation and Uncertainty Analysis Derived from Laboratory Study Farizal Hakiki; Dara Ayuda Maharsi; Taufan Marhaendrajana
Journal of Engineering and Technological Sciences Vol. 47 No. 6 (2015)
Publisher : Institute for Research and Community Services, Institut Teknologi Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.5614/j.eng.technol.sci.2015.47.6.9

This paper presents a numerical simulation study on coreflood scale derived from a laboratory study conducted on light oil and water-wet sandstone samples from fields at Tempino and Kenali Asam, Sumatra, Indonesia. A rigorous laboratory study prompted a specified surfactant type among dozens of screened samples, i.e. AN3NS and AN2NS-M for Kenali Asam and Tempino, respectively. The coreflood scale numerical simulation study was performed using a commercial simulator, on the basis of the results from the laboratory study, at a constant temperature of 68°C, 0.3 cc/min injection rate and under 120 psia confining pressure. To get better recovery, the cores were tested using surfactant and polymer in a blended mode, containing 0.03% w/w polymer diluted in each field brine, which accommodated around 8000 ppm salinity. The most significant variable in the multiphase flow is the relative permeability curve, which is affected by interfacial tension (IFT) during waterflooding and surfactant-polymer (SP) flooding. This study shows that relative permeability will be shifted at ultra-low IFT (10-3 to 10-4 mN/m). This shifting phenomenon is governed by the interpolation parameter set, which implicitly represents the capillary number. Further work in matching the numerical results to the coreflood was conducted by changing the interpolation parameters.

Wettability Alteration Induced by Surface Roughening During Low Salinity Waterflooding Taufan Marhaendrajana; Muhammad Ghifari Ridwan; Maulana Insan Kamil; Pudji Permadi
Journal of Engineering and Technological Sciences Vol. 50 No. 5 (2018)
Publisher : Institute for Research and Community Services, Institut Teknologi Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.5614/j.eng.technol.sci.2018.50.5.4

Wettability alteration during low salinity waterflooding (LSW) is expected to be one of the prominent reasons for enhanced oil recovery. However, the underlying mechanisms of improved oil recovery in sandstone during LSW are not entirely clear. Thus, a series of experiments was carried out to investigate the underlying mechanisms that drive the wettability alteration. FTIR spectroscopy was combined with thermogravimetric analysis to quantify the amount of adsorbed hydrocarbon components in sandstone with various clay contents. Afterward, the time-dependent contact angle in fabricated sandstone substrate (RMS roughness 9.911.31) was observed with various clay and brine contents to monitor the wettability alteration during LSW. The existence of divalent ions (Ca2+ and Mg2+) was found to stabilize the sandstone and prevent it from swelling. Surprisingly, with the presence of divalent ions, the rate of contact angle change was insignificant (, even though a reduction of divalent ions occurred and the rate of contact angle change with the sole presence of NaCl was notably altered (. Furthermore, the presence of higher clay content showed an increased contact angle alteration. We propose that these phenomena are partially driven by macroscopic phenomena of clay swelling, which leads to surface roughening and enhances the water-wetness.

Correlation between Phase Behavior and Interfacial Tension for Mixtures of Amphoteric and Nonionic Surfactant with Waxy Oil Rani Kurnia; Deana Wahyuningrum; Doddy Abdassah; Taufan Marhaendrajana
Journal of Engineering and Technological Sciences Vol. 53 No. 5 (2021)
Publisher : Institute for Research and Community Services, Institut Teknologi Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.5614/j.eng.technol.sci.2021.53.5.1

Phase behavior tests in the surfactant screening process for EOR applications remain one of the relatively convenient ways to design an optimum surfactant formulation. However, phase behavior studies are unable to provide quantitative data for interfacial tension, which is one of the parameters that must be considered when selecting surfactants for EOR. Several studies related to the prediction of interfacial tension through phase behavior testing have been carried out. In this paper, the Huh correlation was used to estimate the interfacial tension value based on phase behavior tests. It was found that the current form of the Huh correlation may be applied for the below-to-optimum salinity condition. Furthermore, the constants of the equation vary depending on the surfactant type and mixtures.

Hasil Studi Laboratorium Penentuan Karakteristik Alamiah Surfaktan Natrium Lignosulfonat Dari Ampas Tebu Sebagai Fluida Injeksi Di Reservoir Minyak Rini Setiati; Septoratno Siregar; Taufan Marhaendrajana; Deana Wahyuningrum
JURNAL PENELITIAN DAN KARYA ILMIAH LEMBAGA PENELITIAN UNIVERSITAS TRISAKTI Vol. 3 No. 1 (2018)
Publisher : Lembaga Penelitian dan Pengabdian kepada Masyarakat Universitas Trisakti

Surfaktan Natrium Lignosulfonat (NaLS) dari ampas tebu merupakan salah satu pengembangan surfaktan lignosulfonat yang dibuat dari limbah nabati, yaitu adalah ampas tebu. Pada studi ini telah diperoleh hasil sintesa ampas tebu menjadi surfaktan lignosulfonat yang jika dikembangkan akan dapat menjadi alternatif surfaktan sebagai fluida injesi di reservoir minyak. Dari hasil penelitian dan pengujian yang telah dilakukan, surfaktan NaLS ampas tebu ini mempunyai kesamaan komponen dengan surfaktan lignosulfonat standar yaitu terdiri dari gugus ulur alkena, gugus ulur sulfonat, gugus tekuk karboksilat dan gugus tekuk ester. Berdasarkan analisis spektrum NMR, molekul monomer lignosulfonat tersebut mempunyai atom C, O, H dan S di dalam dengan jumlah atom C = 11, O = 8, H = 16, dan S = 1, sehingga rumus empiris monomer lignosulfonat adalah (C11H16O8S)n, dengan massa molekul relatif 308,06. Berdasarkan struktur monomer lignosulfonat ampas tebu, maka gugus-gugus fungsi dalam strukturnya dapat dikelompokkan sebagai gugus hidrofil atau gugus hidrofob dan dapat dihitung nilai HLB (Hidrofil-lipofilik Balance) yang dimiliki oleh surfaktan NaLS ampas tebu tersebut yaitu sebesar 11,62. Dengan nilai HLB ini maka surfaktan NaLS ampas tebu ini sesuai penggunaannya sebagai sistem tipe emulsi O/W (oil in water), yang berarti surfaktan tersebut larut dalam air dan dapat digunakan sebagai fluida injeksi.

Hasil Studi Laboratorium Penentuan Karakteristik Alamiah Surfaktan Natrium Lignosulfonat Dari Ampas Tebu Sebagai Fluida Injeksi Di Reservoir Minyak Rini Setiati; Septoratno Siregar; Taufan Marhaendrajana; Deana Wahyuningrum
JURNAL PENELITIAN DAN KARYA ILMIAH LEMBAGA PENELITIAN UNIVERSITAS TRISAKTI Vol. 3 No. 1 (2018)
Publisher : Lembaga Penelitian dan Pengabdian kepada Masyarakat Universitas Trisakti

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25105/pdk.v3i1.2483

Surfaktan Natrium Lignosulfonat (NaLS) dari ampas tebu merupakan salah satu pengembangan surfaktan lignosulfonat yang dibuat dari limbah nabati, yaitu adalah ampas tebu. Pada studi ini telah diperoleh hasil sintesa ampas tebu menjadi surfaktan lignosulfonat yang jika dikembangkan akan dapat menjadi alternatif surfaktan sebagai fluida injesi di reservoir minyak. Dari hasil penelitian dan pengujian yang telah dilakukan, surfaktan NaLS ampas tebu ini mempunyai kesamaan komponen dengan surfaktan lignosulfonat standar yaitu terdiri dari gugus ulur alkena, gugus ulur sulfonat, gugus tekuk karboksilat dan gugus tekuk ester. Berdasarkan analisis spektrum NMR, molekul monomer lignosulfonat tersebut mempunyai atom C, O, H dan S di dalam dengan jumlah atom C = 11, O = 8, H = 16, dan S = 1, sehingga rumus empiris monomer lignosulfonat adalah (C11H16O8S)n, dengan massa molekul relatif 308,06. Berdasarkan struktur monomer lignosulfonat ampas tebu, maka gugus-gugus fungsi dalam strukturnya dapat dikelompokkan sebagai gugus hidrofil atau gugus hidrofob dan dapat dihitung nilai HLB (Hidrofil-lipofilik Balance) yang dimiliki oleh surfaktan NaLS ampas tebu tersebut yaitu sebesar 11,62. Dengan nilai HLB ini maka surfaktan NaLS ampas tebu ini sesuai penggunaannya sebagai sistem tipe emulsi O/W (oil in water), yang berarti surfaktan tersebut larut dalam air dan dapat digunakan sebagai fluida injeksi.

OPTIMASI PEMISAHAN LIGNIN AMPAS TEBU DENGAN MENGGUNAKAN NATRIUM HIDROKSIDA Rini Setiati; Deana Wahyuningrum; Septoratno Siregar; Taufan Marhaendrajana
ETHOS (Jurnal Penelitian dan Pengabdian) Vol 4 No.2 (Juni, 2016) Ethos: Jurnal Penelitian dan Pengabdian (Sains & Teknologi)
Publisher : Universitas Islam Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29313/ethos.v0i0.1970

Lignin atau zat kayu adalah salah satu zat komponen penyusun tumbuhan. Komposisi bahan penyusun ini berbeda-beda bergantung jenisnya. Lignin terutama terakumulasi pada batang tumbuhan berbentuk pohon dan semak. Pada batang, lignin berfungsi sebagai bahan pengikat komponen penyusun lainnya, sehingga suatu pohon bisa berdiri tegak (seperti semen pada sebuah batang beton). Lignin merupakan bahan baku pembentuk Lignosulfonat. Lignosulfonat adalah salah satu jenis surfaktan anionik yang dapat digunakan sebagai bahan baku injeksi dalam metoda Injeksi Surfaktan untuk meningkatkan perolehan produksi minyak pada industri perminyakan. Ampas tebu adalah salah satu bahan limbah yang di dalamnya masih terdapat lignin. Ampas tebu adalah hasil samping dari proses ekstraksi cairan tebu. Ampas tebu yang dipergunakan adalah ampas tebu yang telah mengalami proses penggilingan ke lima kali dari proses pembuatan gula. Selama ini ampas tebu digunakan sebagai bahan bakar pabrik gula dan pakan ternak. Dengan proses pemisahan lignin dari ampas tebu ini dapat memberi nilai tambah pemanfaatan ampas tebu sekaligus sebagai alternatif pengolahan ampas tebu sebagai limbah pabrik gula. Salah satu metoda yang digunakan untuk memisahkan lignin dari ampas tebu adalah dengan menggunakan reagen Natrium Hidroksida. Dalam penelitian ini proses hidrolisis lignoselulosa dari ampas tebu menjadi lignin menggunakan variasi konsentrasi natrium hidroksida (NaOH) dan variasi ukuran serbuk ampas tebu. Hasil lignin yang terbentuk dikarakterisasi dengan metode spektroskopi FTIR untuk menentukan gugus-gugus fungsi khas yang terdapat pada struktur lignin dan dibandingkan dengan spektrum FTIR lignin komersial standar sehingga dapat diketahui optimasi pemisahan lignin tersebut.

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